Synthesis, Morpho-structural Characterization and Environmental Application of Titania Photocatalysts Obtained by Rapid Crystallization PDF Download
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Author: Zsolt Pap
Publisher:
ISBN:
Category :
Languages : en
Pages : 190
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Book Description
Author: Zsolt Pap
Publisher:
ISBN:
Category :
Languages : en
Pages : 190
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Book Description
Author: Michał Marszewski
Publisher:
ISBN:
Category : Nanostructured materials
Languages : en
Pages : 191
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Book Description
The objectives of this dissertation are the design, synthesis, and characterization of titania materials with surface area, porosity, crystallinity and doping tailored toward photocatalytic applications. Ultimately, the research should result in a strategy allowing the synthesis of titania with all these important features. The synthetic methods investigated in this research will include: i) soft-templating, ii) hard-templating, and iii) modified precursor strategy. Soft-templating strategy uses organic templates--either block copolymers or surfactants--that under specific conditions assemble into micelles, and later, these micelles are used to template the desired material around them. The resulting organic-inorganic composite is then calcined in air to remove the organic template and recover the final material with high surface area and large pore volume. This work explores 1) synthesis of titania materials in the presence of polymer templates, and the effects of different synthetic conditions on the structure of the resulting materials. Hard-templating, in contrast to soft-templating, uses inorganic templates. The hard template is introduced during the synthesis to cast its shape onto the fabricated material and removed afterwards, when the material has formed. The final material is an inverse replica of the hard template used, typically with a well-developed mesostructure. This work explores 1) hard templating synthesis of titania materials using silica and alumina, and 2) the effects of the template amount and type. The modified precursor strategy is a novel synthetic method, developed in this research, and designed specifically to achieve titania material with high surface area, large pore volume, high crystallinity, and possibly doping. The modified precursors are prepared by reacting generic titania precursors, such as titanium isopropoxide (TIPO), with organic acids, which results in substitution of some or all alkoxide groups in TIPO structure. The goal is to introduce new, easily carbonizable groups in TIPO structure so that the modified precursor can serve as titania and carbon precursor simultaneously. Subsequently, during carbonization in inert atmosphere, a carbon framework is formed that works as a scaffold, protecting titania during its crystallization. Afterwards, the carbon scaffold is removed by calcination in air. This work explores the modified precursor strategy by 1) preparing titania materials from TIPO modified with different carboxylic acids and 2) investigating the effect of the modifying acid on the properties of the carbon-titania composites and the final titania materials.
Author: Shawn Kendale Blue
Publisher:
ISBN:
Category : Azo dyes
Languages : en
Pages : 87
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Book Description
Studies the synthesis of two types of titanium-based catalysts, ultrasonically treated titania powder and zeolite-supported TiO2. The synthesized catalysts are characterized utilizing both SEM (Scanning Electron Microscopy) and elemental analysis. The synthesized catalysts are then kinetically characterized in the degradation of direct black 38 azo dye.
Author: Dmitry V. Bavykin
Publisher: Royal Society of Chemistry
ISBN: 1847559107
Category : Science
Languages : en
Pages : 177
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Book Description
This exciting new book is a unique compilation of data from a wide range of chemical and spectroscopic instrumentation and the integration of nanostructure characterisation drawn from physical, chemical, electrochemical, spectroscopic and electron microscopic measurements. It fills a gap in the current nanomaterials literature by documenting the latest research from scientific journals and patent literature to provide a concise yet balanced and integrated treatment of an interesting topic: titanium oxide nanostructures within the emerging fashionable area of nanomaterials. Of particular interest are the following key chapters: * Modification and Coating Techniques - provides a unique summary and discussion of available techniques to coat surfaces with nanostructured materials * Chemical Properties - relates structure to surface chemistry and hence applications * Structural and Physical Properties - reviews the relationship between nanostructure and physical properties providing a basis for the rationalisation of applications The book, a valuable reference point, is aimed at professionals, postgraduates and industrial research workers in nanomaterials. Readers will gain a knowledge of the methods for synthesising nanomaterials as well as an understanding of their structure and resulting physical characteristics and a knowledge of their (existing and potential) applications.
Author: Chaudhery Mustansar Hussain
Publisher: John Wiley & Sons
ISBN: 352734294X
Category : Technology & Engineering
Languages : en
Pages : 898
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Book Description
An overview of the current state of nanotechnology-based devices with applications in environmental science, focusing on nanomaterials and polymer nanocomposites. The handbook pays special attention to those nanotechnology-based approaches that promise easier, faster and cheaper processes in environmental monitoring and remediation. Furthermore, it presents up-to-date information on the economics, toxicity and regulations related to nanotechnology in detail. The book closes with a look at the role of nanotechnology for a green and sustainable future. With its coverage of existing and soon-to-be-realized devices this is an indispensable reference for both academic and corporate R&D.
Author: Fabian I. Ezema
Publisher: Springer Nature
ISBN: 3030684628
Category : Technology & Engineering
Languages : en
Pages : 926
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Book Description
This book guides beginners in the areas of thin film preparation, characterization, and device making, while providing insight into these areas for experts. As chemically deposited metal oxides are currently gaining attention in development of devices such as solar cells, supercapacitors, batteries, sensors, etc., the book illustrates how the chemical deposition route is emerging as a relatively inexpensive, simple, and convenient solution for large area deposition. The advancement in the nanostructured materials for the development of devices is fully discussed.
Author: Avanish Kumar Srivastava
Publisher: CRC Press
ISBN: 9814411361
Category : Science
Languages : en
Pages : 418
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Book Description
Nanomaterials, their synthesis, and property studies have been an obsession with modern current physicists, chemist, and materials scientists for their vast array of technological implications and the remarkable way their properties are modified or enhanced when the size dimensions are reduced to the realm of nanometers. Although nanomaterials, for
Author: Walid A. Daoud
Publisher: John Wiley & Sons
ISBN: 1118652363
Category : Technology & Engineering
Languages : en
Pages : 513
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Book Description
With increasing demand for hygienic, self-disinfecting and contamination free surfaces, interest in developing self-cleaning protective materials and surfaces has grown rapidly in recent times. This new title comprises of invited chapters from renowned researchers in the area of self-cleaning nano-coatings and the result is a comprehensive review of current research on both hydrophobic and hydrophilic (photocatalytic effect) self-cleaning materials.
Author: L Karthik
Publisher: CRC Press
ISBN: 0429555784
Category : Medical
Languages : en
Pages : 299
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Book Description
Biological Synthesis of Nanoparticles and Their Applications gives insight into the synthesis of nanoparticles utilizing the natural routes. It demonstrates various strategies for the synthesis of nanoparticles utilizing plants, microscopic organisms like bacteria, fungi, algae and so forth. It orchestrates interdisciplinary hypothesis, ideas, definitions, models and discoveries associated with complex cell of the prokaryotes and eukaryotes. Highlights: Discusses biological approach towards the nanoparticle synthesis Describes the role of nanotechnology in the field of medicine and its medical devices Covers application and usage of the chemicals at the molecular level to act as catalysts and binding products for both organic and inorganic Chemical Reactions Reviews application in physics such as solar cells, photovoltaics and other usage Microorganisms can aggregate and detoxify substantial metals because of different reductase enzymes, which can diminish metal salts to metal nanoparticles. The readers after going through this book will have detailed account of mechanism of bio-synthesis of nanoparticles.
Author: Geoffrey R Mitchell
Publisher: Royal Society of Chemistry
ISBN: 1849735573
Category : Technology & Engineering
Languages : en
Pages : 289
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Book Description
Electrospinning techniques are used to produce novel nanoscale fibrous materials used in a diverse range of applications. Electrospinning: Principles Practice and Possibilities provides a snapshot of the current cutting edge developments of the field. The first chapter introduces readers to electrospinning, followed by different techniques to prepare fibres such as melt electrospinning and colloidal electrospinning, as well as the properties, structures and uses of the nanofibrous materials in energy applications and regenerative medicine and future directions. This balanced and authoritative book will appeal to a broad audience of postgraduate students, industrial and academic researchers in the physical and life sciences as well as engineering.
