Application of Electron Spectroscopy to Surface Chemical Studies PDF Download
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Author: Mohammed H. Matloob
Publisher:
ISBN:
Category :
Languages : en
Pages : 130
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Book Description
The potential of photoelectron spectroscopy in studying the molecular events at solid surfaces was investigated in the present thesis. In addition to the general introduction the first chapter outlined the basic concepts of photoelectron spectroscopy and its application to surface chemistry. The major parts of the various experiments techniques used were described in chapter 2 together with the way of handling the data (including the method of estimating the coverage) ...........
Author: Mohammed H. Matloob
Publisher:
ISBN:
Category :
Languages : en
Pages : 130
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Book Description
The potential of photoelectron spectroscopy in studying the molecular events at solid surfaces was investigated in the present thesis. In addition to the general introduction the first chapter outlined the basic concepts of photoelectron spectroscopy and its application to surface chemistry. The major parts of the various experiments techniques used were described in chapter 2 together with the way of handling the data (including the method of estimating the coverage) ...........
Author: Hassan Windawi
Publisher: John Wiley & Sons
ISBN:
Category : Electron spectroscopy
Languages : en
Pages : 238
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Book Description
Good,No Highlights,No Markup,all pages are intact, Slight Shelfwear,may have the corners slightly dented, may have slight color changes/slightly damaged spine.
Author: H. Ibach
Publisher: Springer Science & Business Media
ISBN: 3642810993
Category : Science
Languages : en
Pages : 265
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Book Description
The development of surface physics and surface chemistry as a science is closely related to the technical development of a number of methods involving electrons either as an excitation source or as an emitted particle carrying characteristic information. Many of these various kinds of electron spectroscopies have become commercially available and have made their way into industrial laboratories. Others are still in an early stage, but may become of increasing importance in the future. In this book an assessment of the various merits and possible drawbacks of the most frequently used electron spectroscopies is attempted. Emphasis is put on prac tical examples and experimental design rather than on theoretical considerations. The book addresses itself to the reader who wishes to know which electron spectroscopy or which combination of different electron spectroscopies he may choose for the particular problems under investigation. After a brief introduction the practical design of electron spectrometers and their figures of merit important for the different applications are discussed in Chapter 2. Chapter 3 deals with electron excited electron spectroscopies which are used for the elemental analysis of surfaces. Structure analysis by electron diffrac tion is described in Chapter 4 with special emphasis on the use of electron diffrac tion for the investigation of surface imperfections. For the application of electron diffraction to surface crystallography in general, the reader is referred to Volume 4 of "Topics in Applied Physics".
Author: Spyridon Zafeiratos
Publisher: World Scientific
ISBN: 180061330X
Category : Science
Languages : en
Pages : 548
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Book Description
X-ray photoelectron spectroscopy (XPS) has become a standard practice technique, and automated XPS facilities can be found in industry and in universities all over the world. This transformed XPS from an advanced characterization method for dedicated research, to a rather standard analysis technique of surface analysis. The catalyst's surface state is probably the most prominent factor that influences the catalytic performance. It is therefore no surprise that XPS has become an indispensable tool in studies of solid catalysts. It has been directly used to investigate issues such as the surface composition of the active catalyst and reaction and deactivation mechanisms.The objective of this book is to provide a comprehensive overview of the current status and future perspectives of X-ray photoelectron spectroscopy dedicated to catalytic applications, including thermal catalysis, electrocatalysis, and photo(electro)catalysis. The book contains 13 chapters, starting with the necessary introduction of the technique background, including basic phenomena and instrumentation aspects. The second part of the book focuses on the presentation of long-established applications of the technique, such as XPS studies of model catalysts. Finally, the book describes relatively recent developments of this method for cutting-edge surface characterization mainly using synchrotron X-ray radiation.
Author: Siegfried Hofmann
Publisher: Springer Science & Business Media
ISBN: 3642273815
Category : Science
Languages : en
Pages : 545
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Book Description
To anyone who is interested in surface chemical analysis of materials on the nanometer scale, this book is prepared to give appropriate information. Based on typical application examples in materials science, a concise approach to all aspects of quantitative analysis of surfaces and thin films with AES and XPS is provided. Starting from basic principles which are step by step developed into practically useful equations, extensive guidance is given to graduate students as well as to experienced researchers. Key chapters are those on quantitative surface analysis and on quantitative depth profiling, including recent developments in topics such as surface excitation parameter and backscattering correction factor. Basic relations are derived for emission and excitation angle dependencies in the analysis of bulk material and of fractional nano-layer structures, and for both smooth and rough surfaces. It is shown how to optimize the analytical strategy, signal-to-noise ratio, certainty and detection limit. Worked examples for quantification of alloys and of layer structures in practical cases (e.g. contamination, evaporation, segregation and oxidation) are used to critically review different approaches to quantification with respect to average matrix correction factors and matrix relative sensitivity factors. State-of-the-art issues in quantitative, destructive and non-destructive depth profiling are discussed with emphasis on sputter depth profiling and on angle resolved XPS and AES. Taking into account preferential sputtering and electron backscattering corrections, an introduction to the mixing-roughness-information depth (MRI) model and its extensions is presented.
Author: D.J. O'Connor
Publisher: Springer Science & Business Media
ISBN: 3662027674
Category : Science
Languages : en
Pages : 457
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Book Description
The idea for this book stemmed from a remark by Philip Jennings of Murdoch University in a discussion session following a regular meeting of the Australian Surface Science group. He observed that a text on surface analysis and applica tions to materials suitable for final year undergraduate and postgraduate science students was not currently available. Furthermore, the members of the Australian Surface Science group had the research experience and range of coverage of sur face analytical techniques and applications to provide a text for this purpose. A of techniques and applications to be included was agreed at that meeting. The list intended readership of the book has been broadened since the early discussions, particularly to encompass industrial users, but there has been no significant alter ation in content. The editors, in consultation with the contributors, have agreed that the book should be prepared for four major groups of readers: - senior undergraduate students in chemistry, physics, metallurgy, materials science and materials engineering; - postgraduate students undertaking research that involves the use of analytical techniques; - groups of scientists and engineers attending training courses and workshops on the application of surface analytical techniques in materials science; - industrial scientists and engineers in research and development seeking a description of available surface analytical techniques and guidance on the most appropriate techniques for particular applications. The contributors mostly come from Australia, with the notable exception of Ray Browning from Stanford University.
Author: V.I. Nefedov
Publisher: CRC Press
ISBN: 1466564733
Category : Science
Languages : en
Pages : 200
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Book Description
This volume outlines the physical and methodical concepts of X-ray photoelectron spectroscopy (XPS) specifically for surface studies using both inner and valence electron levels. It discusses the theory and practice of XPS qualitative and quantitative analysis of solid state surfaces and provides lists of extended experimental and theoretical data necessary for the determination of concentration and thin film thicknesses. In addition it covers the many problems concerning in-depth profiling, ion sputtering rate and damages of the structure of altered layers, as well as applications of angular dependence of the intensities and photoelectron diffraction for surface studies. Also provided are the applications of XPS for the investigations of catalysts, adsorption, electronic surface states, oxydation of semi-conductors and alloys, minerals, including lunar regolith and natural gold, glasses, radiation damage, surface diffusion, polymers, etc.
Author: L. Fiermans
Publisher: Springer Science & Business Media
ISBN: 1468428179
Category : Science
Languages : en
Pages : 485
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Book Description
Surface physics and chemistry have in recent years become one of the most active fields in solid state research. A number of techniques have been developed, and both the experimental aspect and the correlated theory are evolving at an extremely fast rate. Electron and ion spectroscopy are of major importance in this development. In this volume, which contains edited and extended versions of eight sets of lectures given at the NATO Advanced Study Institute held at Ghent, Belgium, from August 29 to September 9, 1977, a re view of the state of the art in these fields is given from both an experimental and a theoretical point of view. Electron emission techniques such as UPS (ultraviolet photoemission spectroscopy), XPS (x-ray photoemission spectroscopy), and AES (Auger electron spectroscopy) constitute the major part of this volume, reflecting the fact that they continue to be the most widely applied surface techniques. Recent developments in the application of synchrotron radiation to angle-resolved photoelectron spectroscopy are extensively covered, from an experimental point of view by Prof. W. E. Spicer (Stanford University, U.S.A.) and from a theoretical point of view by Dr. A. Liebsch (Kernforschungsanlage Julich, Germany). Emphasis is put on the study of energy bands in layered structures, and on chemisorption on well-defined surfaces. Chemisorption and catalysis on metals is treated in detail by Prof. G. Ertl (Universitat Munchen, Germany). This chapter contains a review of the application of the different surface techniques to specific surface systems.
Author: C. R. Brundle
Publisher: Mittal Publications
ISBN: 9788170998259
Category : Electron spectroscopy
Languages : en
Pages : 274
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Book Description
Author: Thomas Carlson
Publisher: Springer Science & Business Media
ISBN: 1475701187
Category : Science
Languages : en
Pages : 427
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Book Description
In 1970 when I first seriously contemplated writing a book on electron spectroscopy, I recognized the impossibility of completely reaching my desired goals. First, the field was expanding (and still is) at such a rate that a definitive statement of the subject is not possible. The act of following the literature comprehensively and summarizing its essential content proved to be a diver gent series. On the other hand, the field has increased to such a size that violent changes in its basic makeup no longer occur with the frequency that was present in its early days. Furthermore, the excitement of electron spectro scopy lies in its many-faceted interrelationships. In the era of specialization, electron spectroscopy is an open-ended subject continually bringing together new aspects of science. I wished to discuss not just one type of electron spectro scopy, but as many as would be possible. The book as it stands concentrates its attention on x-ray photoelectron spectroscopy, but also presents the basis of Auger electron spectroscopy and uv photoelectron spectroscopy, as well as mentioning many of the other branches of the field. A large, many-author volume might be an answer to some of these problems. However, though anyone person possesses only a limited amount of expertise, I have always enjoyed books by a single author since what they lack in detailed knowledge they gain in a unified viewpoint. I hope the final product, though limited in its attainment of these goals, will still be of some merit.
