Experimental Methods for Evaluation of Hydrotreating Catalysts

Experimental Methods for Evaluation of Hydrotreating Catalysts PDF Author: Jorge Ancheyta
Publisher: John Wiley & Sons
ISBN: 1119517990
Category : Technology & Engineering
Languages : en
Pages : 429

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Book Description
Presents detailed information and study cases on experiments on hydrotreating catalysts for the petroleum industry Catalytic hydrotreating (HDT) is a process used in the petroleum refining industry for upgrading hydrocarbon streams—removing impurities, eliminating metals, converting asphaltene molecules, and hydrocracking heavy fractions. The major applications of HDT in refinery operations include feed pretreatment for conversion processes, post-hydrotreating distillates, and upgrading heavy crude oils. Designing HDT processes and catalysts for successful commercial application requires experimental studies based on appropriate methodologies. Experimental Methods for Evaluation of Hydrotreating Catalysts provides detailed descriptions of experiments in different reaction scales for studying the hydrotreating of various petroleum distillates. Emphasizing step-by-step methodologies in each level of experimentation, this comprehensive volume presents numerous examples of evaluation methods, operating conditions, reactor and catalyst types, and process configurations. In-depth chapters describe experimental setup and procedure, analytical methods, calculations, testing and characterization of catalyst and liquid products, and interpretation of experiment data and results. The text describes experimental procedure at different levels of experimentation—glass reactor, batch reactor, continuous stirred tank reactor, and multiple scales of tubular reactors—using model compounds, middle distillates and heavy oil. This authoritative volume: Introduces experimental setups used for conducting research studies, such as type of operation, selection of reactor, and analysis of products Features examples focused on the evaluation of different reaction parameters and catalysts with a variety of petroleum feedstocks Provides experimental data collected from different reaction scales Includes experiments for determining mass transfer limitations and deviation from ideality of flow pattern Presents contributions from leading scientists and researchers in the field of petroleum refining Experimental Methods for Evaluation of Hydrotreating Catalysts is an indispensable reference for researchers and professionals working in the area of catalytic hydrotreating, as well as an ideal textbook for courses in fields such as chemical engineering, petrochemical engineering, and biotechnology.

Experimental Methods for Evaluation of Hydrotreating Catalysts

Experimental Methods for Evaluation of Hydrotreating Catalysts PDF Author: Jorge Ancheyta
Publisher: John Wiley & Sons
ISBN: 1119517990
Category : Technology & Engineering
Languages : en
Pages : 429

Get Book Here

Book Description
Presents detailed information and study cases on experiments on hydrotreating catalysts for the petroleum industry Catalytic hydrotreating (HDT) is a process used in the petroleum refining industry for upgrading hydrocarbon streams—removing impurities, eliminating metals, converting asphaltene molecules, and hydrocracking heavy fractions. The major applications of HDT in refinery operations include feed pretreatment for conversion processes, post-hydrotreating distillates, and upgrading heavy crude oils. Designing HDT processes and catalysts for successful commercial application requires experimental studies based on appropriate methodologies. Experimental Methods for Evaluation of Hydrotreating Catalysts provides detailed descriptions of experiments in different reaction scales for studying the hydrotreating of various petroleum distillates. Emphasizing step-by-step methodologies in each level of experimentation, this comprehensive volume presents numerous examples of evaluation methods, operating conditions, reactor and catalyst types, and process configurations. In-depth chapters describe experimental setup and procedure, analytical methods, calculations, testing and characterization of catalyst and liquid products, and interpretation of experiment data and results. The text describes experimental procedure at different levels of experimentation—glass reactor, batch reactor, continuous stirred tank reactor, and multiple scales of tubular reactors—using model compounds, middle distillates and heavy oil. This authoritative volume: Introduces experimental setups used for conducting research studies, such as type of operation, selection of reactor, and analysis of products Features examples focused on the evaluation of different reaction parameters and catalysts with a variety of petroleum feedstocks Provides experimental data collected from different reaction scales Includes experiments for determining mass transfer limitations and deviation from ideality of flow pattern Presents contributions from leading scientists and researchers in the field of petroleum refining Experimental Methods for Evaluation of Hydrotreating Catalysts is an indispensable reference for researchers and professionals working in the area of catalytic hydrotreating, as well as an ideal textbook for courses in fields such as chemical engineering, petrochemical engineering, and biotechnology.

Catalytic In-Situ Upgrading of Heavy and Extra-Heavy Crude Oils

Catalytic In-Situ Upgrading of Heavy and Extra-Heavy Crude Oils PDF Author: Mikhail A. Varfolomeev
Publisher: John Wiley & Sons
ISBN: 1119871492
Category : Technology & Engineering
Languages : en
Pages : 564

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Book Description
Catalytic In-Situ Upgrading of Heavy and Extra-Heavy Crude Oils A comprehensive guide to a cutting-edge and cost-effective refinement process for heavy oil Oil sufficiently viscous that it cannot flow normally from production wells is called heavy oil and constitutes as much as 70% of global oil reserves. Extracting and refining this oil can pose significant challenges, including very high transportation costs. As a result, processes which produce and partially refine heavy oil in situ, known as catalytic upgrading, are an increasingly important part of the heavy oil extraction process, and the reduced carbon footprint associated with these methods promises to make them even more significant in the coming years. Catalytic In-Situ Upgrading of Heavy and Extra-Heavy Crude Oils provides a comprehensive introduction to these processes. It introduces the properties and characteristics of heavy and extra-heavy oil before discussing different catalysts and catalyzing processes, their mechanisms and underlying physics, and more. It offers the full sweep of description and analysis required for petroleum and chemical engineers to understand this vital aspect of the modern oil industry. Readers will also find: Detailed discussion of subjects including electron paramagnetic resonance spectroscopy, nuclear magnetic resonance spectroscopy, and more Analysis of both liquid catalysts and nanoparticle catalysts A numerical simulation of the catalytic in-situ oil upgrading process Catalytic In-Situ Upgrading of Heavy and Extra-Heavy Crude Oils is a valuable reference for petroleum and chemical engineers as well as advanced undergraduate and graduate students in related fields.

Hydrogen Applications and Technologies

Hydrogen Applications and Technologies PDF Author: Mohammad Reza Rahimpour
Publisher: CRC Press
ISBN: 1040122981
Category : Technology & Engineering
Languages : en
Pages : 411

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Book Description
Hydrogen has wide applications across many industries, including petroleum refineries, hydrotreating processes, and metallurgy applications. In addition, a number of valuable chemicals, such as ammonia, alcohols, and acids, are manufactured directly or indirectly with hydrogen. Hydrogen Applications and Technologies covers the utilization of hydrogen in petrochemical products, vehicles, and power generation systems, as well as in refinery hydrotreating, metallurgy, welding, annealing, and the heat‐treating of metals. Describes the application of hydrogen in producing valuable chemicals in detail Comprehensively discusses hydrogen utilization as an energy source Covers the application of hydrogen in power generation systems and across various industries Reviews hydrogen’s role as an agent in chemical reactions Part of the multivolume Handbook of Hydrogen Production and Applications, this stand-alone book guides researchers and academics in chemical, environmental, energy, and related areas of engineering interested in development and implementation of hydrogen production technologies.

Deactivation of Heavy Oil Hydroprocessing Catalysts

Deactivation of Heavy Oil Hydroprocessing Catalysts PDF Author: Jorge Ancheyta
Publisher: John Wiley & Sons
ISBN: 1118769813
Category : Technology & Engineering
Languages : en
Pages : 360

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Book Description
Written by a scientist and researcher with more than 25 years of experience in the field, this serves as a complete guide to catalyst activity loss during the hydroprocessing of heavy oils. Explores the physical and chemical properties of heavy oils and hydroprocessing catalysts; the mechanisms of catalyst deactivation; catalyst characterization by a variety of techniques and reaction conditions; laboratory and commercial information for model validations; and more Demonstrates how to develop correlations and models for a variety of reaction scales with step-by-step descriptions and detailed experimental data Contains important implications for increasing operational efficiencies within the petroleum industry An essential reference for professionals and researchers working in the refining industry as well as students taking courses on chemical reaction engineering

Fossil Energy Update

Fossil Energy Update PDF Author:
Publisher:
ISBN:
Category : Fossil fuels
Languages : en
Pages : 806

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Book Description


New Frontiers in Catalysis, Parts A-C

New Frontiers in Catalysis, Parts A-C PDF Author: L. Guczi
Publisher: Elsevier
ISBN: 0080887147
Category : Technology & Engineering
Languages : en
Pages : 2955

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Book Description
These volumes comprise the proceedings of the major international meeting on catalysis which is held at 4 year intervals. The programme focussed on New Frontiers in Catalysis including nontraditional catalytic materials and environmental catalysis. The contributions cover a wide range of fundamental, applied, industrial and engineering aspects of catalysis. The extensive range of highly efficient industrial techniques for observing and characterizing catalytically important surfaces is evident.The programme covered the following sessions: Mechanism, theory, in situ methods; Catalytic reaction on atomically clean surfaces; Catalytic reaction on zeolites and related substances; New methods and principles for catalyst preparation; Hydrotreatment reactions (HDS, HDN); Characterization of catalysts, application of novel techniques; Selective oxidation; New catalytic aspects of heteropoly acids and related compounds; Reaction of hydrocarbons; Nontraditional catalytic materials; Fuel upgrading; Alkane activation; Acid-base catalysis; New selective catalytic reactons, fine chemicals; Environmental catalysis; Industrial catalysis, deactivation, reactivation; Synthesis from syngas; Electrocatalysis; Photocatalysis.The invited lectures and 433 papers included in these volumes present an update on all areas of catalysis and applications.

Heterogeneous Catalysis and its Industrial Applications

Heterogeneous Catalysis and its Industrial Applications PDF Author: Martin Schmal
Publisher: Springer
ISBN: 9783319092492
Category : Science
Languages : en
Pages : 0

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Book Description
This book aims to introduce the basic concepts involved in industrial catalytic processes. It is profusely illustrated with experimental results with the main objective of guiding how to select a suitable catalyst for specific processes. The book is divided in two parts. In the first part the basic concepts are addressed, regarding the existing theories, activity patterns and adsorption-desorption phenomena. In the second part the key experimental methods for the physicochemical characterization of catalysts are presented, as well as the currently used catalyst pre and post treatments. The last chapter describes some important in situ characterization techniques (e.g. XPS and TEM) and surface model patterns related to surface modifications occurring during the reaction. Thoroughly illustrated with microscopy images, spectroscopy data and schematics of reaction mechanisms, the book provides a powerful learning tool for students in undergraduate and graduate level courses on the field of catalysis. Exercises and resolved problems are provided, as well as experimental procedures to support laboratory classes. Furthermore, the content is presented in a carefully chosen sequence, reflecting the 30 year teaching experience of the author. The author, Professor Martin Schmal, sees the present book as a way of conveying basic knowledge needed for the development of more efficient catalysts (i.e. nanostructured materials) and novel industrial chemical processes in the fields of environmental chemistry, fine chemistry, hydrotreating of heavy oils, hydrogen production and biomass processing.

Springer Handbook of Petroleum Technology

Springer Handbook of Petroleum Technology PDF Author: Chang Samuel Hsu
Publisher: Springer
ISBN: 3319493477
Category : Science
Languages : en
Pages : 1243

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Book Description
This handbook provides a comprehensive but concise reference resource for the vast field of petroleum technology. Built on the successful book "Practical Advances in Petroleum Processing" published in 2006, it has been extensively revised and expanded to include upstream technologies. The book is divided into four parts: The first part on petroleum characterization offers an in-depth review of the chemical composition and physical properties of petroleum, which determine the possible uses and the quality of the products. The second part provides a brief overview of petroleum geology and upstream practices. The third part exhaustively discusses established and emerging refining technologies from a practical perspective, while the final part describes the production of various refining products, including fuels and lubricants, as well as petrochemicals, such as olefins and polymers. It also covers process automation and real-time refinery-wide process optimization. Two key chapters provide an integrated view of petroleum technology, including environmental and safety issues.Written by international experts from academia, industry and research institutions, including integrated oil companies, catalyst suppliers, licensors, and consultants, it is an invaluable resource for researchers and graduate students as well as practitioners and professionals.

Modeling and Simulation of Catalytic Reactors for Petroleum Refining

Modeling and Simulation of Catalytic Reactors for Petroleum Refining PDF Author: Jorge Ancheyta
Publisher: John Wiley & Sons
ISBN: 1118002164
Category : Technology & Engineering
Languages : en
Pages : 449

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Book Description
Modeling and Simulation of Catalytic Reactors for Petroleum Refining deals with fundamental descriptions of the main conversion processes employed in the petroleum refining industry: catalytic hydrotreating, catalytic reforming, and fluid catalytic cracking. Common approaches for modeling of catalytic reactors for steady-state and dynamic simulations are also described and analyzed. Aspects such as thermodynamics, reaction kinetics, process variables, process scheme, and reactor design are discussed in detail from both research and commercial points of view. Results of simulation with the developed models are compared with those determined at pilot plant scale as well as commercial practice. Kinetics data used in the reactor model are either taken from the literature or obtained under controlled experiments at the laboratory.

Practical Advances in Petroleum Processing

Practical Advances in Petroleum Processing PDF Author: Chang Samuel Hsu
Publisher: Springer Science & Business Media
ISBN: 0387257896
Category : Science
Languages : en
Pages : 894

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Book Description
Includes topics not found together in books on petroleum processing: economics, automation, process modeling, online optimization, safety, environmental protection Combines overviews of petroleum composition, refinery processes, process automation, and environmental protection with comprehensive chapters on recent advances in hydroprocessing, FCC, lubricants, hydrogen management Gives diverse perspectives, both geographic and topical, because contributors include experts from eight different countries in North America, Europe and Asia, representing oil companies, universities, catalyst vendors, process licensors, consultants and engineering contractors