Mass Spectrometry in Polymer Chemistry PDF Download
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Author: Christopher Barner-Kowollik
Publisher: John Wiley & Sons
ISBN: 3527641831
Category : Science
Languages : en
Pages : 501
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Book Description
Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.
Author: Christopher Barner-Kowollik
Publisher: John Wiley & Sons
ISBN: 3527641831
Category : Science
Languages : en
Pages : 501
Get Book Here
Book Description
Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.
Author: Giorgio Montaudo
Publisher: CRC Press
ISBN: 1420037757
Category : Science
Languages : en
Pages : 601
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Book Description
Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results
Author: Liang Li
Publisher: John Wiley & Sons
ISBN: 0470567228
Category : Science
Languages : en
Pages : 325
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Book Description
Principles and Practices of Polymer Mass Spectrometry helps readers acquire the skills necessary for selecting the optimal methods, handling samples, analyzing the data, and interpreting the results of the mass spectrometry of polymers. This guide describes the principles of polymer MS and best practices in polymer characterization. It discusses different approaches, including MALDI, ESI, TOF MS, and FT-MS. It provides a guide to developing appropriate sample preparation protocols for different polymers. Complete with examples of applications and experiments, this is an excellent reference for scientists, researchers, graduate students, and others.
Author: Harald Pasch
Publisher: Springer Science & Business Media
ISBN: 9783540442592
Category : Science
Languages : en
Pages : 334
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Book Description
MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF instrumentation. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers. With many examples, the monograph examines experimental protocols for the determination of endgroups, the analysis of copolymers and additives, and the coupling of liquid chromatography and MALDI-TOF in detail.
Author: Minna Hakkarainen
Publisher: Springer
ISBN: 9783642446849
Category : Technology & Engineering
Languages : en
Pages : 0
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Book Description
Emerging Mass Spectrometric Tools for Analysis of Polymers and Polymer Additives, by Nina Aminlashgari and Minna Hakkarainen. Analysis of Polymer Additives and Impurities by Liquid Chromatography/Mass Spectrometry and Capillary Electrophoresis/Mass Spectrometry, by Wolfgang Buchberger and Martin Stiftinger. Direct Insertion Probe Mass Spectrometry of Polymers, by Jale Hacaloglu Mass Spectrometric Characterization of Oligo- and Polysaccharides and Their Derivatives, by Petra Mischnick. Electrospray Ionization-Mass Spectrometry for Molecular Level Understanding of Polymer Degradation, by Minna Hakkarainen.
Author: J.L. Koenig
Publisher: Elsevier
ISBN: 0080541577
Category : Technology & Engineering
Languages : en
Pages : 509
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Book Description
This revised and updated Second Edition of the best-selling reference/text is essential reading for students and scientists who seek a thorough and practical introduction to the field of polymer spectroscopy. Eleven chapters cover the fundamental aspects and experimental applications of the primary spectroscopic methods. The advantages and disadvantages of the various techniques for particular polymer systems are also discussed. The goal of the author is not to make the reader an expert in the field, but rather to provide enough information about the different spectroscopic methods that the reader can determine how the available techniques can be used to solve a particular polymer problem. This Second Edition contains new and updated information on techniques in IR and NMR, as well as an all-new chapter on Mass Spectrometry.
Author: Shin Tsuge
Publisher: Elsevier
ISBN: 0444538933
Category : Science
Languages : en
Pages : 405
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Book Description
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. - Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification - Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique - All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification - Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample
Author: Edward Grant Brame
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 312
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Book Description
Applications of Polymer Spectroscopy focuses on the use of spectroscopy for the determination of polymer structure. This book is divided into three general areas of spectroscopy: nuclear magnetic resonance (NMR) spectroscopy, infrared spectroscopy, and mass spectroscopy. This text is comprised of 16 chapters and begins with a discussion on the applications of NMR spectroscopy, including carbon-13 NMR, proton NMR, and fluorine-19 NMR. The next section considers infrared spectroscopy, with special consideration to the Fourier transform method and the dynamic method of handling the examination of ...
Author: Muhammad Imran Malik
Publisher: Elsevier
ISBN: 012822598X
Category : Technology & Engineering
Languages : en
Pages : 670
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Book Description
Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. - Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity - Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material - Establishes a strong link between basic principles, characterization techniques, and real-life applications
Author: Muralisrinivasan Natamai Subramanian
Publisher: CRC Press
ISBN: 1000794377
Category : Science
Languages : en
Pages : 236
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Book Description
Basics of Polymer Chemistry is of great interest to the chemistry audience. The basic properties of polymers, including diverse fundamental and applied aspects, are presented. This book constitutes a basis for understanding polymerization, and it presents a comprehensive overview of the scientific research of polymers. The chapters presented can be used as a reference for those interested in understanding the sustainable development in polymers.Basics of Polymer Chemistry provides a balanced coverage of the key developments in this field, and highlights recent and emerging technical achievements. The topics covered present a comprehensive overview of the subject area and are therefore of interest to professors and students. The recent developments in polymerization using catalysts, homo and copolymerization are presented, and it contains current efforts in designing new polymer architectures. Improved property performance attributes of the polymers by controlling their molecular-structural characteristics such as molecular weight distribution, comonomer type content distribution, and branching level are also discussed.
