High Resolution NMR in Solids Selective Averaging PDF Download
Are you looking for read ebook online? Search for your book and save it on your Kindle device, PC, phones or tablets. Download High Resolution NMR in Solids Selective Averaging PDF full book. Access full book title High Resolution NMR in Solids Selective Averaging by Ulrich Haeberlen. Download full books in PDF and EPUB format.
Author: Ulrich Haeberlen
Publisher: Elsevier
ISBN: 0323160255
Category : Science
Languages : en
Pages : 205
Get Book Here
Book Description
High Resolution NMR in Solids: Selective Averaging presents the principles and applications of the four approaches to high resolution NMR in solids — magic-angle sample spinning, multiple-pulse, proton-enhanced nuclear induction, and indirect detection methods. Divided into six chapters, this book initially describes the tensorial properties of nuclear spin interactions in both ordinary and spin spaces. It then deals with the manifestations of nuclear magnetic shielding in NMR spectra of both single-crystal and powder samples, and then discusses the techniques for analyzing spectra and rotation patterns in terms of shielding tensors. A wide range of NMR phenomena that are result of intentional or natural, selective or unselective averaging processes and the average Hamiltonian theory that yields the inclusion of correction are covered. This book also provides a detailed discussion on multiple-pulse sequences intended for high resolution NMR in solids. The concluding chapter examines the applications of multiple-pulse techniques, with particular emphasis on measurements of 19F and 1H shielding tensors. Discussions on rotations of angular momentum operators; time ordering and the Magnus expansion; off-resonance averaging of the second-order dipolar Hamiltonian; and phase transients are covered in the supplemental texts.
Author: Ulrich Haeberlen
Publisher: Elsevier
ISBN: 0323160255
Category : Science
Languages : en
Pages : 205
Get Book Here
Book Description
High Resolution NMR in Solids: Selective Averaging presents the principles and applications of the four approaches to high resolution NMR in solids — magic-angle sample spinning, multiple-pulse, proton-enhanced nuclear induction, and indirect detection methods. Divided into six chapters, this book initially describes the tensorial properties of nuclear spin interactions in both ordinary and spin spaces. It then deals with the manifestations of nuclear magnetic shielding in NMR spectra of both single-crystal and powder samples, and then discusses the techniques for analyzing spectra and rotation patterns in terms of shielding tensors. A wide range of NMR phenomena that are result of intentional or natural, selective or unselective averaging processes and the average Hamiltonian theory that yields the inclusion of correction are covered. This book also provides a detailed discussion on multiple-pulse sequences intended for high resolution NMR in solids. The concluding chapter examines the applications of multiple-pulse techniques, with particular emphasis on measurements of 19F and 1H shielding tensors. Discussions on rotations of angular momentum operators; time ordering and the Magnus expansion; off-resonance averaging of the second-order dipolar Hamiltonian; and phase transients are covered in the supplemental texts.
Author:
Publisher:
ISBN:
Category : Magnetic resonance
Languages : en
Pages : 190
Get Book Here
Book Description
Author:
Publisher:
ISBN:
Category :
Languages : en
Pages : 0
Get Book Here
Book Description
Author: T. Asakura
Publisher: Elsevier
ISBN: 0080541461
Category : Science
Languages : en
Pages : 1017
Get Book Here
Book Description
In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods.This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described.Features of this book:• Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field• Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists.This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.
Author: S.J. Spells
Publisher: Springer Science & Business Media
ISBN: 9401112622
Category : Science
Languages : en
Pages : 380
Get Book Here
Book Description
The last decade or so has seen a dramatic increase in the amount of detailed structural information available from a range of experimental techniques. Exciting new techniques such as atomic force microscopy have become widely available, while the potential of established methods like X-ray diffraction and electron microscopy has been greatly enhanced by powerful new sources and analytical methods. Progress in computing has also had a widespread impact: in areas such as neutron scattering, large data sets can now be manipulated more readily. The software supplied with commercial instruments generally provides more sophisti cated analytical facilities, while time-resolved X-ray studies rely on rapid data handling capabilities. The polymer scientist is faced with an expanding array of experimental tools for addressing both fundamental science and industrial problems. This work reviews some recent developments in structural techniques, with the aim of presenting the current 'state of the art' in a selection of areas.
Author: Graham A. Webb
Publisher: Academic Press
ISBN: 0123743370
Category : Science
Languages : en
Pages : 225
Get Book Here
Book Description
The great importance of NMR in many areas of scientific research is once again highlighted in this volume of Annual Reports on NMR Spectroscopy. Provides updates on the latest developments in NMR spectroscopy Includes comprehensive review articles Highlights the increasing importance of NMR spectroscopy as a technique for structural determination
Author: B. Blümich
Publisher: Springer Science & Business Media
ISBN: 3642784836
Category : Science
Languages : en
Pages : 286
Get Book Here
Book Description
1. A.-R. Grimmer, Berlin, FRG; B. Bl}mich, Aachen, FRG: Introduction to Solid-State NMR 2. F. Laupretre, Paris, France: High-Resolution 13C NMRInvestigations of Local Dynamics in Bulk Polymers at Temperatures Below andAbove the Glass-Transition Temperature 3. D. Raftery, Philadelphia, PA;B.F. Chmelka, Santa Barbara, CA: Xenon NMR Spectroscopy 4. G. Fleischer, Leipzig, FRG; F. Fujara, Mainz, FRG: NMR as a Generalized Incoherent Scattering Experiment 5. P. Bl}mler, B. Bl}mich, Mainz, FRG: NMR Imaging of Solids.
Author: Bernhard Blümich
Publisher: Springer Science & Business Media
ISBN: 9783540236054
Category : Medical
Languages : en
Pages : 262
Get Book Here
Book Description
The NMR Notebook is a set of lecture notes for scientists and engineers who want to refresh their knowledge on NMR. Equally, the Notebookgiveslecturers an aid to provide a framework of basic knowhow covering all fields of NMR,i.e. NMR methodology and hardware, chemical analysis, 2D-spectroscopy, NMR imaging, flow NMR, and quality-control NMR. The material is presented in a Power-Pointformat, with pairs of sheets addressing particular topics. One sheet is text, stating the key information, the other a color illustration. Rigorous derivations are avoided in favor of intuitive arguments. The notebook is intended for beginning graduate students and doctoral students of Physics, Chemistry, Chemical Engineering, and Material Science. The information has been organized and selected fora one-semester, two-hour course. At present there is no other teaching and learning text that addresses the different aspects of NMR in such a comprehensive fashion
Author: A. Abragam
Publisher: Oxford University Press
ISBN: 9780198539629
Category : Medical
Languages : en
Pages : 586
Get Book Here
Book Description
This book is a tribute to E.L. Hahn, an outstanding physicist whose discovery of spin echoes and demonstration of nuclear free induction decay led to the most important methods of modern nuclear magnetic resonance. The wide impact of these methods in physics, chemistry, biology, and medicine is fully acknowledged. In addition, Hahn's fundamental contributions in nuclear quadrupole echo phenomena, level crossing techniques, self-induced transparency and laser physics have been of paramount importance. Reflecting the diversity of these key discoveries and their vital influence, the articles presented here offer a stimulating and challenging contribution to the scientific literature which will be read by students and research workers from the wide range of disciplines using NMR techniques.
Author: Donald O. Thompson
Publisher: Springer Science & Business Media
ISBN: 1461528488
Category : Technology & Engineering
Languages : en
Pages : 2393
Get Book Here
Book Description
These Proceedings, consisting of Parts A and B, contain the edited versions of most of the papers presented at the annual Review of Progress in Quantitative Nondestructive Evaluation held at the University of California San Diego, in La Jolla, California on July 19- July 24, 1992. The Review was organized by the Center for NDE at Iowa State University and the Ames Laboratory of the USDOE in cooperation with a number of organizations including the Air Force Wright Laboratory Materials Directorate, the American Society for Nondestructive Testing, the Center for NDE at Johns Hopkins University, the Department of Energy, the Federal Aviation Administration, the National Institute of Standards and Technology, the National Science Foundation IndustrylUniversity Cooperative Research Centers, and the Working Group in Quantitative NDE. This year's Review of Progress in QNDE was attended by approximately 475 participants from the U. S. and many foreign countries who presented over 380 papers. With such a large volume of work to review, the meeting was divided into 36 sessions with as many as four sessions running concurrently. The Review covered all phases of NDE research and development from fundamental investigations to engineering applications or inspection systems, and it included all methods of inspection science from acoustics to x-rays. During the last twenty years, the participants of the Review have contributed to its steady growth. Thanks to their efforts, the Review is today one of the largest and most significant gatherings of NDE researchers and engineers anywhere in the world.
