Synthesis and Characterization of Several Molybdenum Chloride Cluster Compounds PDF Download
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Author: William Winder Beers
Publisher:
ISBN:
Category :
Languages : en
Pages : 276
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Author: William Winder Beers
Publisher:
ISBN:
Category :
Languages : en
Pages : 276
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Author:
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Category :
Languages : en
Pages :
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Investigation into the direct synthesis of Mo4Cl(P(C2H5)3)4 from Mo2(OAc)4 led to a synthetic procedure that produces yields greater than 80%. The single-crystal structure disclosed a planar rectangular cluster of molybdenum atoms. Metal-metal bond distances suggest that the long edges of the rectangular cluster should be considered to be single bonds and the short metal-metal bonds to be triple bonds. This view is reinforced by an extended Hueckel calculation. Attempts to add a metal atom to Mo4Cl(PR3)4 to form Mo5Cl10(PR3)3 led instead to a compound with the composition Mo8Cl16(PR3)4. Solution and reflectance uv-visible spectra and x-ray photoelectron spectra suggest that tetranuclear molybdenum units are present. The facile reaction between Mo8Cl16(PR3)4 and PR3 imply that the linkage between tetrameric units is weak.
Author: Deborah Ann Spink
Publisher:
ISBN:
Category :
Languages : en
Pages : 152
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Author: Diana Rose Tomchick
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Category :
Languages : en
Pages : 542
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Author: Paul Ernest Lamberty
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Category : Molybdenum-iron-sulphur complex
Languages : en
Pages : 176
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Category : Power resources
Languages : en
Pages : 518
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![The Synthesis and Characterization of the Molybdenum-iron-sulfur Clusters [S2MoS2FeL2]2, [S2MoS2FeS2FeL2]3, and [S2MoS2FeS2FeS2MoS2]4 PDF](https://books.google.com/books/content/images/frontcover/-x3bDqAubX8C?fife=w80-h100)
Author: Robert Hugo Tieckelmann
Publisher:
ISBN:
Category : Complex compounds
Languages : en
Pages : 222
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Author: Zoltan Nagy
Publisher: Springer Science & Business Media
ISBN: 1489905456
Category : Science
Languages : en
Pages : 485
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Electrochemical synthesis of inorganic compounds is a relatively unknown field. The successful, large industrial processes, such as chlorine-caustic production, are well known, but the large number of other compounds that have been synthesized electrochemically are much less appreciated, even by electrochemists and inorganic chemists. The last comprehensive book on this subject was published in the 1930's and no modern review or summary of the whole field is in existence. But the field is in no way dormant, as attested by the large number of publications, undiminished throughout the years, describing new syntheses and improvements of old ones. Indeed, it can be expected that practical applications of electrochemical inor ganic syntheses will increase in the future as an increasing portion of our energy will be available in electrical form. Electrochemical processes have important advantages over chemical routes: often the selectivity of the reaction can be better controlled through the use of potential control at the electrode, and the creation of environmen tally harmful waste material can be avoided more easily since one is using the purest reagent - the electron. In addition to development of new synthetic routes, many old ones, which were found to be un economical in the past, are worth reexamining in light of the recent considerable advances in cell design principles, materials of construc tion, and electrode and separator materials, together with our im proved understanding of electrode reactions and electrocatalysis. It is in the hope of accelerating this process that this bibliography is published.
Author: Rabindranath Bissessur
Publisher:
ISBN:
Category : Molybdenum compounds
Languages : en
Pages : 566
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Author:
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ISBN:
Category :
Languages : en
Pages : 118
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