Manufacturing and Mechanical Characterization of Low-cost Isotropic Pitch-based Carbon Fiber

Manufacturing and Mechanical Characterization of Low-cost Isotropic Pitch-based Carbon Fiber PDF Author: Viren Jayantibhai Patel
Publisher:
ISBN:
Category : Carbon fiber-reinforced plastics
Languages : en
Pages : 54

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Book Description
The purpose of this study was to manufacture and mechanically characterize low-cost carbon fiber derived from pitch-based precursor that meets or exceeds the general-purpose carbon fiber. For this study, isotropic coal-tar pitch precursor was used due to its ease in manufacturing carbon fiber and low-cost starting material. Various analyses such as elemental composition, softening point, TGA, FT-IR, NMR, single carbon fiber testing, and SEM were performed to fully characterize the precursor and carbon fiber. Using melt spinning method, the precursor was melt spun at 235 °C, a pressure of 1.5 MPa and a winding speed of 400 rpm to achieve continuous small diameter fibers known as spun/green fibers. The winding speed of the drum collector and the spinneret diameter controlled the overall diameter of the carbon fibers. The green fibers then underwent the thermal treatment processes of stabilization and carbonization. The green fibers were oxidized at 300 °C with a heating rate of 0.25 °C/min in air. Later, they were carbonized at 1100 °C with a heating rate of 1 °C/min in an inert environment. Experimentally it was determined that smaller diameter carbon fibers were easy to fully oxidize with a smaller heating rate. This also resulted in higher mechanical properties due to less defects in their structures. The isotropic pitch-based carbon fiber manufactured in this study have the maximum tensile strength and elastic modulus of 927 MPa and 86 GPa, respectively.

Manufacturing and Mechanical Characterization of Low-cost Isotropic Pitch-based Carbon Fiber

Manufacturing and Mechanical Characterization of Low-cost Isotropic Pitch-based Carbon Fiber PDF Author: Viren Jayantibhai Patel
Publisher:
ISBN:
Category : Carbon fiber-reinforced plastics
Languages : en
Pages : 54

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Book Description
The purpose of this study was to manufacture and mechanically characterize low-cost carbon fiber derived from pitch-based precursor that meets or exceeds the general-purpose carbon fiber. For this study, isotropic coal-tar pitch precursor was used due to its ease in manufacturing carbon fiber and low-cost starting material. Various analyses such as elemental composition, softening point, TGA, FT-IR, NMR, single carbon fiber testing, and SEM were performed to fully characterize the precursor and carbon fiber. Using melt spinning method, the precursor was melt spun at 235 °C, a pressure of 1.5 MPa and a winding speed of 400 rpm to achieve continuous small diameter fibers known as spun/green fibers. The winding speed of the drum collector and the spinneret diameter controlled the overall diameter of the carbon fibers. The green fibers then underwent the thermal treatment processes of stabilization and carbonization. The green fibers were oxidized at 300 °C with a heating rate of 0.25 °C/min in air. Later, they were carbonized at 1100 °C with a heating rate of 1 °C/min in an inert environment. Experimentally it was determined that smaller diameter carbon fibers were easy to fully oxidize with a smaller heating rate. This also resulted in higher mechanical properties due to less defects in their structures. The isotropic pitch-based carbon fiber manufactured in this study have the maximum tensile strength and elastic modulus of 927 MPa and 86 GPa, respectively.

Carbon Fiber Production from Pitch - Cost Analysis - Carbon Fiber E21A

Carbon Fiber Production from Pitch - Cost Analysis - Carbon Fiber E21A PDF Author: Intratec
Publisher: Intratec Solutions
ISBN: 1945324384
Category : Business & Economics
Languages : en
Pages : 52

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Book Description
This report presents a cost analysis of Carbon Fiber production from pitch. The process starts with a preparation step that converts the pitch into mesophase pitch. The mesophase pitch is then stabilized and passes through carbonization, graphitization, surface treatment and sizing, before being winded. This report examines one-time costs associated with the construction of a United States-based plant and the continuing costs associated with the daily operation of such a plant. More specifically, it discusses: * Capital Investment, broken down by: - Total fixed capital required, divided in production unit (ISBL); infrastructure (OSBL) and contingency - Alternative perspective on the total fixed capital, divided in direct costs, indirect costs and contingency - Working capital and costs incurred during industrial plant commissioning and start-up * Production cost, broken down by: - Manufacturing variable costs (raw materials, utilities) - Manufacturing fixed costs (maintenance costs, operating charges, plant overhead, local taxes and insurance) - Depreciation and corporate overhead costs * Raw materials consumption, products generation and labor requirements * Process block flow diagram and description of industrial site installations (production unit and infrastructure) This report was developed based essentially on the following reference(s): (1) "Fibers, 5. Synthetic Inorganic", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition; (2) US Patent 4999099, issued to Conoco in 2011; (3) Chung, D.D.L., Carbon Fiber Composites, 1994 Keywords: Carbon Fiber, Petroleum Pitch, Coal Tar Pitch, Mesophase Pitch

Characterization of Commercial Carbon Fiber from Standard PAN Precursors and Low-cost Carbon Fiber from Textile PAN Based Precursors

Characterization of Commercial Carbon Fiber from Standard PAN Precursors and Low-cost Carbon Fiber from Textile PAN Based Precursors PDF Author: Joshua David Crabtree
Publisher:
ISBN:
Category :
Languages : en
Pages : 0

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Book Description
There is tremendous need to integrate carbon fiber composites for light-weighting in the transportation sector, especially for automotive composites and in energy generation space associated with wind turbine manufacturing. Tensile properties of carbon fibers are fundamental to designing fiber reinforced polymers and carbon/carbon composites. Carbon fiber suppliers typically follow general guidelines prescribed in the relevant standards (ASTM D4018) to prepare resin reinforced carbon fiber tows for determining the tensile properties. In this study, the effect of manufacturing process associated with carbon fiber tows was evaluated using two methods involving manual tensioned strands or using automated spool method. Important effects associated with fiber spacing, cross-sectional morphology of the infused tows are reported in this study. Single fiber mechanical properties are determined to obtain relationship from multiple length scales and the role of interfacial behavior between the carbon fiber and resin system using single fiber fragmentation. These results, for the first time, revealed important relationships between single fiber, interface, and infused tow based mechanical properties. A new concept for deformation response of infused tows, limit stress, demonstrated a connection in the nonlinearity nature of tensile modulus seen for carbon fibers in single fiber state and in tow format. Limit stress showed good representation of the relative role of relationships (interfacial behavior, crack propagation, and stress transfer) from limit stress to failure stress. Three low-cost precursors, oxidized PAN, and carbon fiber, from the Carbon Fiber Technology Facility with differences in spin finish and/or tenacity are studied in detail through various stages of oxidative stabilization and carbonization to develop improved understanding of the precursor properties and final textile PAN based carbon fiber properties. A systematic approach consisting of DSC, TGA, FT-IR, XRD, single fiber testing, and infused tow testing were considered in evaluating the process-structure-tensile property relationship for the three precursors. The results identified the role of spin finish and tenacity on the performance of low-cost carbon fiber. This part of the research provides an important conclusion that the carbon fiber manufacturing process using textile PAN precursors is industrially robust and is not strongly dependent on precursor tenacity or surface finish.

Carbon Fibers, Third Edition,

Carbon Fibers, Third Edition, PDF Author: Jean-Baptiste Donnet
Publisher: CRC Press
ISBN: 9780824701727
Category : Technology & Engineering
Languages : en
Pages : 590

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Book Description
"Third Edition offers the latest information on the structural, surface, mechanical, electronic, thermal, and magnetic properties of carbon fibers as well as their manufacture and industrial applications from many of the world's most distinguished specialists in the field. "

Carbon Fiber Production from PAN - Cost Analysis - Carbon Fiber E11A

Carbon Fiber Production from PAN - Cost Analysis - Carbon Fiber E11A PDF Author: Intratec
Publisher: Intratec
ISBN:
Category : Business & Economics
Languages : en
Pages : 101

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Book Description
This report presents a cost analysis of Carbon Fiber production from polyacrylonitrile (PAN) fiber. In this process, PAN fiber is first stabilized. The stabilized PAN passes then through carbonization, surface treatment and sizing, before being winded. This report was developed based essentially on the following reference(s): (1) "Fibers, 5. Synthetic Inorganic", Ullmann's Encyclopedia of Industrial Chemistry, 7th edition (2) US Patent 8137810, issued to Toray in 2012; Keywords: Polyacrylonitrile, carbon fiber, acrylic fiber, PAN

Carbon Reinforcements and Carbon/Carbon Composites

Carbon Reinforcements and Carbon/Carbon Composites PDF Author: E. Fitzer
Publisher: Springer Science & Business Media
ISBN: 3642587453
Category : Technology & Engineering
Languages : en
Pages : 353

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Book Description
Advanced composite materials have been a major research focus for the past forty years. As a reinforcement for conventional materials including glass, ceramics and polymers, carbon has proved to be the most successful. Carbon gives these materials flexibility so that they may be produced in bulk form with a wide variety of properties. Whereas carbon/carbon composites are the most effective materials in extreme temperature conditions. Application ranges from brakes to missile nose cones. Carbon Reinforcements and Carbon/Carbon Composites gives the present state on this subject in comprehensive form, as well as projections for other "High Tech" materials and their application.

High-Performance and Specialty Fibers

High-Performance and Specialty Fibers PDF Author: Japan The Society of Fiber Science and Techno
Publisher: Springer
ISBN: 4431552030
Category : Technology & Engineering
Languages : en
Pages : 441

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Book Description
This book reviews the key technologies and characteristics of the modern man-made specialty fibers mainly developed in Japan. Since the production of many low-cost man-made fibers shifted to China and other Asian countries, Japanese companies have focused on production of high-quality, high-performance super fibers as well as highly functionalized fibers so-called ‘Shin-gosen’. ZylonTM and DyneemaTM manufactured by Toyobo, TechnoraTM produced by Teijin, and VectranTM developed by Kuraray are those examples of super fibers. Carbon fibers ToraycaTM from Toray have occupied the most advanced high-performance application area. Various types of polyester fibers having design-shaped cross-sections and special fiber morphologies and those showing specific physico-chemical properties have also been developed to acquire a high-value textile market of the world. This book describes how these high-tech fibers have been developed and what aspects are the most important in each fiber based on its structure-property relationship. Famous specialists both in industry and academia are responsible for the contents, explaining the design concepts and the special technologies for the production of these special fibers. For university teachers and students, this volume is an excellent textbook that elucidates the basic concepts of modern fibers. At the same time, researchers, both in academia and industry, will find a comprehensive overview of recent man-made fibers. This publication, presenting the most easily understandable general survey of specialty man-made fibers to date, is dedicated to the 70th-anniversary of the Society of Fiber Science and Technology, Japan.

Carbon Fiber

Carbon Fiber PDF Author: Vincent Kelly
Publisher:
ISBN: 9781856174305
Category : Carbon fibers
Languages : en
Pages : 512

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Book Description
Provides an account of the manufacturing processes for PAN, pitch and carbonized viscose rayon carbon fibres. This book includes a section on carbon fiber testing and characterization, followed by a section on textile conversion of carbon fibers and techniques for mixing carbon fiber and composite substrates.

Carbon Fiber

Carbon Fiber PDF Author: Pratima Bajpai
Publisher: Elsevier
ISBN: 012821905X
Category : Technology & Engineering
Languages : en
Pages : 246

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Book Description
Carbon Fiber, Second Edition, brings together available information on the production, properties, application and future of carbon fibers. This book will be of interest to those involved in the investigation of carbon fiber, carbon fiber manufacturing, and users. In addition, the recycling of carbon fiber reinforced polymers and the manufacturing of composites from recycled carbon fiber reinforced polymers are discussed. The book offers in-depth coverage on the production of carbon fiber and the global carbon fiber market, demand and major growth drivers. Carbon structures from biowaste, waste lignin and novel processes to obtain high purity lignin are presented, along with future directions. Provides thorough and in-depth coverage of carbon fiber production Presents the global carbon fiber market, demand and major growth drivers Covers carbon structures from biowaste and waste lignin Discusses novel process to obtain high purity lignin Includes discussions of future directions for the carbon fiber industry

Carbon-Carbon Composites

Carbon-Carbon Composites PDF Author: E. Savage
Publisher: Springer Science & Business Media
ISBN: 9401115869
Category : Technology & Engineering
Languages : en
Pages : 393

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Book Description
Carbon fibre reinforced carbon composites form a very specialized group of materials. They may be considered as a development of the family of carbon fibre reinforced polymer composites which are becoming ever more prevalent in modern engineering. Since the early 1960s a large number of so-called 'advanced materials' have appeared on the scene. Carbon~arbon is arguably the most successful of all these products finding many and varied applications. In the field of Formula 1 motor racing for example, the present levels of performance simply could not be achieved without the use of carbon-carbon brakes and clutches. Despite the materials' obvious assets, they have not, and will not, reach their full potential until their inherent problems of excessive production costs and oxidation resistance have been addressed properly. In this respect the 'carbon-carbon story', of much potential but only limited success, serves as a lesson to all those involved in materials research, development and application. In writing this book I have tried to set up a logical progression of what the materials are, how they are made, what their assets and deficiencies are, what they are used for and to what extent they are commercially exploited. Each specialized chapter may be considered in isolation or as part of a sequence, whereas the final chapter provides a summary of the principal concepts as well as a basic review of the economic situation past, present and, hopefully, future.