Powder Surface Area and Porosity

Powder Surface Area and Porosity PDF Author: S. Lowell
Publisher: Springer Science & Business Media
ISBN: 9400955626
Category : Science
Languages : en
Pages : 244

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Book Description
The rapid growth of interest in powders and their surface properties in many diverse industries prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. It is intended as an introduction to some of the elementary theory and experimental methods used to study the surface area, porosity and density of powders. It may be found useful by those with little or no training in solid surfaces who have the need to quickly learn the rudiments of surface area, density and pore-size measurements. Syosset, New York S. Lowell May, 1983 J. E. Shields Xl List of symbols Use of symbols for purposes other than those indicated in the following list are so defined in the text. Some symbols not shown in this list are defined in the text. d adsorbate cross-sectional area A area; condensation coefficient; collision frequency C BET constant c concentration D diameter; coefficient of thermal diffusion E adsorption potential f permeability aspect factor F flow rate; force; feed rate 9 gravitational constant G Gibbs free energy GS free surface energy h heat of immersion per unit area; height H enthalpy Hi heat of immersion Hsv heat of adsorption BET intercept; filament current k thermal conductivity; specific reaction rate K Harkins-Jura constant I length L heat of liquefaction M mass M molecular weight n number of moles N number of molecules; number of particles N Avagadro's number .

Powder Surface Area and Porosity

Powder Surface Area and Porosity PDF Author: S. Lowell
Publisher: Springer Science & Business Media
ISBN: 9400955626
Category : Science
Languages : en
Pages : 244

Get Book Here

Book Description
The rapid growth of interest in powders and their surface properties in many diverse industries prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. It is intended as an introduction to some of the elementary theory and experimental methods used to study the surface area, porosity and density of powders. It may be found useful by those with little or no training in solid surfaces who have the need to quickly learn the rudiments of surface area, density and pore-size measurements. Syosset, New York S. Lowell May, 1983 J. E. Shields Xl List of symbols Use of symbols for purposes other than those indicated in the following list are so defined in the text. Some symbols not shown in this list are defined in the text. d adsorbate cross-sectional area A area; condensation coefficient; collision frequency C BET constant c concentration D diameter; coefficient of thermal diffusion E adsorption potential f permeability aspect factor F flow rate; force; feed rate 9 gravitational constant G Gibbs free energy GS free surface energy h heat of immersion per unit area; height H enthalpy Hi heat of immersion Hsv heat of adsorption BET intercept; filament current k thermal conductivity; specific reaction rate K Harkins-Jura constant I length L heat of liquefaction M mass M molecular weight n number of moles N number of molecules; number of particles N Avagadro's number .

Powder Surface Area and Porosity

Powder Surface Area and Porosity PDF Author: Seymour Lowell
Publisher: Springer Science & Business Media
ISBN: 9780412396908
Category : Technology & Engineering
Languages : en
Pages : 274

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Book Description
The rapid growth of interest in powders and their surface properties in many diverse industries prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. It is intended as an introduction to some of the elementary theory and experimental methods used to study the surface area, porosity, density, and particle size of powders. It may be found useful by those with little or no training in solid surfaces who have the need to learn quickly the rudiments of surface area, density, pore size, and particle size measurements. S. Lowell J.E. Shields Symbols Use of symbols for purposes other than those indicated in the following table are so defined in the text. Some symbols not shown in the table are also defined in the text. d adsorbate cross-sectional area A area; condensation coefficient; collision frequency C BET constant c concentration D diameter; coefficient of thermal diffusion E adsorption potential permeability aspect factor f F flow rate; force; feed rate g gravitational constant G Gibbs free energy S G free surface energy h heat of immersion per unit area; height H enthalpy heat of immersion Hi heat of adsorption Hsv BET intercept; filament current k thermal conductivity; specific reaction rate K Harkins-Jura constant C length L heat of liquefaction M mass M molecular weight MPa megapascals number of moles n number of molecules; number of particles N N Avogadro's num'ber molecular collisions per square cm per second

Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density

Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density PDF Author: S. Lowell
Publisher: Springer Science & Business Media
ISBN: 1402023030
Category : Science
Languages : en
Pages : 365

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Book Description
The growth of interest in newly developed porous materials has prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. One might consider this new book as the 4th edition of "Powder Surface Area and Porosity" (Lowell & Shields), but for this new edition we set out to incorporate recent developments in the understanding of fluids in many types of porous materials, not just powders. Based on this, we felt that it would be prudent to change the title to "Characterization of Porous Solids and Powders: Surface Area, Porosity and Density". This book gives a unique overview of principles associated with the characterization of solids with regard to their surface area, pore size, pore volume and density. It covers methods based on gas adsorption (both physi and chemisorption), mercury porosimetry and pycnometry. Not only are the theoretical and experimental basics of these techniques presented in detail but also, in light of the tremendous progress made in recent years in materials science and nanotechnology, the most recent developments are described. In particular, the application of classical theories and methods for pore size analysis are contrasted with the most advanced microscopic theories based on statistical mechanics (e.g. Density Functional Theory and Molecular Simulation). The characterization of heterogeneous catalysts is more prominent than in earlier editions; the sections on mercury porosimetry and particularly chemisorption have been updated and greatly expanded.

Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density

Characterization of Porous Solids and Powders: Surface Area, Pore Size and Density PDF Author: Seymour Lowell
Publisher: Springer Science & Business Media
ISBN: 9781402023026
Category : Science
Languages : en
Pages : 370

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Book Description
The growth of interest in newly developed porous materials has prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. One might consider this new book as the 4th edition of "Powder Surface Area and Porosity" (Lowell & Shields), but for this new edition we set out to incorporate recent developments in the understanding of fluids in many types of porous materials, not just powders. Based on this, we felt that it would be prudent to change the title to "Characterization of Porous Solids and Powders: Surface Area, Porosity and Density". This book gives a unique overview of principles associated with the characterization of solids with regard to their surface area, pore size, pore volume and density. It covers methods based on gas adsorption (both physi and chemisorption), mercury porosimetry and pycnometry. Not only are the theoretical and experimental basics of these techniques presented in detail but also, in light of the tremendous progress made in recent years in materials science and nanotechnology, the most recent developments are described. In particular, the application of classical theories and methods for pore size analysis are contrasted with the most advanced microscopic theories based on statistical mechanics (e.g. Density Functional Theory and Molecular Simulation). The characterization of heterogeneous catalysts is more prominent than in earlier editions; the sections on mercury porosimetry and particularly chemisorption have been updated and greatly expanded.

Powder Surface Area and Porosity

Powder Surface Area and Porosity PDF Author: S. Lowell
Publisher: Springer Science & Business Media
ISBN: 9401579555
Category : Technology & Engineering
Languages : en
Pages : 261

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Book Description
The rapid growth of interest in powders and their surface properties in many diverse industries prompted the writing of this book for those who have the need to make meaningful measurements without the benefit of years of experience. It is intended as an introduction to some of the elementary theory and experimental methods used to study the surface area, porosity, density, and particle size of powders. It may be found useful by those with little or no training in solid surfaces who have the need to learn quickly the rudiments of surface area, density, pore size, and particle size measurements. S. Lowell J.E. Shields Symbols Use of symbols for purposes other than those indicated in the following table are so defined in the text. Some symbols not shown in the table are also defined in the text. d adsorbate cross-sectional area A area; condensation coefficient; collision frequency C BET constant c concentration D diameter; coefficient of thermal diffusion E adsorption potential permeability aspect factor f F flow rate; force; feed rate g gravitational constant G Gibbs free energy S G free surface energy h heat of immersion per unit area; height H enthalpy heat of immersion Hi heat of adsorption Hsv BET intercept; filament current k thermal conductivity; specific reaction rate K Harkins-Jura constant C length L heat of liquefaction M mass M molecular weight MPa megapascals number of moles n number of molecules; number of particles N N Avogadro's num'ber molecular collisions per square cm per second

Introduction to Powder Surface Area

Introduction to Powder Surface Area PDF Author: Seymour Lowell
Publisher: John Wiley & Sons
ISBN:
Category : Science
Languages : en
Pages : 224

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Book Description
Good,No Highlights,No Markup,all pages are intact, Slight Shelfwear,may have the corners slightly dented, may have slight color changes/slightly damaged spine.

Surface Area and Porosity Determinations by Physisorption

Surface Area and Porosity Determinations by Physisorption PDF Author: James B. Condon
Publisher: Elsevier
ISBN: 0080481264
Category : Technology & Engineering
Languages : en
Pages : 297

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Book Description
Surface Area and Porosity Determinations by Physisorption is a practical guide for industry or academics to the measurement of surface area and pore size using the tool of physical adsorption. Starting with a brief description of what physical adsorption is and the raw data that is obtained. The instrumentation for measuring this isotherm is described in some details. Recommendations are presented as to what instrumentation would be most appropriate for a particular application. An appendix of current commercial instruments is included. The mathematics required for the simple analysis of the obtained isotherm is presented with step-wise instructions for the analysis of the more useful analysis methods. Subsequent chapters describe the analyses and the theories behind the analyses in more detail.* Includes over 150 figures and tables which illustrate the equipment and examples data acquired * Provides a practical guide for measuring and interpreting physical adsorption * Up-to-date aspects of the more subtle physical adsorption theories such as density functional theory and the quantum mechanical chi theory are presented

Adsorption by Powders and Porous Solids

Adsorption by Powders and Porous Solids PDF Author: Jean Rouquerol
Publisher: Academic Press
ISBN: 0080970362
Category : Technology & Engineering
Languages : en
Pages : 647

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Book Description
The declared objective of this book is to provide an introductory review of the various theoretical and practical aspects of adsorption by powders and porous solids with particular reference to materials of technological importance. The primary aim is to meet the needs of students and non-specialists who are new to surface science or who wish to use the advanced techniques now available for the determination of surface area, pore size and surface characterization. In addition, a critical account is given of recent work on the adsorptive properties of activated carbons, oxides, clays and zeolites. - Provides a comprehensive treatment of adsorption at both the gas/solid interface and the liquid/solid interface - Includes chapters dealing with experimental methodology and the interpretation of adsorption data obtained with porous oxides, carbons and zeolites - Techniques capture the importance of heterogeneous catalysis, chemical engineering and the production of pigments, cements, agrochemicals, and pharmaceuticals

Particle Size Measurement

Particle Size Measurement PDF Author: Terence Allen
Publisher: Springer
ISBN: 0412729504
Category : Technology & Engineering
Languages : en
Pages : 526

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Book Description
This is the fifth edition of the highly successful work first published in 1968, comprising two definitive volumes on particle characterisation. The first volume is devoted to sampling and particle size measurement, while surface area and pore size determination are reviewed in volume 2. Particle size and characterisation are central to understanding powder properties and behaviour. This book describes numerous potential measuring devices, how they operate and their advantages and disadvantages. It comprise a fully comprehensive treatise on the wide range of available equipment with an extensive literature survey, and a list of manufacturers and suppliers. The author's blend of academic and industrial experience results in a readable technical book with information on how to analyse, present, and extract useful information from data. This is an essential reference book for both industrial and academic research workers in a variety of areas including: pharmaceuticals, food science, pollution analysis and control, electronic materials, agricultural products, polymers, pigments and chemicals.

Fundamentals of Laser Powder Bed Fusion of Metals

Fundamentals of Laser Powder Bed Fusion of Metals PDF Author: Igor Yadroitsev
Publisher: Elsevier
ISBN: 0128240911
Category : Technology & Engineering
Languages : en
Pages : 678

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Book Description
Laser powder bed fusion of metals is a technology that makes use of a laser beam to selectively melt metal powder layer-by-layer in order to fabricate complex geometries in high performance materials. The technology is currently transforming aerospace and biomedical manufacturing and its adoption is widening into other industries as well, including automotive, energy, and traditional manufacturing. With an increase in design freedom brought to bear by additive manufacturing, new opportunities are emerging for designs not possible previously and in material systems that now provide sufficient performance to be qualified in end-use mission-critical applications. After decades of research and development, laser powder bed fusion is now enabling a new era of digitally driven manufacturing. Fundamentals of Laser Powder Bed Fusion of Metals will provide the fundamental principles in a broad range of topics relating to metal laser powder bed fusion. The target audience includes new users, focusing on graduate and undergraduate students; however, this book can also serve as a reference for experienced users as well, including senior researchers and engineers in industry. The current best practices are discussed in detail, as well as the limitations, challenges, and potential research and commercial opportunities moving forward. - Presents laser powder bed fusion fundamentals, as well as their inherent challenges - Provides an up-to-date summary of this advancing technology and its potential - Provides a comprehensive textbook for universities, as well as a reference for industry - Acts as quick-reference guide