A New High-temperature Calorimeter PDF Download
Are you looking for read ebook online? Search for your book and save it on your Kindle device, PC, phones or tablets. Download A New High-temperature Calorimeter PDF full book. Access full book title A New High-temperature Calorimeter by Raleigh L. McKisson. Download full books in PDF and EPUB format.
Author: Raleigh L. McKisson
Publisher:
ISBN:
Category :
Languages : en
Pages : 30
Get Book Here
Book Description
Author: Raleigh L. McKisson
Publisher:
ISBN:
Category :
Languages : en
Pages : 30
Get Book Here
Book Description
Author: Mike Reading
Publisher: Springer Science & Business Media
ISBN: 9781402037498
Category : Medical
Languages : en
Pages : 352
Get Book Here
Book Description
MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.
Author: Christoph Schick
Publisher: Springer
ISBN: 3319313290
Category : Technology & Engineering
Languages : en
Pages : 796
Get Book Here
Book Description
In the past decades, the scan rate range of calorimeters has been extended tremendously at the high end, from approximately 10 up to 10 000 000 °C/s and more. The combination of various calorimeters and the newly-developed Fast Scanning Calorimeters (FSC) now span 11 orders of magnitude, by which many processes can be mimicked according to the time scale(s) of chemical and physical transitions occurring during cooling, heating and isothermal stays in case heat is exchanged. This not only opens new areas of research on polymers, metals, pharmaceuticals and all kinds of substances with respect to glass transition, crystallization and melting phenomena, it also enables in-depth study of metastability and reorganization of samples on an 1 to 1000 ng scale. In addition, FSC will become a crucial tool for understanding and optimization of processing methods at high speeds like injection molding. The book resembles the state-of-the art in Thermal Analysis & Calorimetry and is an excellent starting point for both experts and newcomers in the field.
Author: G.W.H. Höhne
Publisher: Springer Science & Business Media
ISBN: 366203302X
Category : Science
Languages : en
Pages : 233
Get Book Here
Book Description
Differential Scanning Calorimetry (DSC) is a well established measuring method which is used on a large scale in different areas of research, development, and quality inspection and testing. Over a large temperature range, thermal effects can be quickly identified and the relevant temperature and the characteristic caloric values determined using substance quantities in the mg range. Measurement values obtained by DSC allow heat capacity, heat of transition, kinetic data, purity and glass transition to be determined. DSC curves serve to identify substances, to set up phase diagrams and to determine degrees of crystallinity. This book provides, for the first time, an overall description of the most impor tant applications of Differential Scanning Calorimetry. Prerequisites for reliable measurement results, optimum evaluation of the measurement curves and esti mation of the uncertainties of measurement are, however, the knowledge of the theoretical bases of DSC, a precise calibration of the calorimeter and the correct analysis of the measurement curve. The largest part of this book deals with these basic aspects: The theory of DSC is discussed for both heat flux and power compensated instruments; temperature calibration and caloric calibration are described on the basis of thermodynamic principles. Desmearing of the measurement curve in different ways is presented as a method for evaluating the curves of fast transitions.
Author: Stefan Mathias Sarge
Publisher: John Wiley & Sons
ISBN: 3527649387
Category : Science
Languages : en
Pages : 346
Get Book Here
Book Description
Clearly divided into three parts, this practical book begins by dealing with all fundamental aspects of calorimetry. The second part looks at the equipment used and new developments. The third and final section provides measurement guidelines in order to obtain the best results. The result is optimized knowledge for users of this technique, supplemented with practical tips and tricks.
Author: W. Zielenkiewicz
Publisher: Springer Science & Business Media
ISBN: 1402007973
Category : Science
Languages : en
Pages : 198
Get Book Here
Book Description
Calorimetry is one of the oldest areas of physical chemistry. The date on which calorimetry came into being may be taken as 13 June 1783, the day on which Lavoisier and Laplace presented a contribution entitled ,,Memoire de la Chaleur“ at a session of the Academie Française. Throughout the existence of calorimetry, many new methods have been developed and the measuring techniques have been improved. At p- sent, numerous laboratories worldwide continue to focus attention on the development and applications of calorimetry, and a number of com- nies specialize in the production of calorimeters. The calorimeter is an instrument that allows heat effects in it to be determined by directly measurement of temperature. Accordingly, to determine a heat effect, it is necessary to establish the relationship - tween the heat effect generated and the quantity measured in the ca- rimeter. It is this relationship that unambiguously determines the mathematical model of the calorimeter. Depending on the type of ca- rimeter applied, the accuracy required, and the conditions of heat and mass transfer that prevail in the device, the relationship between the measured and generated quantities can assume different mathematical forms.
Author: Peter J. Haines
Publisher: Royal Society of Chemistry
ISBN: 9780854046102
Category : Education
Languages : en
Pages : 244
Get Book Here
Book Description
The use of thermal and calorimetric methods has shown rapid growth over the last two decades, in an increasingly wide range of applications. In addition, a number of powerful new techniques have been developed. This book supplies a concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Brief accounts of the basic theory are reinforced with detailed applications of the methods and contemporary developments. Also included is information on standard test methods and manufacturers. Written by acknowledged experts, Principles of Thermal Analysis and Calorimetry is up-to-date, wide-ranging and practical. It will be an important source of information for many levels of readership in a variety of areas, from students and lecturers through to industrial and laboratory staff and consultants.
Author:
Publisher:
ISBN:
Category : Weights and measures
Languages : en
Pages : 1164
Get Book Here
Book Description
Author: Ele Eugene Stansbury
Publisher:
ISBN:
Category : Calorimeters
Languages : en
Pages : 72
Get Book Here
Book Description
Author: James M. Jacobs
Publisher:
ISBN:
Category : Fluid dynamics
Languages : en
Pages : 444
Get Book Here
Book Description
A total of 2519 annotated references to the unclassified report literature is presented. Subjects covered under heat transfer and fluid flow include radioinduced heating; boiling; boiler, evaporators, pump, and heat exchanger design; hydrodynamics; coolants and their properties; thermal and flow instrumentation; high temperature materials; thermal properties of materials; and thermal insulation. Subjects covered less completely include thermodynamics; aerodynamics; high temperature corrosion; corrosion specific to heat transfer systems; erosion; mass transfer; corrosion film formation and effects; coolant processing and radioactivity; radiation effects of heat transfer materials; and pertinent data of thermonuclear processes. Subject, report number availability, and author indexes are given.
