Solid State NMR of Polymers

Solid State NMR of Polymers PDF Author: T. Asakura
Publisher: Elsevier
ISBN: 0080541461
Category : Science
Languages : en
Pages : 1017

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Book Description
In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods.This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described.Features of this book:• Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field• Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists.This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.

Solid State NMR of Polymers

Solid State NMR of Polymers PDF Author: T. Asakura
Publisher: Elsevier
ISBN: 0080541461
Category : Science
Languages : en
Pages : 1017

Get Book Here

Book Description
In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods.This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described.Features of this book:• Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field• Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists.This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.

NMR of Polymers

NMR of Polymers PDF Author: Frank A. Bovey
Publisher: Academic Press
ISBN: 0080537588
Category : Science
Languages : en
Pages : 471

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Book Description
NMR has made important contributions to our understanding of structure–property relationships in polymers. This book provides an up-to-date and comprehensive overview of the fundamentals of NMR, with applications of multidimensional NMR and the new solution and solid-state methods in polymer science. NMR of Polymers is written by leading authorities for graduate students and professionals in academia and industry. Provides comprehensive overview of NMR in Polymer Science Covers multidimensional NMR Includes new solution and solid state methods Addresses chain conformation and dynamics

Nuclear Magnetic Resonance in Solid Polymers

Nuclear Magnetic Resonance in Solid Polymers PDF Author: Vincent J. McBrierty
Publisher:
ISBN: 9780521301404
Category : Technology & Engineering
Languages : en
Pages : 347

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Book Description
This book is an authoritative and comprehensive account of the principles and practice of NMR spectroscopy of solids as applied to polymeric materials to determine their structure and dynamics at a molecular level. NMR spectroscopy has been applied to the characterization of polymers in solid state for over 40 years. The past few decades have seen the development of many new NMR capabilities, including high-resolution techniques for solids, multi-dimensional methods, deuterium NMR and others. All of these developments have contributed to a dramatic increase in the power and applicability of NMR for the characterization, at a molecular level, of the dynamics and structural organization of polymeric solids. The applications chapters emphasize the polymer types and properties. The authors have included an introduction to all the main principles of the technique involved in its application to solid polymers. Rigorous and detailed analytical treatment of all main areas is also available.

NMR Methods for Characterization of Synthetic and Natural Polymers

NMR Methods for Characterization of Synthetic and Natural Polymers PDF Author: Rongchun Zhang
Publisher: Royal Society of Chemistry
ISBN: 178801863X
Category : Science
Languages : en
Pages : 590

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Book Description
Since the introduction of FT-NMR spectroscopy around five decades ago, NMR has achieved significant advances in hardware and methodologies, accompanied with the enhancement of spectral resolution and signal sensitivity. Rapid developments in the polymers field mean that accurate and quantitative characterization of polymer structures and dynamics is the keystone for precisely regulating and controlling the physical and chemical properties of the polymer. This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.

NMR Spectroscopy of Polymers

NMR Spectroscopy of Polymers PDF Author: Tatsuki Kitayama
Publisher: Springer Science & Business Media
ISBN: 3662089823
Category : Technology & Engineering
Languages : en
Pages : 231

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Book Description
Based on the authors ́ extensive experimental experience, NMR Spectroscopy of Polymers explains the practical use of NMR spectroscopy in polymer chemistry.

NMR Spectroscopy of Polymers in Solution and in the Solid State

NMR Spectroscopy of Polymers in Solution and in the Solid State PDF Author: H. N. Cheng
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 474

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Book Description
NMR Spectroscopy of Polymers in Solution and in the Solid State includes 31 chapters, which are divided into the following sections: overview, solid state NMR of polymers, solution NMR of synthetic polymers, solution NMR of biopolymers, combined NMR-separation techniques, and dynamics of polymers in solution. NMR Spectroscopy of Polymers in Solution and in the Solid State brings together a variety of papers on both solution and solid state NMR in one convenient volume. Practicing NMR spectroscopists, students, and other newcomers to the field will benefit from the book's dual coverage.

Solid State NMR

Solid State NMR PDF Author: Klaus Müller
Publisher: John Wiley & Sons
ISBN: 352731816X
Category : Science
Languages : en
Pages : 562

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Book Description
Solid State NMR A thorough and comprehensive textbook covering the theoretical background, experimental approaches, and major applications of solid-state NMR spectroscopy Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful non-destructive technique capable of providing information about the molecular structure and dynamics of molecules. Alongside solution-state NMR, a well-established technique to study chemical structures and investigate physico-chemical properties of molecules in solutions, solid-state NMR (SSNMR) offers many exciting possibilities for the analysis of solid and soft materials across scientific fields. SSNMR shows unique capabilities for a detailed investigation of structural and dynamic properties of materials over wide space and time ranges. For this reason, and thanks to significant advances in the past several years, the application of SSNMR to materials is rapidly increasing in disciplines such as chemistry, physics, and materials and life sciences. Solid State NMR: Principles, Methods, and Applications offers a systematic introduction to the theory, methodological concepts, and major experimental methods of SSMR spectroscopy. Exploring the unique potential of SSNMR for the structural and dynamic characterization of soft and either amorphous or crystalline solid materials, this comprehensive textbook provides foundational knowledge and recent developments of SSNMR, covering physical and theoretical background, experimental methods, and applications to pharmaceuticals, polymers, inorganic and hybrid materials, liquid crystals, and model membranes. Written by two expert authors to ensure a clear and consistent presentation of the subject, this textbook: Includes a brief introduction to the historical aspects and broad theoretical background of solid-state NMR spectroscopy Provides helpful illustrations to explain the various SSNMR concepts and methods Features accessible descriptive text with self-consistent use of quantum mechanics Covers the experimental aspects of SSNMR spectroscopy and in particular a description of many useful pulse sequences Contains references to relevant literature Solid State NMR: Principles, Methods, and Applications is the ideal textbook for university courses on SSNMR, advanced spectroscopies, and a valuable single-volume reference for spectroscopists, chemists, and researchers in the field of materials.

A Practical Guide to Understanding the NMR of Polymers

A Practical Guide to Understanding the NMR of Polymers PDF Author: Peter A. Mirau
Publisher: Wiley-Interscience
ISBN:
Category : Science
Languages : en
Pages : 440

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Book Description
A Practical Guide to Understanding the NMR of Polymers presents an introduction to the theory and practice of NMR, and includes sections on the fundamental principles of NMR and the applications to polymers. This book will help readers understand how these methods can be used to determine the chemical structure of polymers that influences the macroscopic properties. Solid state NMR methods are introduced to enable the readers to measure the structure of polymers on longer length scales. It is also shown how NMR is used to measure the molecular dynamics that can be related to the mechanical properties of polymers.

Spectroscopic Analyses

Spectroscopic Analyses PDF Author: Eram Sharmin
Publisher: BoD – Books on Demand
ISBN: 9535136275
Category : Science
Languages : en
Pages : 242

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Book Description
The book presents developments and applications of these methods, such as NMR, mass, and others, including their applications in pharmaceutical and biomedical analyses. The book is divided into two sections. The first section covers spectroscopic methods, their applications, and their significance as characterization tools; the second section is dedicated to the applications of spectrophotometric methods in pharmaceutical and biomedical analyses. This book would be useful for students, scholars, and scientists engaged in synthesis, analyses, and applications of materials/polymers.

NMR Spectroscopy and Polymer Microstructure

NMR Spectroscopy and Polymer Microstructure PDF Author: Alan E. Tonelli
Publisher: Wiley-VCH
ISBN:
Category : Science
Languages : en
Pages : 278

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Book Description
Describes both high resolution solution and solid state techniques; presents applications to synthetic and biological polymers; demonstrates the connection between microstructures, conformations, and NMR spectra of polymers. Annotation copyrighted by Book News, Inc., Portland, OR