Identification Techniques in Gas Chromatography

Identification Techniques in Gas Chromatography PDF Author: D. A. Leathard
Publisher: John Wiley & Sons
ISBN:
Category : Science
Languages : en
Pages : 300

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Book Description

Identification Techniques in Gas Chromatography

Identification Techniques in Gas Chromatography PDF Author: D. A. Leathard
Publisher: John Wiley & Sons
ISBN:
Category : Science
Languages : en
Pages : 300

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Book Description


Practical Gas Chromatography

Practical Gas Chromatography PDF Author: Katja Dettmer-Wilde
Publisher: Springer
ISBN: 3642546404
Category : Science
Languages : en
Pages : 904

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Book Description
Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.

Instrumental Methods for Analysis of Soils and Plant Tissue

Instrumental Methods for Analysis of Soils and Plant Tissue PDF Author: Leo Marcellus Walsh
Publisher: Wiley-Blackwell
ISBN:
Category : Technology & Engineering
Languages : en
Pages : 246

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Book Description
Use of Automated Combustion Techniques for Total Carbon Total Nitrogen and Total Sulfur Analysis of Soils1 -- Fluorometry and Nephelometry: Techniques and Uses in Soil Plant and Water Analysis -- Gas Chromatography: Techniques and Uses in Soil Plant and Water Analysis1 -- Atomic Absorption and Flame Photometry: Techniques and Uses in Soil Plant and Water Analysis -- Neutron Activation: Techniques and Possible Uses in Soil and Plant Analysis -- Electron Microprobe: Techniques and Uses in Soil and Plant Analysis1 -- Specific Ion Electrodes: Techniques and Uses in Soil Plant and Water Analysis -- X-Ray Emission Spectrograph: Techniques and Uses for Plant and Soil Studies1 -- Simultaneous Determinations of Phosphorus Potassium Calcium and Magnesium in Wet Digestion Solutions of Plant Tissue by AutoAnalyzer1 -- Determination of Phosphorus Potassium Calcium and Magnesium Simultaneously in North Carolina Ammonium Acetate and Bray P1 Soil Extracts by AutoAnalyzer1 -- Front Matter.

Identification Techniques in Gas Chromatography, [by] D.A. Leathard [and] B.C. Shurlock

Identification Techniques in Gas Chromatography, [by] D.A. Leathard [and] B.C. Shurlock PDF Author: D. A. Leathard
Publisher:
ISBN:
Category : Chemistry, Analytic
Languages : en
Pages : 282

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Book Description


Basic Gas Chromatography

Basic Gas Chromatography PDF Author: Harold M. McNair
Publisher: John Wiley & Sons
ISBN: 1119450756
Category : Science
Languages : en
Pages : 293

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Book Description
Basic Gas Chromatography, Third Edition provides a brief introduction to GC following the objectives for titles in this series. It should appeal to readers with varying levels of education and emphasizes a practical, applied approach to the subject. : This book provides a quick need-to-know introduction to gas chromatography; still the most widely used instrumental analysis technique, and is intended to assist new users in gaining understanding quickly and as a quick reference for experienced users. The new edition provides updated chapters that reflect changes in technology and methodology, especially sample preparation, detectors and multidimensional chromatography. The book also covers new detectors recently introduced and sample preparation methods that have become much more easily accessible since the previous edition.

A Practical Guide to Gas Analysis by Gas Chromatography

A Practical Guide to Gas Analysis by Gas Chromatography PDF Author: John Swinley
Publisher: Elsevier
ISBN: 0128188898
Category : Science
Languages : en
Pages : 442

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Book Description
A Practical Gas Analysis by Gas Chromatography provides a detailed overview of the most important aspects of gas analysis by gas chromatography (GC) for both the novice and expert. Authors John Swinley and Piet de Coning provide the necessary information on the selection of columns and components, thus allowing the reader to assemble custom gas analysis systems for specific needs. The book brings together a wide range of disparate literature on this technique that will fill a crucial gap for those who perform different types of research, including lab operators, separation scientists, graduate students and academic researchers. This highly practical, up-to-date reference can be consulted in the lab to guide key decisions about proper setup, hardware and software selection, calibration, analysis, and more, allowing researchers to avoid the common pitfalls caused by incorrect infrastructure. - Shows, in detail, how valve configurations work, allowing readers to understand the building blocks of extremely complex systems - Presents the complete infrastructure for setting up a gas analysis laboratory in a single source - Includes a full chapter on practical analytical systems for analyzing various gas mixtures

Gas Chromatography and Mass Spectrometry: A Practical Guide

Gas Chromatography and Mass Spectrometry: A Practical Guide PDF Author: O. David Sparkman
Publisher: Academic Press
ISBN: 0080920152
Category : Science
Languages : en
Pages : 633

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Book Description
The second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensible resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information on chromatographic peak deconvolution has been added along with a more in-depth understanding of the use of mass spectral databases in the identification of unknowns. Since the last edition, a number of advances in GC inlet systems and sample introduction techniques have occurred, and they are included in the new edition. Other updates include a discussion on fast GC and options for combining GC detectors with mass spectrometry. The section regarding GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types has the same number of compound types as the original edition, but the information in each section has been expanded to not only explain some of the spectra but to also explain why certain fragmentations take place. The number of Appendices has been increased from 12 to 17. The Appendix on Atomic Masses and Isotope Abundances has been expanded to provide tools to aid in determination of elemental composition from isotope peak intensity ratios. An appendix with examples on "Steps to follow in the determination of elemental compositions based on isotope peak intensities" has been added. Appendices on whether to use GC/MS or LC/MS, third-party software for use in data analysis, list of information required in reporting GC/MS data, X+1 and X+2 peak relative intensities based on the number of atoms of carbon in an ion, and list of available EI mass spectral databases have been added. Others such as the ones on derivatization, isotope peak patterns for ions with Cl and/or Br, terms used in GC and in mass spectrometry, and tips on setting up, maintaining and troubleshooting a GC/MS system have all been expanded and updated. - Covers the practical instruction necessary for successful operation of GC/MS equipment - Reviews the latest advances in instrumentation, ionization methods, and quantitation - Includes troubleshooting techniques and a variety of additional information useful for the GC/MS practitioner - A true benchtop reference - A guide to a basic understanding of the components of a Gas Chromatograph-Mass Spectrometer (GC-MS) - Quick References to data interpretation - Ready source for information on new analyses

Gas Chromatography

Gas Chromatography PDF Author: Peter Kusch
Publisher: BoD – Books on Demand
ISBN: 1838818650
Category : Science
Languages : en
Pages : 144

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Book Description
Gas chromatography (GC) is one of the most important types of chromatography used in analytical chemistry for separating and analyzing chemical organic compounds. Today, gas chromatography is one of the most widespread investigation methods of instrumental analysis. This technique is used in the laboratories of chemical, petrochemical, and pharmaceutical industries, in research institutes, and also in clinical, environmental, and food and beverage analysis. This book is the outcome of contributions by experts in the field of gas chromatography and includes a short history of gas chromatography, an overview of derivatization methods and sample preparation techniques, a comprehensive study on pyrazole mass spectrometric fragmentation, and a GC/MS/MS method for the determination and quantification of pesticide residues in grape samples.

Basic Gas Chromatography-Mass Spectrometry

Basic Gas Chromatography-Mass Spectrometry PDF Author: F.W. Karasek
Publisher: Elsevier
ISBN: 0080929060
Category : Science
Languages : en
Pages : 210

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Book Description
The book begins by covering the basic principles of both gas chromatography (GC) and mass spectrometry (MS) to the extent necessary to understand and deal with the data generated in a GC-MS analysis. The focus then turns to the particular requirements created by a direct combination of these two techniques into a single instrumentation system. The data generated and their use are covered in detail. The role of the computer and its specific software receives special attention, especially in the matter of compound identification via mass spectral search techniques. GC-MS-computer instrumentation has reached such a plateau of excellence today that the present commercial systems will not be obsolete for a long time to come. Therefore, a detailed description of these systems is not only informative but is also pertinent to the subject matter of this book. Finally, representative applications and results obtained with GC-MS-computer techniques are presented and chosen in such a way as to permit extrapolation of specific applications to similar problems encountered by the reader. To aid the reader in mastering the subject matter and increase understanding, interpretation problems and suggested readings are included. The format is instructional, informative and application-oriented with material presented in such a way as to be useful to a broad spectrum of people.The book serves as a text in its own right.The software package Gas Chromatography-Mass Spectrometry: A Knowledge Base, by F.A. Settle, Jr. and M.A. Pleva provides rapid access to a wealth of current information in the GC-MS field. Its three diskettes (51/4 inch) allow the user three ways to access: the index mode, the tree mode and a keyword search mode. The package may be purchased separately and is available for the IBM-PC and compatibles.The software provides a valuable supplement to the book.

Advanced Techniques in Gas Chromatography-Mass Spectrometry (GC-MS-MS and GC-TOF-MS) for Environmental Chemistry

Advanced Techniques in Gas Chromatography-Mass Spectrometry (GC-MS-MS and GC-TOF-MS) for Environmental Chemistry PDF Author:
Publisher: Newnes
ISBN: 0444626247
Category : Science
Languages : en
Pages : 525

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Book Description
Gas chromatography mass spectrometry (GC-MS) has been the technique of choice of analytical scientists for many years. The latest developments in instrumentation, including tandem mass spectrometry (MS-MS) and time-of-flight (TOF) detectors, have opened up and broadened the scope of environmental analytical chemistry. This book summarizes the major advances and relevant applications of GC-MS techniques over the last 10 years, with chapters by leading authors in the field of environmental chemistry. The authors are drawn from academia, industry and government. The book is organized in three main parts. Part I covers applications of basic GC-MS to solve environmental-related problems. Part II focuses on GC-MS-MS instrumentation for the analyses of a broad range of analysis in environmental samples (pesticides, persistent organic pollutants, endocrine disruptors, etc.). Part III covers the use of more advanced GC-MS techniques using low- and high-resolution mass spectrometry for many applications related to the environment, food and industry. - Summarizes the major advances of GC-MS techniques in the last decade - Presents relevant applications of GC-MS techniques - Covers academic, industrial and governmental sectors