Methods of Analysis for Petrochemicals

Methods of Analysis for Petrochemicals PDF Author: Edwin Robert Littmann
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 392

Get Book

Book Description
CONTENTS - Distillation of Naphtha, Gasoline, Kerosene, Jet Fuel and Similar Products - Vacuum Distillation - Distillation of Aromatic Hydrocarbons - Determination of High-Boiling Fractions in Isopropyl Ether - Test for Light Ends in Isobutylene and Similar Products - Flash Point by the Tag Closed Tester (Abel Flash Point) - Flash and Fire Points by the Cleveland Open Cup (Marcusson Flash Point) - Flash Point by the Pensky-Martens Closed Tester - Determining the Nonvolatile Matter in CTLA Polymers - Rapid Method for Comparative Evaporation Rates of Solvents - Gravity of Petroleum Products by the Hydrometer - Specific Gravity by Means of the Pycnometer - Viscosity Determination by the Saybolt Viscometer - Determination of the Kinematic Viscosity of Petroleum Products by Glass Viscometers - Color of Petroleum Products by the Tag-Robinson Colorimeter (Color Stability of Lubricants) - Color of White Petroleum Products by the Saybolt Chromometer - Determining the Color of Solvents by the Platinum-Cobalt System - Gardner's Method of Determining the Color of Solvents - Determination of the Acid Wash Color of Industrial Aromatic Hydrocarbons - Sulfur by Lamp (Closed System) - Doctor Test - Determination of Sulfur in Petroleum Products - Heavier than Illuminating Oils - Qualitative Detection of Sulfur Gases in Industrial Aromatic Hydrocarbons - Detection of Thiophene in Benzene - Ash and Water-Soluble Ash Content of Petroleum Oils - Cloud and Pour Points of Petroleum Products (Dilute Pour Point) - Detecting Oxidizable Matter in Solvents (Permanganate Test) - Permanaganate Time Test (Improved Visual Method) - Holde Hard Asphalt Test - Determination of the Gumming Properties of Gasoline by Means of a Copper Dish - Determination of Water in Petroleum Products by the Karl Fischer Reagent - Determination of Water in Hydrocarbon Gases by the Karl Fischer Reagent - Acidity of Industrial Aromatic Hydrocarbons - Determination of the Unsaponifiable Matter in, and the Neutralization Number of, Naphthenic Acids - Aniline Point - Wijs' Iodine Number - Bromine Number (Lewis and Bradstreet Method) - Determination of the Bromine Index of Xylene - Determination of the Available Cyclopentadiene and Methylcyclopentadienes in Dimers - Determination of Cyclopentadiene in Isoprene - Determination of the Total Conjugated Diolefin Content of Isoprene - Complete Analysis of Distilled Isobutylene by Infrared Spectrometry - Solubility of Pentachlorophenol in Petroleum Oils - Determination of Lower Ketones - Determination of the Alcohol Content by Acetylation - Water Dilution of Alcohol - Determination of Alcohol Content by Specific Gravity - Test for Mixed Alcohols (Hydroxyl Number) - Acetone in Isopropyl Alcohol by Ultraviolet Spectrometry - Ester Content of Solvents - Tests for Specification Grades of Ethyl Ether - Determination of the Carbonyl Compounds in Petrochemical Products (Carbonyl Number) - Determination of Peroxides in Isopropyl Ether - Peroxide Number of Petroleum Products - Determination of the Residual Odor of Heavy Petroleum Solvents - Amino-Type Inhibitors in Gasoline - Determination of tert-Butylcatechol Inhibitor in Unsaturated Heavy Hydrocarbons - Flash Point by the Tag Open Cup-a-Naphthol in Ether - Sampling and Testing Lacquer Solvents and Diluents - Index -

Methods of Analysis for Petrochemicals

Methods of Analysis for Petrochemicals PDF Author: Edwin Robert Littmann
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 392

Get Book

Book Description
CONTENTS - Distillation of Naphtha, Gasoline, Kerosene, Jet Fuel and Similar Products - Vacuum Distillation - Distillation of Aromatic Hydrocarbons - Determination of High-Boiling Fractions in Isopropyl Ether - Test for Light Ends in Isobutylene and Similar Products - Flash Point by the Tag Closed Tester (Abel Flash Point) - Flash and Fire Points by the Cleveland Open Cup (Marcusson Flash Point) - Flash Point by the Pensky-Martens Closed Tester - Determining the Nonvolatile Matter in CTLA Polymers - Rapid Method for Comparative Evaporation Rates of Solvents - Gravity of Petroleum Products by the Hydrometer - Specific Gravity by Means of the Pycnometer - Viscosity Determination by the Saybolt Viscometer - Determination of the Kinematic Viscosity of Petroleum Products by Glass Viscometers - Color of Petroleum Products by the Tag-Robinson Colorimeter (Color Stability of Lubricants) - Color of White Petroleum Products by the Saybolt Chromometer - Determining the Color of Solvents by the Platinum-Cobalt System - Gardner's Method of Determining the Color of Solvents - Determination of the Acid Wash Color of Industrial Aromatic Hydrocarbons - Sulfur by Lamp (Closed System) - Doctor Test - Determination of Sulfur in Petroleum Products - Heavier than Illuminating Oils - Qualitative Detection of Sulfur Gases in Industrial Aromatic Hydrocarbons - Detection of Thiophene in Benzene - Ash and Water-Soluble Ash Content of Petroleum Oils - Cloud and Pour Points of Petroleum Products (Dilute Pour Point) - Detecting Oxidizable Matter in Solvents (Permanganate Test) - Permanaganate Time Test (Improved Visual Method) - Holde Hard Asphalt Test - Determination of the Gumming Properties of Gasoline by Means of a Copper Dish - Determination of Water in Petroleum Products by the Karl Fischer Reagent - Determination of Water in Hydrocarbon Gases by the Karl Fischer Reagent - Acidity of Industrial Aromatic Hydrocarbons - Determination of the Unsaponifiable Matter in, and the Neutralization Number of, Naphthenic Acids - Aniline Point - Wijs' Iodine Number - Bromine Number (Lewis and Bradstreet Method) - Determination of the Bromine Index of Xylene - Determination of the Available Cyclopentadiene and Methylcyclopentadienes in Dimers - Determination of Cyclopentadiene in Isoprene - Determination of the Total Conjugated Diolefin Content of Isoprene - Complete Analysis of Distilled Isobutylene by Infrared Spectrometry - Solubility of Pentachlorophenol in Petroleum Oils - Determination of Lower Ketones - Determination of the Alcohol Content by Acetylation - Water Dilution of Alcohol - Determination of Alcohol Content by Specific Gravity - Test for Mixed Alcohols (Hydroxyl Number) - Acetone in Isopropyl Alcohol by Ultraviolet Spectrometry - Ester Content of Solvents - Tests for Specification Grades of Ethyl Ether - Determination of the Carbonyl Compounds in Petrochemical Products (Carbonyl Number) - Determination of Peroxides in Isopropyl Ether - Peroxide Number of Petroleum Products - Determination of the Residual Odor of Heavy Petroleum Solvents - Amino-Type Inhibitors in Gasoline - Determination of tert-Butylcatechol Inhibitor in Unsaturated Heavy Hydrocarbons - Flash Point by the Tag Open Cup-a-Naphthol in Ether - Sampling and Testing Lacquer Solvents and Diluents - Index -

Guide to ASTM Test Methods for the Analysis of Petroleum Products and Lubricants

Guide to ASTM Test Methods for the Analysis of Petroleum Products and Lubricants PDF Author: R. A. Nadkarni
Publisher: Astm International
ISBN: 9780803120877
Category : Technology & Engineering
Languages : en
Pages : 389

Get Book

Book Description
Summarizes the essential elements of all analytical tests used to characterize petroleum products. The 350 plus entries are alphabetically arranged by chemical and physical properties, such as apparent viscosity, density, metal analysis, sulfur determination, vapor pressure, and water. Each entry co

Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring

Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring PDF Author: Melissa N. Dunkle
Publisher: John Wiley & Sons
ISBN: 1119523303
Category : Science
Languages : en
Pages : 464

Get Book

Book Description
A thorough introduction to environmental monitoring in the oil and gas industry Analytical Techniques in the Oil and Gas Industry for Environmental Monitoring examines the analytical side of the oil and gas industry as it also provides an overall introduction to the industry. You’ll discover how oil and natural gas are sourced, refined, and processed. You can learn about what’s produced from oil and natural gas, and why evaluating these sourced resources is important. The book discusses the conventional analyses for oil and natural gas feeds, along with their limitations. It offers detailed descriptions of advanced analytical techniques that are commercially available, plus explanations of gas and oil industry equipment and instrumentation. You’ll find technique descriptions supplemented with a list of references as well as with real-life application examples. With this book as a reference, you can prepare to apply specific analytical methods in your organization’s lab environment. Analytical Techniques can also serve as your comprehensive resource on key techniques in the characterization of oil and gas samples, within both refinery and environmental contexts. Understand of the scope of oil and gas industry techniques available Consider the benefits and limitations of each available process Prepare for applying analytical techniques in your lab See real examples and a list of references for each technique Read descriptions of off-line analytics, as well as on-line and process applications As a chemist, engineer, instructor, or student, this book will also expand your awareness of the role these techniques have in environmental monitoring and environmental impact assessments.

Corrosion in the Petrochemical Industry, Second Edition

Corrosion in the Petrochemical Industry, Second Edition PDF Author:
Publisher: ASM International
ISBN: 1627080945
Category : Technology & Engineering
Languages : en
Pages : 426

Get Book

Book Description
Originally published in 1994, this second edition of Corrosion in the Petrochemical Industry collects peer-reviewed articles written by experts in the field of corrosion that were specifically chosen for this book because of their relevance to the petrochemical industry. This edition expands coverage of the different forms of corrosion, including the effects of metallurgical variables on the corrosion of several alloys. It discusses protection methods, including discussion of corrosion inhibitors and corrosion resistance of aluminum, magnesium, stainless steels, and nickels. It also includes a section devoted specifically to petroleum and petrochemical industry related issues.

Industrial Energy Management

Industrial Energy Management PDF Author: Victor Kaiser
Publisher: Editions TECHNIP
ISBN: 9782710806455
Category : Business & Economics
Languages : en
Pages : 150

Get Book

Book Description
This monography presents the tools available for the follow-up and the analysis of the energy input to the refining and petrochemicals industries. The first part familiarizes the reader with energy accounting in a production plant. This analytic accounting presents separately the quantitative, qualitative and economic aspects of using energy. The second part treats of the thermodynamic analysis of energy input based on the exergy (available work) balances. Apart from leading to a judgement of how efficiently the energy is put to work in the applied technology, the reader also finds a guide to distillation column sequencing and heat exchange network synthesis. The thermoeconomics are also dealt with. This book is written for the practicing engineer in industry and for the postgraduate students.

Analytical Methods in Petroleum Upstream Applications

Analytical Methods in Petroleum Upstream Applications PDF Author: Cesar Ovalles
Publisher: CRC Press
ISBN: 1482230887
Category : Science
Languages : en
Pages : 337

Get Book

Book Description
Effective measurement of the composition and properties of petroleum is essential for its exploration, production, and refining; however, new technologies and methodologies are not adequately documented in much of the current literature. Analytical Methods in Petroleum Upstream Applications explores advances in the analytical methods and instrument

Efficient Petrochemical Processes

Efficient Petrochemical Processes PDF Author: Frank (Xin X.) Zhu
Publisher: John Wiley & Sons
ISBN: 1119487870
Category : Technology & Engineering
Languages : en
Pages : 432

Get Book

Book Description
A GUIDE TO THE DESIGN, OPERATION, CONTROL, TROUBLESHOOTING, OPTIMIZATION AS WELL AS THE RECENT ADVANCES IN THE FIELD OF PETROCHEMICAL PROCESSES Efficient Petrochemical Processes: Technology, Design and Operation is a guide to the tools and methods for energy optimization and process design. Written by a panel of experts on the topic, the book highlights the application of these methods on petrochemical technology such as the aromatics process unit. The authors describe practical approaches and tools that focus on improving industrial energy efficiency, reducing capital investment, and optimizing yields through better design, operation, and optimization. The text is divided into sections that cover the range of essential topics: petrochemical technology description; process design considerations; reaction and separation design; process integration; process system optimization; types of revamps; equipment assessment; common operating issues; and troubleshooting case analysis. This important book: Provides the basic knowledge related to fundamentals, design, and operation for petrochemical processes Applies process integration techniques and optimization techniques that improve process design and operations in the petrochemical process Provides practical methods and tools for industrial practitioners Puts the focus on improving industrial energy efficiency, reducing capital investment, and optimizing yields Contains information on the most recent advances in the field. Written for managers, engineers, and operators working in process industries as well as university students, Efficient Petrochemical Processes: Technology, Design and Operation explains the most recent advances in the field of petrochemical processes and discusses in detail catalytic and adsorbent materials, reaction and separation mechanisms.

Developments Towards the Comprehensive Analysis of Petrochemical Streams

Developments Towards the Comprehensive Analysis of Petrochemical Streams PDF Author: Johannes Hendrik Wium Potgieter
Publisher:
ISBN:
Category :
Languages : en
Pages :

Get Book

Book Description
Pertrochemical products derived from crude oil and Fischer-Tropsch (FT) processes contain a variety of compounds over a wide carbon number range and a large number of fuels and chemicals are produced during product workup. The characterisation of these fuels and chemicals as well as intermediate process streams is very important to control conversion processes. The analysis of any one of these phases is very challenging. Typical oil phase samples may contain thousands of compounds. In many cases, complete characterisation of these complex samples is possible with comprehensive two-dimensional gas chromatography (GCAÌ30́4GC), but even with the increase in separation power obtained by comprehensive GC, peak co-elution still occurs when complex samples are analysed. In this work chromatographic techniques were investigated and the hyphenation of these techniques was evaluated, addressing some of the remaining analytical challenges in petrochemical analysis. The on-line hyphenation of supercritical fluid chromatography (SFC) to a GCAÌ30́4GC system as a pre-separation technique was successfully developed to address the challenge of the separation between cyclic and non-cyclic alkenes and alkanes. The developed SFC preseparation method also pre-separated the sample of interest into other chemical groups (saturates, unsaturates, oxygenates and aromatics) for further characterisation by GCAÌ30́4GC. On-line hydrogenation after GCAÌ30́4GC separation was successfully developed to address the challenge of distinguishing between isomeric cyclic and double bond containing compounds with the same (two or more) double bond equivalents. The number of rings and alkene double bonds in specific compounds could be determined from the mass spectra of the compounds before and after hydrogenation in a complex petrochemical sample requiring GCAÌ30́4GC separation. A high temperature (HT)-GCAÌ30́4GC method was developed to replace titrimetric procedures traditionally used for the control of oxidation processes of heavy paraffinic fractions. The advantages of the developed HT-GCAÌ30́4GC method include the selective quantification of oxygenate classes and obtaining the concentration for each oxygenate class by carbon number. This allows the optimisation of conditions used to oxidise heavy paraffinic fractions. The challenge of the identification of oxygenates in these oxidised heavy paraffinic fractions was also addressed with the development of a method that pre-separates the oxygenates before subsequent analysis by gas chromatography mass spectrometry, with the use of a supersonic molecular beam (GC-SMB-MS). The EI spectra with enhanced molecular ions obtained by GC-SMB-MS aided tremendously in the identification of oxygenates and the advantage of this procedure was illustrated, whereby the heavy oxygenates in an oxidised heavy paraffinic sample could be better identified. This study successfully addressed various analytical challenges in the field of petrochemical analysis and the developed techniques may be useful for the comprehensive characterisation of various streams in other areas of petrochemical analysis.

Efficient Petrochemical Processes

Efficient Petrochemical Processes PDF Author: Frank (Xin X.) Zhu
Publisher: John Wiley & Sons
ISBN: 1119487889
Category : Technology & Engineering
Languages : en
Pages : 853

Get Book

Book Description
A GUIDE TO THE DESIGN, OPERATION, CONTROL, TROUBLESHOOTING, OPTIMIZATION AS WELL AS THE RECENT ADVANCES IN THE FIELD OF PETROCHEMICAL PROCESSES Efficient Petrochemical Processes: Technology, Design and Operation is a guide to the tools and methods for energy optimization and process design. Written by a panel of experts on the topic, the book highlights the application of these methods on petrochemical technology such as the aromatics process unit. The authors describe practical approaches and tools that focus on improving industrial energy efficiency, reducing capital investment, and optimizing yields through better design, operation, and optimization. The text is divided into sections that cover the range of essential topics: petrochemical technology description; process design considerations; reaction and separation design; process integration; process system optimization; types of revamps; equipment assessment; common operating issues; and troubleshooting case analysis. This important book: Provides the basic knowledge related to fundamentals, design, and operation for petrochemical processes Applies process integration techniques and optimization techniques that improve process design and operations in the petrochemical process Provides practical methods and tools for industrial practitioners Puts the focus on improving industrial energy efficiency, reducing capital investment, and optimizing yields Contains information on the most recent advances in the field. Written for managers, engineers, and operators working in process industries as well as university students, Efficient Petrochemical Processes: Technology, Design and Operation explains the most recent advances in the field of petrochemical processes and discusses in detail catalytic and adsorbent materials, reaction and separation mechanisms.

Risk Analysis and Control for Industrial Processes - Gas, Oil and Chemicals

Risk Analysis and Control for Industrial Processes - Gas, Oil and Chemicals PDF Author: Hans J Pasman
Publisher: Butterworth-Heinemann
ISBN: 0128009128
Category : Technology & Engineering
Languages : en
Pages : 493

Get Book

Book Description
Risk Analysis and Control for Industrial Processes - Gas, Oil and Chemicals provides an analysis of current approaches for preventing disasters, and gives readers an overview on which methods to adopt. The book covers safety regulations, history and trends, industrial disasters, safety problems, safety tools, and capital and operational costs versus the benefits of safety, all supporting project decision processes. Tools covered include present day array of risk assessment, tools including HAZOP, LOPA and ORA, but also new approaches such as System-Theoretic Process Analysis (STPA), Blended HAZID, applications of Bayesian data analytics, Bayesian networks, and others. The text is supported by valuable examples to help the reader achieve a greater understanding on how to perform safety analysis, identify potential issues, and predict the likelihood they may appear. Presents new methods on how to identify hazards of low probability/high consequence events Contains information on how to develop and install safeguards against such events, with guidance on how to quantify risk and its uncertainty, and how to make economic and societal decisions about risk Demonstrates key concepts through the use of examples and relevant case studies