Sol-Gel Preparation of Ion-conducting Ceramics for Use in Thin Films

Sol-Gel Preparation of Ion-conducting Ceramics for Use in Thin Films PDF Author: Margaret Irene Steinhauser
Publisher:
ISBN:
Category :
Languages : en
Pages : 234

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Sol-Gel Preparation of Ion-conducting Ceramics for Use in Thin Films

Sol-Gel Preparation of Ion-conducting Ceramics for Use in Thin Films PDF Author: Margaret Irene Steinhauser
Publisher:
ISBN:
Category :
Languages : en
Pages : 234

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Sol-gel Preparation of Ion-conducting Ceramics for Use in Thin Films. [LaSrCoO[sub 3] ; SrCeY[sub X]O[sub 3].

Sol-gel Preparation of Ion-conducting Ceramics for Use in Thin Films. [LaSrCoO[sub 3] ; SrCeY[sub X]O[sub 3]. PDF Author:
Publisher:
ISBN:
Category :
Languages : en
Pages : 108

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A metal alkoxide sol-gel solution suitable for depositing a thin film of La[sub 0.6]Sr[sub 0.4]CoO[sub 3] on a porous substrate has been developed; such films should be useful in fuel cell electrode and oxygen separation membrane manufacture. Crack-free films have been deposited on both dense and porous substrates by dip-coating and spin-coating techniques followed by a heat treatment in air. Fourier transform infrared spectroscopy was used to determine the chemical structure of metal alkoxide solution system. X-ray diffraction was used to determine crystalline phases formed at various temperatures, while scanning electron microscopy was used to determine physical characteristics of the films. Surface coatings have been successfully applied to porous substrates through the control of the substrate pore size, deposition parameters, and firing parameters. Conditions have been defined for which films can be deposited, and for which the physical and chemical characteristics of the film can be improved. A theoretical discussion of the chemical reactions taking place before and after hydrolysis in the mixed alkoxide solutions is presented, and the conditions necessary for successful synthesis are defined. Applicability of these films as ionic and electronic conductors is discussed.

Sol-gel Preparation of Ion-conducting Ceramics for Use in Thin Films

Sol-gel Preparation of Ion-conducting Ceramics for Use in Thin Films PDF Author:
Publisher:
ISBN:
Category :
Languages : en
Pages : 108

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Book Description
A metal alkoxide sol-gel solution suitable for depositing a thin film of La{sub 0.6}Sr{sub 0.4}CoO3 on a porous substrate has been developed; such films should be useful in fuel cell electrode and oxygen separation membrane manufacture. Crack-free films have been deposited on both dense and porous substrates by dip-coating and spin-coating techniques followed by a heat treatment in air. Fourier transform infrared spectroscopy was used to determine the chemical structure of metal alkoxide solution system. X-ray diffraction was used to determine crystalline phases formed at various temperatures, while scanning electron microscopy was used to determine physical characteristics of the films. Surface coatings have been successfully applied to porous substrates through the control of the substrate pore size, deposition parameters, and firing parameters. Conditions have been defined for which films can be deposited, and for which the physical and chemical characteristics of the film can be improved. A theoretical discussion of the chemical reactions taking place before and after hydrolysis in the mixed alkoxide solutions is presented, and the conditions necessary for successful synthesis are defined. Applicability of these films as ionic and electronic conductors is discussed.

Sol-Gel Preparation of Ion-conducting Geramics for Use in Thin Films

Sol-Gel Preparation of Ion-conducting Geramics for Use in Thin Films PDF Author: Margaret Irene Steinhauser
Publisher:
ISBN:
Category :
Languages : en
Pages : 202

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Sol-gel Deposition of Oxide-ion Conducting Thin Films

Sol-gel Deposition of Oxide-ion Conducting Thin Films PDF Author: Jennifer Woodbridge Pell
Publisher:
ISBN:
Category :
Languages : en
Pages : 1414

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Scientific and Technical Aerospace Reports

Scientific and Technical Aerospace Reports PDF Author:
Publisher:
ISBN:
Category : Aeronautics
Languages : en
Pages : 380

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Book Description
Lists citations with abstracts for aerospace related reports obtained from world wide sources and announces documents that have recently been entered into the NASA Scientific and Technical Information Database.

Sol-Gel Technology for Thin Films, Fibers, Preforms, Electronics, and Specialty Shapes

Sol-Gel Technology for Thin Films, Fibers, Preforms, Electronics, and Specialty Shapes PDF Author: Lisa C. Klein
Publisher: William Andrew Publishing
ISBN: 9780815511540
Category : Technology & Engineering
Languages : en
Pages : 407

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Book Description
Covers principles, developments, and applications of sol-gel technology for thin films, fibers, preforms, electronics, and specialty shapes.

Recent Applications in Sol-Gel Synthesis

Recent Applications in Sol-Gel Synthesis PDF Author: Usha Chandra
Publisher: BoD – Books on Demand
ISBN: 9535132458
Category : Science
Languages : en
Pages : 312

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Book Description
Versatility, extended compositional ranges, better homogeneity, lesser energy consumption, and requirement of nonexpensive equipments have boosted the use of sol-gel process on top of the popularity in the synthesis of nanosystems. The sol-gel technique has not only revolutionized oxide ceramics industry and/or material science but has also extended widely into multidimensional applications. The book Recent Applications in Sol-Gel Synthesis comprises 14 chapters that deal mainly with the application-oriented aspects of the technique. Sol-gel prepared metal oxide (MO) nanostructures like nanospheres, nanorods, nanoflakes, nanotubes, and nanoribbons have been employed in biomedical applications involving drug deliveries, mimicking of natural bone, and antimicrobial activities. The possibility of controlling grain size in aerogel and preparation of ultrahigh-temperature ceramic (UHTC)-based materials, fluorescent glasses, ultraviolet photosensors, and photocatalysts have been discussed in detail by the experts in the field. The usefulness of sol-gel materials as active GRIN, as textile finisher, and as leather modifier with water-repellent and oil-resistive properties would be an incentive for researchers keen to pursue the field.

Handbook of Sol-Gel Science and Technology

Handbook of Sol-Gel Science and Technology PDF Author: Lisa Klein
Publisher: Springer Nature
ISBN: 3319321013
Category : Technology & Engineering
Languages : en
Pages : 3755

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Book Description
This completely updated and expanded second edition stands as a comprehensive knowledgebase on both the fundamentals and applications of this important materials processing method. The diverse, international team of contributing authors of this reference clarify in extensive detail properties and applications of sol-gel science and technology as it pertains to the production of substances, active and non-active, including optical, electronic, chemical, sensor, bio- and structural materials. Essential to a wide range of manufacturing industries, the compilation divides into the three complementary sections: Sol-Gel Processing, devoted to general aspects of processing and recently developed materials such as organic-inorganic hybrids, photonic crystals, ferroelectric coatings, and photocatalysts; Characterization of Sol-Gel Materials and Products, presenting contributions that highlight the notion that useful materials are only produced when characterization is tied to processing, such as determination of structure by NMR, in-situ characterization of the sol-gel reaction process, determination of microstructure of oxide gels, characterization of porous structure of gels by the surface measurements, and characterization of organic-inorganic hybrid; and Applications of Sol-Gel Technology, covering applications such as the sol-gel method used in processing of bulk silica glasses, bulk porous gels prepared by sol-gel method, application of sol-gel method to fabrication of glass and ceramic fibers, reflective and antireflective coating films, application of sol-gel method to formation of photocatalytic coating films, and application of sol-gel method to bioactive coating films. The comprehensive scope and integrated treatment of topics make this reference volume ideal for R&D scientists and engineers across a wide range of disciplines and professional interests.

Sol-Gel Technology for Thin Films, Fibers, Preforms, Electronics and Specialty Shapes

Sol-Gel Technology for Thin Films, Fibers, Preforms, Electronics and Specialty Shapes PDF Author: Lisa C. Klein
Publisher: William Andrew
ISBN: 9781493303342
Category : Technology & Engineering
Languages : en
Pages : 428

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Book Description
Covers principles, developments, and applications of sol-gel technology for thin films, fibers, preforms, electronics, and specialty shapes.