Author: Francis Onuska
Publisher: Springer Science & Business Media
ISBN: 1468446886
Category : Science
Languages : en
Pages : 291
Book Description
Open Tubular Column Gas Chromatography in Environmental Sciences
Author: Francis Onuska
Publisher: Springer Science & Business Media
ISBN: 1468446886
Category : Science
Languages : en
Pages : 291
Book Description
Publisher: Springer Science & Business Media
ISBN: 1468446886
Category : Science
Languages : en
Pages : 291
Book Description
Open Tubular Column Gas Chromatography in Environmental Sciences
Author: Francis Onuska
Publisher: Springer
ISBN: 9781468446906
Category : Science
Languages : en
Pages : 282
Book Description
The method of choice for analysis of organic pollutants in the environ ment is gas chromatography, using one of the most common detection systems such as flame ionization, electron capture, and mass spectro metric detection. Perhaps the most prevalent difference in practice among the envi ronmental analytical chemists involves the type of column used in gas chromatography. The traditional packed-column gas chromatography is rapidly being replaced with wall-coated open tubular (WCOT) columns. However, in using WCOT columns there are difficulties in reporting analytical data and the means of quantitation. This book is intended to present a survey of the salient features of WCOT column gas chromatography that relate to the selection ofWCOT columns, their technology, separation efficiency, and determination of the principal groups of organic micropollutants, such as hydrocarbons, aromatics, polynuclear aromatic hydrocarbons, organochlorine pollu tants, chlorinated phenols, dioxins, dibenzofurans, ureas, carbamates, and odor-causing substances in complex environmental matrices. Hence, it is the hope of the authors that the content of this book will be of significance to a wide spectrum of disciplines that include environmental chemistry, industrial hygiene and health, toxicology, genetics, and in dustry.
Publisher: Springer
ISBN: 9781468446906
Category : Science
Languages : en
Pages : 282
Book Description
The method of choice for analysis of organic pollutants in the environ ment is gas chromatography, using one of the most common detection systems such as flame ionization, electron capture, and mass spectro metric detection. Perhaps the most prevalent difference in practice among the envi ronmental analytical chemists involves the type of column used in gas chromatography. The traditional packed-column gas chromatography is rapidly being replaced with wall-coated open tubular (WCOT) columns. However, in using WCOT columns there are difficulties in reporting analytical data and the means of quantitation. This book is intended to present a survey of the salient features of WCOT column gas chromatography that relate to the selection ofWCOT columns, their technology, separation efficiency, and determination of the principal groups of organic micropollutants, such as hydrocarbons, aromatics, polynuclear aromatic hydrocarbons, organochlorine pollu tants, chlorinated phenols, dioxins, dibenzofurans, ureas, carbamates, and odor-causing substances in complex environmental matrices. Hence, it is the hope of the authors that the content of this book will be of significance to a wide spectrum of disciplines that include environmental chemistry, industrial hygiene and health, toxicology, genetics, and in dustry.
Analytical Gas Chromatography
Author: Walter Jennings
Publisher: Elsevier
ISBN: 0323141072
Category : Science
Languages : en
Pages : 270
Book Description
Analytical Gas Chromatography is a free-standing introduction to and guide through the rapidly progressing field of analytical gas chromatography. The book is divided into 10 chapters that cover various aspects of analytical gas chromatography, from most advantageous column type to troubleshooting. The opening chapters of the book discuss the advantages of the open tubular column over the packed column. This topic is followed by significant chapters on various variables in the gas chromatographic process, including sample injection, stationary phase, carrier gas, and installation. The effect of changes in these variables on the solution elution order is also considered. A chapter also examines the influence of instrumental design features, such as excessive or unswept volumes in the flow path; suitability of the detection mode; and speed and fidelity of the data-handling equipment. The book also presents selected methods that have been employed to achieve better results for a given gas chromatographic problem. The application areas of gas chromatographic process, including food, flavor, fragrance, petroleum- and chemical-related, environment, biology, and medicine, are also presented. The concluding chapter addresses the basic troubleshooting knowledge and considers other chromatographic problems and methods for their rectification.
Publisher: Elsevier
ISBN: 0323141072
Category : Science
Languages : en
Pages : 270
Book Description
Analytical Gas Chromatography is a free-standing introduction to and guide through the rapidly progressing field of analytical gas chromatography. The book is divided into 10 chapters that cover various aspects of analytical gas chromatography, from most advantageous column type to troubleshooting. The opening chapters of the book discuss the advantages of the open tubular column over the packed column. This topic is followed by significant chapters on various variables in the gas chromatographic process, including sample injection, stationary phase, carrier gas, and installation. The effect of changes in these variables on the solution elution order is also considered. A chapter also examines the influence of instrumental design features, such as excessive or unswept volumes in the flow path; suitability of the detection mode; and speed and fidelity of the data-handling equipment. The book also presents selected methods that have been employed to achieve better results for a given gas chromatographic problem. The application areas of gas chromatographic process, including food, flavor, fragrance, petroleum- and chemical-related, environment, biology, and medicine, are also presented. The concluding chapter addresses the basic troubleshooting knowledge and considers other chromatographic problems and methods for their rectification.
Encyclopedia of Analytical Science
Author:
Publisher: Elsevier
ISBN: 008101984X
Category : Science
Languages : en
Pages : 5142
Book Description
The third edition of the Encyclopedia of Analytical Science, Ten Volume Set is a definitive collection of articles covering the latest technologies in application areas such as medicine, environmental science, food science and geology. Meticulously organized, clearly written and fully interdisciplinary, the Encyclopedia of Analytical Science, Ten Volume Set provides foundational knowledge across the scope of modern analytical chemistry, linking fundamental topics with the latest methodologies. Articles will cover three broad areas: analytical techniques (e.g., mass spectrometry, liquid chromatography, atomic spectrometry); areas of application (e.g., forensic, environmental and clinical); and analytes (e.g., arsenic, nucleic acids and polycyclic aromatic hydrocarbons), providing a one-stop resource for analytical scientists. Offers readers a one-stop resource with access to information across the entire scope of modern analytical science Presents articles split into three broad areas: analytical techniques, areas of application and and analytes, creating an ideal resource for students, researchers and professionals Provides concise and accessible information that is ideal for non-specialists and readers from undergraduate levels and higher
Publisher: Elsevier
ISBN: 008101984X
Category : Science
Languages : en
Pages : 5142
Book Description
The third edition of the Encyclopedia of Analytical Science, Ten Volume Set is a definitive collection of articles covering the latest technologies in application areas such as medicine, environmental science, food science and geology. Meticulously organized, clearly written and fully interdisciplinary, the Encyclopedia of Analytical Science, Ten Volume Set provides foundational knowledge across the scope of modern analytical chemistry, linking fundamental topics with the latest methodologies. Articles will cover three broad areas: analytical techniques (e.g., mass spectrometry, liquid chromatography, atomic spectrometry); areas of application (e.g., forensic, environmental and clinical); and analytes (e.g., arsenic, nucleic acids and polycyclic aromatic hydrocarbons), providing a one-stop resource for analytical scientists. Offers readers a one-stop resource with access to information across the entire scope of modern analytical science Presents articles split into three broad areas: analytical techniques, areas of application and and analytes, creating an ideal resource for students, researchers and professionals Provides concise and accessible information that is ideal for non-specialists and readers from undergraduate levels and higher
Marine Biogenic Lipids, Fats & Oils
Author: Robert George Ackman
Publisher: CRC Press
ISBN: 9780849348891
Category : Science
Languages : en
Pages : 474
Book Description
This monograph will put the biogenic marine lipids of many organisms in perspective. Volume 1 of 2.
Publisher: CRC Press
ISBN: 9780849348891
Category : Science
Languages : en
Pages : 474
Book Description
This monograph will put the biogenic marine lipids of many organisms in perspective. Volume 1 of 2.
Hyphenations of Capillary Chromatography with Mass Spectrometry
Author: Peter Q. Tranchida
Publisher: Elsevier
ISBN: 012809639X
Category : Science
Languages : en
Pages : 516
Book Description
Hyphenations of Capillary Chromatography with Mass Spectrometry provides comprehensive coverage of capillary chromatography with mass spectrometry—both single and multidimensional approaches. The book examines nearly all capillary chromatography approaches, combined with a variety of MS forms, giving readers a wide and detailed view on current-day analytical strategies and applications. Of particular focus are novel developments in the field of MS, such as the Orbitrap, HR ToF, ToF MS with variable electron-impact energy, fast MS-MS and APGC technology. Junior scientists conducting research on mono-dimensional chromatography-MS fundamental relationships and experienced analytical chemists working in conventional capillary chromatography and classical multidimensional chromatography will find this an ideal application-based reference on the hyphenations of these domains. Combines mass spectrometry with a range of chromatographic approaches Emphasizes the importance of both capillary chromatography and mass spectrometry methods, thus stimulating separation scientists to fully exploit both analytical dimensions Authored by two of the world’s leading analytical chemists who have a total of more than 40 years of experience in research and instruction
Publisher: Elsevier
ISBN: 012809639X
Category : Science
Languages : en
Pages : 516
Book Description
Hyphenations of Capillary Chromatography with Mass Spectrometry provides comprehensive coverage of capillary chromatography with mass spectrometry—both single and multidimensional approaches. The book examines nearly all capillary chromatography approaches, combined with a variety of MS forms, giving readers a wide and detailed view on current-day analytical strategies and applications. Of particular focus are novel developments in the field of MS, such as the Orbitrap, HR ToF, ToF MS with variable electron-impact energy, fast MS-MS and APGC technology. Junior scientists conducting research on mono-dimensional chromatography-MS fundamental relationships and experienced analytical chemists working in conventional capillary chromatography and classical multidimensional chromatography will find this an ideal application-based reference on the hyphenations of these domains. Combines mass spectrometry with a range of chromatographic approaches Emphasizes the importance of both capillary chromatography and mass spectrometry methods, thus stimulating separation scientists to fully exploit both analytical dimensions Authored by two of the world’s leading analytical chemists who have a total of more than 40 years of experience in research and instruction
Chromatography Today
Author: C.F. Poole
Publisher: Elsevier
ISBN: 0444596194
Category : Science
Languages : en
Pages : 1037
Book Description
Chromatography Today provides a comprehensive coverage of various separation methods: gas, liquid, thin-layer, and supercritical fluid-chromatography, and capillary electrophoresis. Particular attention is paid to the optimization of these techniques in terms of kinetic parameters and retention mechanisms. When these facts are understood, method selection and optimization becomes a more logical process. Sample preparation methods are treated fully as they frequently represent an integral part of the total analytical method. Also described are preparative-scale separations used for isolating significant amounts of product which are generally achieved under conditions that are not identical to those used for analytical separations. The most common hyphenated methods used for sample identification are discussed from the perspective of the information they yield and the requirements of common interfaces. The scope and level of discussion are designed to be appropriate for various user groups. This book should be suitable for use as a graduate-level student textbook in separation science, a text for professional institutes offering short courses in chromatography, and as a self-study guide for chromatographers to refresh their knowledge of the latest developments in the field. The book is extensively illustrated with over 200 figures, 110 tables and 3,300 references, largely to the contemporary literature.
Publisher: Elsevier
ISBN: 0444596194
Category : Science
Languages : en
Pages : 1037
Book Description
Chromatography Today provides a comprehensive coverage of various separation methods: gas, liquid, thin-layer, and supercritical fluid-chromatography, and capillary electrophoresis. Particular attention is paid to the optimization of these techniques in terms of kinetic parameters and retention mechanisms. When these facts are understood, method selection and optimization becomes a more logical process. Sample preparation methods are treated fully as they frequently represent an integral part of the total analytical method. Also described are preparative-scale separations used for isolating significant amounts of product which are generally achieved under conditions that are not identical to those used for analytical separations. The most common hyphenated methods used for sample identification are discussed from the perspective of the information they yield and the requirements of common interfaces. The scope and level of discussion are designed to be appropriate for various user groups. This book should be suitable for use as a graduate-level student textbook in separation science, a text for professional institutes offering short courses in chromatography, and as a self-study guide for chromatographers to refresh their knowledge of the latest developments in the field. The book is extensively illustrated with over 200 figures, 110 tables and 3,300 references, largely to the contemporary literature.
Principles and Practice of Modern Chromatographic Methods
Author: Kevin Robards
Publisher: Academic Press
ISBN: 012822097X
Category : Science
Languages : en
Pages : 532
Book Description
Principles and Practice of Modern Chromatographic Methods, Second Edition takes a comprehensive, unified approach in its presentation of chromatographic techniques. Like the first edition, the book provides a scientifically rigid, but easy-to-follow presentation of chromatography concepts that begins with the purpose and intent of chromatographic theory - the "what and why that are left out of other books attempting to cover these principles. This fully revised second edition brings the content up-to-date, covering recent developments in several new sections and an additional chapter on composite methods. New topics include sample profiling, sample preparation, sustainable green chemistry, 2D chromatography, miniaturization/nano-LC, HILIC, and more. - Contains thorough chapters that begin with an updated schematic overview and a visual representation of the content - Avoids the obfuscation of different terminologies and classification systems that are prevalent in the area, such as the relationship between liquid chromatography and column chromatography - Provides integrated and comprehensive topic coverage based on chromatographic bibliometrics and survey reports on the relative usage of chromatographic techniques
Publisher: Academic Press
ISBN: 012822097X
Category : Science
Languages : en
Pages : 532
Book Description
Principles and Practice of Modern Chromatographic Methods, Second Edition takes a comprehensive, unified approach in its presentation of chromatographic techniques. Like the first edition, the book provides a scientifically rigid, but easy-to-follow presentation of chromatography concepts that begins with the purpose and intent of chromatographic theory - the "what and why that are left out of other books attempting to cover these principles. This fully revised second edition brings the content up-to-date, covering recent developments in several new sections and an additional chapter on composite methods. New topics include sample profiling, sample preparation, sustainable green chemistry, 2D chromatography, miniaturization/nano-LC, HILIC, and more. - Contains thorough chapters that begin with an updated schematic overview and a visual representation of the content - Avoids the obfuscation of different terminologies and classification systems that are prevalent in the area, such as the relationship between liquid chromatography and column chromatography - Provides integrated and comprehensive topic coverage based on chromatographic bibliometrics and survey reports on the relative usage of chromatographic techniques
Gas Chromatography
Author: Colin Poole
Publisher: Elsevier
ISBN: 0128206772
Category : Science
Languages : en
Pages : 938
Book Description
Gas Chromatography, Second Edition, offers a single source of authoritative information on all aspects relating to the practice of gas chromatography. A focus on short, topic-focused chapters facilitates the identification of information that will be of immediate interest for familiar or emerging uses of gas chromatography. The book gives those working in both academia and industry the opportunity to learn, refresh and deepen their understanding of fundamental and instrumental aspects of gas chromatography and tools for the interpretation and management of chromatographic data. Users will find a consolidated guide to the selection of separation conditions and the use of auxiliary techniques. This new edition restores the contemporary character of the book with respect to those involved in advancing the technology, analyzing the data produced, or applying the technique to new application areas. New topics covered include hyphenated spectroscopic detectors, micromachined instrument platforms, derivatization and related microchemical techniques, petrochemical applications, volatile compounds in the atmosphere, and more. - Includes chapters written by recognized authoritative and visionary experts in the field, thus providing an overview and focused treatments on a single topic - Provides comprehensive coverage of modern gas chromatography, from theory, to methods and selected applications - Places modern developments in research literature into a general context not always apparent to inexperienced users of the techniques
Publisher: Elsevier
ISBN: 0128206772
Category : Science
Languages : en
Pages : 938
Book Description
Gas Chromatography, Second Edition, offers a single source of authoritative information on all aspects relating to the practice of gas chromatography. A focus on short, topic-focused chapters facilitates the identification of information that will be of immediate interest for familiar or emerging uses of gas chromatography. The book gives those working in both academia and industry the opportunity to learn, refresh and deepen their understanding of fundamental and instrumental aspects of gas chromatography and tools for the interpretation and management of chromatographic data. Users will find a consolidated guide to the selection of separation conditions and the use of auxiliary techniques. This new edition restores the contemporary character of the book with respect to those involved in advancing the technology, analyzing the data produced, or applying the technique to new application areas. New topics covered include hyphenated spectroscopic detectors, micromachined instrument platforms, derivatization and related microchemical techniques, petrochemical applications, volatile compounds in the atmosphere, and more. - Includes chapters written by recognized authoritative and visionary experts in the field, thus providing an overview and focused treatments on a single topic - Provides comprehensive coverage of modern gas chromatography, from theory, to methods and selected applications - Places modern developments in research literature into a general context not always apparent to inexperienced users of the techniques
Trace Environmental Quantitative Analysis
Author: Paul R. Loconto
Publisher: CRC Press
ISBN: 1000244830
Category : Science
Languages : en
Pages : 767
Book Description
An introduction to the importance of trace environmental quantitative analysis. Fundamental principles are introduced for the more significant experimental approaches to sample preparation. Principles of instrumental analysis (determinative techniques) for trace organics and trace inorganics analysis. Fundamental principles of measurement and environmental sampling. An introduction to the statistical treatment of trace analytical data. How to calculate instrument detection limits based on weighted least squares confidence band calibration statistics. Includes an updated series of student-tested experiments.
Publisher: CRC Press
ISBN: 1000244830
Category : Science
Languages : en
Pages : 767
Book Description
An introduction to the importance of trace environmental quantitative analysis. Fundamental principles are introduced for the more significant experimental approaches to sample preparation. Principles of instrumental analysis (determinative techniques) for trace organics and trace inorganics analysis. Fundamental principles of measurement and environmental sampling. An introduction to the statistical treatment of trace analytical data. How to calculate instrument detection limits based on weighted least squares confidence band calibration statistics. Includes an updated series of student-tested experiments.