Towards an Unambiguous Electron Magnetic Chiral Dichroism (EMCD) Measurement in a Transmission Electron Microscope (TEM) PDF Download
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Author: Christian Hurm
Publisher: Logos Verlag Berlin GmbH
ISBN: 3832521089
Category : Science
Languages : en
Pages : 122
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Book Description
The intention of the ChiralTEM project (2004-2007) was the detection of electron (energy loss) magnetic chiral dichroism in a transmission electron microscope (TEM), in analogy to X-ray magnetic circular dichroism (XMCD). For the experiments, single-crystal electron transparent specimen's with magnetic induction perpendicular to the specimen's plane are required. In this thesis, different preparation techniques are evaluated regarding their usability to produce ideal specimen's for a verification of EMCD. After the demonstration of a dichroic measurement, an obvious way to prove the chiral effect is to invert the specimen's magnetization from parallel to antiparallel to the electron beam trajectory, leaving all other parameters of the experimental setup unchanged. For this case, one would - according to theory - expect a change in the dichroic signal measured. In the magnetic field of the objective lens of a 300kV TEM, typical ferromagnetic specimens will be close to saturation perpendicular to the specimen's plane. Reversing the current through the coils of the objective lens will then simply invert the magnetization of the specimen. In consequence, any magnetic chiral effect is expected to change sign. A switching unit for Tecnai microscopes has been constructed for save commutation of the lens currents. The direct sensitivity of the dichroic signal to the direction of the magnetization gives evidence to the magnetic origin of the effect.
Author: Christian Hurm
Publisher: Logos Verlag Berlin GmbH
ISBN: 3832521089
Category : Science
Languages : en
Pages : 122
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Book Description
The intention of the ChiralTEM project (2004-2007) was the detection of electron (energy loss) magnetic chiral dichroism in a transmission electron microscope (TEM), in analogy to X-ray magnetic circular dichroism (XMCD). For the experiments, single-crystal electron transparent specimen's with magnetic induction perpendicular to the specimen's plane are required. In this thesis, different preparation techniques are evaluated regarding their usability to produce ideal specimen's for a verification of EMCD. After the demonstration of a dichroic measurement, an obvious way to prove the chiral effect is to invert the specimen's magnetization from parallel to antiparallel to the electron beam trajectory, leaving all other parameters of the experimental setup unchanged. For this case, one would - according to theory - expect a change in the dichroic signal measured. In the magnetic field of the objective lens of a 300kV TEM, typical ferromagnetic specimens will be close to saturation perpendicular to the specimen's plane. Reversing the current through the coils of the objective lens will then simply invert the magnetization of the specimen. In consequence, any magnetic chiral effect is expected to change sign. A switching unit for Tecnai microscopes has been constructed for save commutation of the lens currents. The direct sensitivity of the dichroic signal to the direction of the magnetization gives evidence to the magnetic origin of the effect.
Author: Peter Schattschneider
Publisher: CRC Press
ISBN: 9814303178
Category : Science
Languages : en
Pages : 274
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Book Description
This book describes energy loss magnetic chiral dichroism (EMCD), a phenomenon in energy loss spectroscopy discovered in 2006. EMCD is the equivalent of XMCD but is based on fast probe electrons in the electron microscope. A spatial resolution of 2 nm has been demonstrated, and the lattice-resolved mapping of atomic spins appears feasible. EMCD is,
Author: Anne M. Coghill
Publisher: American Chemical Society
ISBN: 9780841239494
Category : Authorship
Languages : en
Pages : 0
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Book Description
In the time since the second edition of The ACS Style Guide was published, the rapid growth of electronic communication has dramatically changed the scientific, technical, and medical (STM) publication world. This dynamic mode of dissemination is enabling scientists, engineers, and medicalpractitioners all over the world to obtain and transmit information quickly and easily. An essential constant in this changing environment is the requirement that information remain accurate, clear, unambiguous, and ethically sound.This extensive revision of The ACS Style Guide thoroughly examines electronic tools now available to assist STM writers in preparing manuscripts and communicating with publishers. Valuable updates include discussions of markup languages, citation of electronic sources, online submission ofmanuscripts, and preparation of figures, tables, and structures. In keeping current with the changing environment, this edition also contains references to many resources on the internet.With this wealth of new information, The ACS Style Guide's Third Edition continues its long tradition of providing invaluable insight on ethics in scientific communication, the editorial process, copyright, conventions in chemistry, grammar, punctuation, spelling, and writing style for any STMauthor, reviewer, or editor. The Third Edition is the definitive source for all information needed to write, review, submit, and edit scholarly and scientific manuscripts.
Author: Surender Kumar Sharma
Publisher: Springer
ISBN: 3319929550
Category : Technology & Engineering
Languages : en
Pages : 612
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Book Description
This book focuses on the widely used experimental techniques available for the structural, morphological, and spectroscopic characterization of materials. Recent developments in a wide range of experimental techniques and their application to the quantification of materials properties are an essential side of this book. Moreover, it provides concise but thorough coverage of the practical and theoretical aspects of the analytical techniques used to characterize a wide variety of functional nanomaterials. The book provides an overview of widely used characterization techniques for a broad audience: from beginners and graduate students, to advanced specialists in both academia and industry.
Author: Alistair M. Stephen
Publisher: CRC Press
ISBN: 1420015168
Category : Technology & Engineering
Languages : en
Pages : 750
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Book Description
Comprehensive in scope, Food Polysaccharides and Their Applications, Second Edition explains the production aspects and the chemical and physical properties of the main classes of polysaccharaides consumed as food, highlighting their nutritional value and their technological characteristics. Chapters in this new edition detail the source,
Author: Baldassare Di Bartolo
Publisher: Springer Science & Business Media
ISBN: 1402047894
Category : Science
Languages : en
Pages : 574
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Book Description
This volume presents the Proceedings of "New Development in Optics and Related Fields," held in Italy in June, 2005. This meeting was organized by the International School of Atomic and Molecular Spectroscopy of the "Ettore Majorana" Center for Scientific Culture. The purpose of this Institute was to provide a comprehensive and coherent treatment of the new techniques and contemporary developments in optics and related fields.
Author: Shayne Cox Gad
Publisher: John Wiley & Sons
ISBN: 0470259809
Category : Science
Languages : en
Pages : 1386
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Book Description
This handbook features contributions from a team of expert authors representing the many disciplines within science, engineering, and technology that are involved in pharmaceutical manufacturing. They provide the information and tools you need to design, implement, operate, and troubleshoot a pharmaceutical manufacturing system. The editor, with more than thirty years' experience working with pharmaceutical and biotechnology companies, carefully reviewed all the chapters to ensure that each one is thorough, accurate, and clear.
Author: Peter W. Hawkes
Publisher: Academic Press
ISBN: 0080984169
Category : Science
Languages : en
Pages : 755
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Book Description
The three volumes in the PRINCIPLES OF ELECTRON OPTICS Series constitute the first comprehensive treatment of electron optics in over forty years. While Volumes 1 and 2 are devoted to geometrical optics, Volume 3 is concerned with wave optics and effects due to wave length. Subjects covered include:Derivation of the laws of electron propagation from SchrUdinger's equationImage formation and the notion of resolutionThe interaction between specimens and electronsImage processingElectron holography and interferenceCoherence, brightness, and the spectral functionTogether, these works comprise a unique and informative treatment of the subject. Volume 3, like its predecessors, will provide readers with both a textbook and an invaluable reference source.
Author: Danzhou Yang
Publisher: Humana
ISBN: 9781493996650
Category : Medical
Languages : en
Pages : 437
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Book Description
This volume covers the structures, properties, and functions of G-quadruplexes in a wide range of biological disciplines, including therapeutic intervention and biomaterial application. The chapters in this book explore a wide range of vital and new experimental techniques used in the study of G-quadruplexes. Written in the highly successful Methods in Molecular Biology series format, chapters include introductions to their respective topics, lists of the necessary materials and reagents, step-by-step, readily reproducible laboratory protocols, and tips on troubleshooting and avoiding known pitfalls. Practical and cutting-edge, G-Quadruplex DNA: Methods and Protocols is a valuable resource for both novice and experienced researchers who work in biophysics, structural biology, computational biology, biochemistry, and molecular and cell biology, and who want to learn more about the potential roles and effects of G-quadruplex in these fields.
Author: Jill Guyonnet
Publisher: Springer Science & Business Media
ISBN: 3319057502
Category : Science
Languages : en
Pages : 167
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Book Description
Using the nano metric resolution of atomic force microscopy techniques, this work explores the rich fundamental physics and novel functionalities of domain walls in ferroelectric materials, the nano scale interfaces separating regions of differently oriented spontaneous polarization. Due to the local symmetry-breaking caused by the change in polarization, domain walls are found to possess an unexpected lateral piezoelectric response, even when this is symmetry-forbidden in the parent material. This has interesting potential applications in electromechanical devices based on ferroelectric domain patterning. Moreover, electrical conduction is shown to arise at domain walls in otherwise insulating lead zirconate titanate, the first such observation outside of multiferroic bismuth ferrite, due to the tendency of the walls to localize defects. The role of defects is then explored in the theoretical framework of disordered elastic interfaces possessing a characteristic roughness scaling and complex dynamic response. It is shown that the heterogeneous disorder landscape in ferroelectric thin films leads to a breakdown of the usual self-affine roughness, possibly related to strong pinning at individual defects. Finally, the roles of varying environmental conditions and defect densities in domain switching are explored and shown to be adequately modelled as a competition between screening effects and pinning.
