Photothermal Spectroscopy Methods for Chemical Analysis PDF Download
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Author: Stephen E. Bialkowski
Publisher: John Wiley & Sons
ISBN: 9780471574675
Category : Science
Languages : en
Pages : 634
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Book Description
A unique guide to the application and theory of photothermalspectroscopy. This book debunks the myth that photothermal spectroscopy is toocomplicated for practical application to chemical analysis, anddemonstrates the advantages this technique has over conventionalspectroscopy in facilitating extremely sensitive measurements ofoptical absorption in homogeneous media. The book covers thesubject from the ground up, lists all practical considerationsneeded to obtain accurate results, and provides a working knowledgeof the various methods in use--including photo acoustics andphotopyroelectric techniques. Bringing together a wealth of information that has been scatteredthroughout the professional literature, Photothermal SpectroscopyMethods for Chemical Analysis covers methods and information thatshould be known to every analytical chemist, including: * Descriptions of photothermal spectroscopy using a consistentmathematical language * Helpful examples from the literature of analytical applicationsand current research * Illustrations of all important points, consistent equations, andnumerous original figures * A discussion of laser technology and how it is used to obtainaccurate results from extremely small samples of a few molecules * Everything spectroscopists need to know to construct their ownapparatus and use it to conduct successful experiments * Tips on how to interpret experimental results effectively whenusing nonlinear processes and in many other situations inphotothermal spectroscopy * Considerations for further study of heterogeneous sampleanalysis * Unified nomenclature of the patchwork of terms used byresearchers in analytical and physical chemistry, physics, andoptical engineering * Equations that are derived with the aid of a symbolic languageprocessor to ensure correct results Photothermal spectroscopy has seen major advances since the adventof laser technology twenty-five years ago. It is now possible,using a laser's coherent and powerful output, to obtain extremelysensitive measurements of optical absorption that exceed those ofmass spectroscopy by two or three times, and produce accurateresults from only a few molecules. Focusing on samples in homogeneous media, this book provides aunique guide--incorporating theory and application--to allavailable photothermal spectroscopy techniques for chemical andmaterial analysis. It uses a systematic approach in itscomprehensive treatment of the theory, and covers all the necessarybackground material, from laser optics to fluid dynamics. This accessible text describes the various processes used to detectthermal perturbation of a sample, ranging from optical excitationto nonlinear processes, and covers all optical principles necessaryto understand photothermal spectroscopy. When dealing withhydrodynamic equations that govern energy transfer in the samplematrix, it provides an original impulse-response approach. Inaddition, the book explains how to construct the apparatus oneneeds to conduct successful photothermal experiments, sincecommercial equipment is not available as in conventionalspectrophotometry. Throughout, this book draws on information from a wide range offields, including analytical spectroscopy, measurement physics,physical optics, and chemical dynamics. Providing clearexplanations at every turn, the author demonstrates a completeunderstanding of the theory and applications as a firm basis forthe correct interpretation of experimental results. For analytical chemists, as well as for students at the graduatelevel, Photothermal Spectroscopy Methods for Chemical Analysis isan unmatched resource that develops a consistent mathematical basisfor signal description, consolidates previous theories, andprovides invaluable insight into laser technology.
Author: Stephen E. Bialkowski
Publisher: John Wiley & Sons
ISBN: 9780471574675
Category : Science
Languages : en
Pages : 634
Get Book Here
Book Description
A unique guide to the application and theory of photothermalspectroscopy. This book debunks the myth that photothermal spectroscopy is toocomplicated for practical application to chemical analysis, anddemonstrates the advantages this technique has over conventionalspectroscopy in facilitating extremely sensitive measurements ofoptical absorption in homogeneous media. The book covers thesubject from the ground up, lists all practical considerationsneeded to obtain accurate results, and provides a working knowledgeof the various methods in use--including photo acoustics andphotopyroelectric techniques. Bringing together a wealth of information that has been scatteredthroughout the professional literature, Photothermal SpectroscopyMethods for Chemical Analysis covers methods and information thatshould be known to every analytical chemist, including: * Descriptions of photothermal spectroscopy using a consistentmathematical language * Helpful examples from the literature of analytical applicationsand current research * Illustrations of all important points, consistent equations, andnumerous original figures * A discussion of laser technology and how it is used to obtainaccurate results from extremely small samples of a few molecules * Everything spectroscopists need to know to construct their ownapparatus and use it to conduct successful experiments * Tips on how to interpret experimental results effectively whenusing nonlinear processes and in many other situations inphotothermal spectroscopy * Considerations for further study of heterogeneous sampleanalysis * Unified nomenclature of the patchwork of terms used byresearchers in analytical and physical chemistry, physics, andoptical engineering * Equations that are derived with the aid of a symbolic languageprocessor to ensure correct results Photothermal spectroscopy has seen major advances since the adventof laser technology twenty-five years ago. It is now possible,using a laser's coherent and powerful output, to obtain extremelysensitive measurements of optical absorption that exceed those ofmass spectroscopy by two or three times, and produce accurateresults from only a few molecules. Focusing on samples in homogeneous media, this book provides aunique guide--incorporating theory and application--to allavailable photothermal spectroscopy techniques for chemical andmaterial analysis. It uses a systematic approach in itscomprehensive treatment of the theory, and covers all the necessarybackground material, from laser optics to fluid dynamics. This accessible text describes the various processes used to detectthermal perturbation of a sample, ranging from optical excitationto nonlinear processes, and covers all optical principles necessaryto understand photothermal spectroscopy. When dealing withhydrodynamic equations that govern energy transfer in the samplematrix, it provides an original impulse-response approach. Inaddition, the book explains how to construct the apparatus oneneeds to conduct successful photothermal experiments, sincecommercial equipment is not available as in conventionalspectrophotometry. Throughout, this book draws on information from a wide range offields, including analytical spectroscopy, measurement physics,physical optics, and chemical dynamics. Providing clearexplanations at every turn, the author demonstrates a completeunderstanding of the theory and applications as a firm basis forthe correct interpretation of experimental results. For analytical chemists, as well as for students at the graduatelevel, Photothermal Spectroscopy Methods for Chemical Analysis isan unmatched resource that develops a consistent mathematical basisfor signal description, consolidates previous theories, andprovides invaluable insight into laser technology.
Author: Stephen E. Bialkowski
Publisher: John Wiley & Sons
ISBN: 1119279070
Category : Science
Languages : en
Pages : 512
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Book Description
Covers the advantages of using photothermal spectroscopy over conventional absorption spectroscopy, including facilitating extremely sensitive measurements and non-destructive analysis This unique guide to the application and theory of photothermal spectroscopy has been newly revised and updated to include new methods and applications and expands on applications to chemical analysis and material science. The book covers the subject from the ground up, lists all practical considerations needed to obtain accurate results, and provides a working knowledge of the various methods in use. Photothermal Spectroscopy Methods, Second Edition includes the latest methods of solid state and materials analysis, and describes new chemical analysis procedures and apparatuses in the analytical chemistry sections. It offers a detailed look at the optics, physical principles of heat transfer, and signal analysis. Information in the temperature change and optical elements in homogeneous samples and photothermal spectroscopy in homogeneous samples has been updated with a better description of diffraction effects and calculations. Chapters on analytical measurement and data processing and analytical applications are also updated and include new information on modern applications and photothermal microscopy. Finally, the Photothermal Spectroscopy of Heterogeneous Sample chapter has been expanded to incorporate new methods for materials analysis. New edition updates and expands on applications to chemical analysis and materials science, including new methods of solid state and materials analysis Includes new chemical analysis procedures and apparatuses Provides an unmatched resource that develops a consistent mathematical basis for signal description, consolidates previous theories, and provides invaluable insight into laser technology Photothermal Spectroscopy Methods, Second Edition will appeal to researchers from both academia and industry (graduate students, postdocs, research scientists, and professors) in the general field of analytical chemistry, optics, and materials science, and researchers and engineers at scientific instrument developers in fields related to photonics and spectroscopy.
Author: Ute Pyell
Publisher: John Wiley & Sons
ISBN: 0470871032
Category : Science
Languages : en
Pages : 552
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Book Description
This book offers a thorough theoretical description of the method, an overview on the current status of the various forms of electrokinetic capillary chromatography, plus a look forward into future developments. Focuses on the technique of electrokinetic capillary chromatography and its applications in various areas, including pharmaceutical, industrial, environmental, and biological chemistry Features invaluable information put together from experienced researchers in the area First book to discuss this technique in detail Covers a topic that is part of the exploding field of hyphenated techniques Selected international contributors working in research in this area
Author: James G. Speight
Publisher: John Wiley & Sons
ISBN: 0471718505
Category : Science
Languages : en
Pages : 239
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Book Description
All the guidance needed to test coal and analyze the results With the skyrocketing costs of most fuel sources, government, industry, and consumers are taking a greater interest in coal, an abundant and inexpensive alternative, which has been made more environmentally friendly through new technology. Published in response to this renewed interest, Handbook of Coal Analysis provides readers with everything they need to know about testing and analyzing coal. Moreover, it explains the meaning of test results and how these results can predict coal behavior and its corresponding environmental impact during use. The thorough coverage of coal analysis includes: * Detailed presentation of necessary standard tests and procedures * Explanation of coal behavior relative to its usage alongside the corresponding environmental issues * Coverage of nomenclature, terminology, sampling, and accuracy and precision of analysis * Step-by-step test method protocols for proximate analysis, ultimate analysis, mineral matter, physical and electrical properties, thermal properties, mechanical properties, spectroscopic properties, and solvent properties * Emphasis on relevant American Society for Testing and Materials (ASTM) standards and test methods, including corresponding International Organization for Standardization (ISO) and British Standards Institution (BSI) test method numbers To assist readers in understanding the material, a glossary of terms is provided. Each term is defined in straightforward language that enables readers to better grasp complex concepts and theory. References at the end of each chapter lead readers to more in-depth discussions of specialized topics. This is an essential reference for analytical chemists, process chemists, and engineers in the coal industry as well as other professionals and researchers who are looking to coal as a means to decrease dependence on foreign oil sources and devise more efficient, cleaner methods of energy production.
Author: James G. Speight
Publisher: John Wiley & Sons
ISBN: 0471739847
Category : Science
Languages : en
Pages : 368
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Book Description
A timely, hands-on guide to environmental issues and regulatorystandards for the petroleum industry Environmental analysis and testing methods are an integral part ofany current and future refining activities. Today's petroleumrefining industry must be prepared to meet a growing number ofchallenges, both environmental and regulatory. Environmental Analysis and Technology for the Refining Industryfocuses on the analytical issues inherent in any environmentalmonitoring or cleanup program as they apply to today's petroleumindustry, not only during the refining process, but also duringrecovery operations, transport, storage, and utilization. Designedto help today's industry professionals identify test methods formonitoring and cleanup of petroleum-based pollutants, the bookprovides examples of the application of environmental regulationsto petroleum refining and petroleum products, as well as currentand proposed methods for the mitigation of environmental effectsand waste management. Part I introduces petroleum technology, refining, and products, andreviews the nomenclature used by refiners, environmentalscientists, and engineers. Part II discusses environmentaltechnology and analysis, and provides information on environmentalregulation and the impact of refining. Coverage includes: * In-depth descriptions of analyses related to gaseous emissions,liquid effluents, and solid waste * A checklist of relevant environmental regulations * Numerous real-world examples of the application of environmentalregulations to petroleum refining and petroleum products * An analysis of current and proposed methods of environmentalprotection and waste management
Author: Perry G. Wang
Publisher: John Wiley & Sons
ISBN: 1118907795
Category : Science
Languages : en
Pages : 257
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Book Description
HIGH THROUGHPUT ANALYSIS FOR FOOD SAFETY MEETS FSMA REQUIREMENTS WITH THE LATEST ADVANCES IN HIGH-THROUGHPUT SCREENING High-Throughput Analysis for Food Safety addresses the fundamental concepts involved in the rapid screening for contaminants, including residual veterinary drugs, proteins, metals, hormones, pesticides, and adulterants. Addressing the need for—and requirements of—rapid screening tests, the book includes discussions of regulations and compliance issues from perspectives of both domestic and global industry and government contributors. The latest developments and most common techniques are focused on, with an emphasis on the applicability of both stand-alone mass spectrometry methods and coupled techniques. Beginning with a review of high-throughput analysis basics, the authors conduct a full exploration of mass spectrometry applications allowing readers to: Survey GC-MS, LC-MS, stand-alone MS, and tandem MS methods in foodanalysis and contaminant screening Review quality control standards, method validation, and ongoing analyticalcontrol Examine the current methods used to detect veterinary medicinal productresidues in food, as well as future directionsRecent Recent incidents around the globe have turned the food industry toward high-throughput analysis, and the Food Safety Modernization Act has made it a legal requirement in the US. This resource provides an in-depth discussion of the latest advances in methods and instrumentation.
Author: James G. Speight
Publisher: John Wiley & Sons
ISBN: 1118986350
Category : Science
Languages : en
Pages : 368
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Book Description
Introduces the reader to the production of the products in a refinery • Introduces the reader to the types of test methods applied to petroleum products, including the need for specifications • Provides detailed explanations for accurately analyzing and characterizing modern petroleum products • Rewritten to include new and evolving test methods • Updates on the evolving test methods and new test methods as well as the various environmental regulations are presented
Author: Peter R. Griffiths
Publisher: John Wiley & Sons
ISBN: 0470106298
Category : Science
Languages : en
Pages : 556
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Book Description
A bestselling classic reference, now expanded and updated to cover the latest instrumentation, methods, and applications The Second Edition of Fourier Transform Infrared Spectrometry brings this core reference up to date on the uses of FT-IR spectrometers today. The book starts with an in-depth description of the theory and current instrumentation of FT-IR spectrometry, with full chapters devoted to signal-to-noise ratio and photometric accuracy. Many diverse types of sampling techniques and data processing routines, most of which can be performed on even the less expensive instruments, are then described. Extensively updated, the Second Edition: * Discusses improvements in optical components * Features a full chapter on FT Raman Spectrometry * Contains new chapters that focus on different ways of measuring spectra by FT-IR spectrometry, including fourteen chapters on such techniques as microspectroscopy, internal and external reflection, and emission and photoacoustic spectrometry * Includes a new chapter introducing the theory of vibrational spectrometry * Organizes material according to sampling techniques Designed to help practitioners using FT-IR capitalize on the plethora of techniques for modern FT-IR spectrometry and plan their experimental procedures correctly, this is a practical, hands-on reference for chemists and analysts. It's also a great resource for students who need to understand the theory, instrumentation, and applications of FT-IR.
Author: Raymond E. March
Publisher: John Wiley & Sons
ISBN: 0471717975
Category : Science
Languages : en
Pages : 389
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Book Description
A definitive reference, completely updated Published in 1989, the First Edition of this book, originally entitled Quadrupole Storage Mass Spectrometry, quickly became the definitive reference in analytical laboratories worldwide. Revised to reflect scientific and technological advances and new applications in the field, the Second Edition includes new chapters covering: * New ion trap instruments of high sensitivity * Peptide analysis by liquid chromatography/ion trap tandem mass spectrometry * Analytical aspects of ion trap mass spectrometry combined with gas chromatography * Simulation of ion trajectories in the ion trap One additional chapter discusses the Rosetta mission, a "comet chaser" that was sent on a ten-year journey in 2004 to study the comet Churyumov-Gerasimenko using, among other instruments, a GC/MS system incorporating a specially designed ion trap mass spectrometer. This comprehensive reference also includes discussions of the history of the quadrupole ion trap, the theory of quadrupole mass spectrometry, the dynamics of ion-trapping chemistry in the quadrupole ion trap, the cylindrical ion trap, miniature traps, and linear ion traps. Complete with conclusions and references, this primer effectively encapsulates the body of knowledge on quadrupole ion trap mass spectrometry. With its concise descriptions of the theory of ion motion and the principles of operation, Quadrupole Ion Trap Mass Spectrometry, Second Edition is ideal for new users of quadrupole devices, as well as for scientists, researchers, and graduate and post-doctoral students working in analytical laboratories.
Author: Charles L. Wilkins
Publisher: John Wiley & Sons
ISBN: 0471748633
Category : Science
Languages : en
Pages : 377
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Book Description
A multidisciplinary approach to understanding the fundamentals of mass spectrometry for bacterial analysis From chemotaxonomy to characterization of targeted proteins, Identification of Microorganisms by Mass Spectrometry provides an overview of both well-established and cutting-edge mass spectrometry techniques for identifying microorganisms. A vital tool for microbiologists, health professionals, and analytical chemists, the text is designed to help scientists select the most effective techniques for use in biomedical, biochemical, pharmaceutical, and bioterror defense applications. Since microbiological applications of mass spectrometry require a basic understanding of both microbiology and analytical chemistry, the editors have incorporated material from both disciplines so that readers from either field will come to understand the necessary principles of the other. Featuring contributions from some of the most recognized experts in both fields, this volume provides specific examples of fundamental methods as well as approaches developed in the last decade, including: * Metastable atom bombardment pyrolysis mass spectrometry * Matrix-assisted laser desorption/ionization mass spectrometry (MALDI) * MALDI time-of-flight mass spectrometry (MALDI-TOF MS) of intact bacteria * High-resolution Fourier transform mass spectrometry (FTMS) * Electrospray ionization (ESI) mass spectrometry Identification of Microorganisms by Mass Spectrometry represents the most comprehensive and up-to-date work on the topic currently available. It is liberally illustrated with figures and tables and covers every aspect of spectrometric identification of microorganisms, including experimental procedures, various means of sample preparation, data analysis, and interpretation of complex mass spectral data.
