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Author: Yong-Cheng Ning
Publisher: John Wiley & Sons
ISBN: 0470828315
Category : Science
Languages : en
Pages : 426
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Book Description
Although there are a number of books in this field, most of them lack an introduction of comprehensive analysis of MS and IR spectra, and others do not provide up-to-date information like tandem MS. This book fills the gap. The merit of this book is that the author will not only introduce knowledge for analyzing nuclear magnetic resonance spectra including 1H spectra (Chapter 1), 13C spectra (Chapter 2) and 2D NMR spectra (Chapter 3), he also arms readers systemically with knowledge of Mass spectra (including EI MS spectra and MS spectra by using soft ionizations) (Chapter 4) and IR spectra (Chapter 5). In each chapter the author presents very practical application skills by providing various challenging examples. The last chapter (Chapter 6) provides the strategy, skills and methods on how to identify an unknown compound through a combination of spectra. Based on nearly 40 years researching and teaching experience, the author also proposes some original and creative ideas, which are very practical for spectral interpretation.
Author: Yong-Cheng Ning
Publisher: John Wiley & Sons
ISBN: 0470828315
Category : Science
Languages : en
Pages : 426
Get Book Here
Book Description
Although there are a number of books in this field, most of them lack an introduction of comprehensive analysis of MS and IR spectra, and others do not provide up-to-date information like tandem MS. This book fills the gap. The merit of this book is that the author will not only introduce knowledge for analyzing nuclear magnetic resonance spectra including 1H spectra (Chapter 1), 13C spectra (Chapter 2) and 2D NMR spectra (Chapter 3), he also arms readers systemically with knowledge of Mass spectra (including EI MS spectra and MS spectra by using soft ionizations) (Chapter 4) and IR spectra (Chapter 5). In each chapter the author presents very practical application skills by providing various challenging examples. The last chapter (Chapter 6) provides the strategy, skills and methods on how to identify an unknown compound through a combination of spectra. Based on nearly 40 years researching and teaching experience, the author also proposes some original and creative ideas, which are very practical for spectral interpretation.
Author: Ernö Pretsch
Publisher: John Wiley & Sons
ISBN: 9783527288267
Category : Science
Languages : en
Pages : 68
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Book Description
A unique advanced textbook on spectroscopy. This interactive tutorial presents text, software and data in a state-of-the-art introduction to the interpretation of 13C- and 1H-nuclear magnetic resonance, infrared, mass and UV/VIS spectra. Designed as a hands-on guide, the newcomer or student learns not only by reading but by experimenting, using the powerful software tools and data provided on the accompanying CD-ROM. The software, based on the outstanding SpecTool product, enables you to learn how to interpret molecular spectra correctly, rapidly and easily. Moreover, you can check your progress by working through the examples embedded in this self-study course that demonstrate how to identify an organic compound and to elucidate its structure. All the material and software presented are the essence of the two authors? longstanding teaching experience.
Author: Mynard Hamming
Publisher: Elsevier
ISBN: 0323143148
Category : Science
Languages : en
Pages : 709
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Book Description
Interpretation of Mass Spectra of Organic Compounds outlines the basic instrumentation, sample handling techniques, and procedures used in the interpretation of mass spectra of organic compounds. The fundamental concepts of ionization, fragmentation, and rearrangement of ions as found in mass spectra are covered in some detail, along with the rectangular array and interpretation maps. Computerization of mass spectral data is also discussed. This book consists of nine chapters and begins with a historical overview of mass spectrometry and a discussion on some important developments in the field, along with a summary of interpretation objectives and methods. The following chapters focus on instruments, ion sources, and detectors; recording of the mass spectrum and the instrumental and sample variables affecting the mass spectrum; sample introduction systems; and fragmentation reactions. Correlations as applied to interpretations are also considered, with emphasis on applications of the branching rule as well as beta-bond and alpha-bond cleavages. Example interpretations, calculations, data-processing procedures, and computer programs are included. This monograph is intended for organic chemists, biochemists, mass spectroscopists, technicians, managers, and others concerned with the whys and wherefores of mass spectrometry.
Author: David Whittaker
Publisher: Royal Society of Chemistry
ISBN: 1847551157
Category : Science
Languages : en
Pages : 272
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Book Description
Spectroscopic data undoubtedly provides a great deal of useful information about organic molecules. Competently deriving structural information from such data therefore, is a requisite skill for many undergraduates studying chemistry. Interpreting Organic Spectra covers the basic principles of spectroscopy in as non-mathematical a way as possible. It assumes no previous knowledge of spectroscopy and avoids excessive theory, approaching the topic as an exercise in pattern recognition. Hence the main focus of the book is in the provision of a variety of spectra for the student to interpret. Students are able to pace their progress by gaining confidence on the simpler spectra, and applying techniques learned to tackle more complex examples. As an introduction to the subject, it is ideal for A-level students as well as chemistry undergraduates and will prove to be a very useful reference tool for teachers and lecturers.
Author: Neil E. Jacobsen
Publisher: John Wiley & Sons
ISBN: 1119047145
Category : Science
Languages : en
Pages : 652
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Book Description
Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings
Author: Lal Dhar Singh Yadav
Publisher: Springer Science & Business Media
ISBN: 1402025750
Category : Science
Languages : en
Pages : 334
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Book Description
Organic Spectroscopy presents the derivation of structural information from UV, IR, Raman, 1H NMR, 13C NMR, Mass and ESR spectral data in such a way that stimulates interest of students and researchers alike. The application of spectroscopy for structure determination and analysis has seen phenomenal growth and is now an integral part of Organic Chemistry courses. This book provides: -A logical, comprehensive, lucid and accurate presentation, thus making it easy to understand even through self-study; -Theoretical aspects of spectral techniques necessary for the interpretation of spectra; -Salient features of instrumentation involved in spectroscopic methods; -Useful spectral data in the form of tables, charts and figures; -Examples of spectra to familiarize the reader; -Many varied problems to help build competence ad confidence; -A separate chapter on ‘spectroscopic solutions of structural problems’ to emphasize the utility of spectroscopy. Organic Spectroscopy is an invaluable reference for the interpretation of various spectra. It can be used as a basic text for undergraduate and postgraduate students of spectroscopy as well as a practical resource by research chemists. The book will be of interest to chemists and analysts in academia and industry, especially those engaged in the synthesis and analysis of organic compounds including drugs, drug intermediates, agrochemicals, polymers and dyes.
Author: Noël P.G. Roeges
Publisher: Wiley
ISBN: 9780471939986
Category : Science
Languages : en
Pages : 356
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Book Description
The accurate interpretation of infrared spectra of organic structures is an extremely important tool for the analytical chemist. Using up-to-date source material, this volume presents a compilation of the infrared absorption regions of ninety of the most important organic molecular fragments. This highly practical guide introduces the reader to a straightforward technique for determining all the fundamental vibrations of a molecular fragment. The set of normal vibrations and the infrared absorption regions of ninety molecular fragments are then discussed and tabulated. The discussion of each fragment is accompanied by a large number of references. A Guide to the Complete Interpretation of Infrared Spectra of Organic Structures offers the analytical chemist the possibility of a more profound interpretation of infrared spectra. In addition, it assumes only a basic knowledge of infrared spectra, and so will prove very useful for non-specialists who use infrared spectroscopy in analysis.
Author: Ernö Pretsch
Publisher: Springer Science & Business Media
ISBN: 3662224550
Category : Science
Languages : en
Pages : 325
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Book Description
Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.
Author: Antonio Randazzo
Publisher: Loghia Di Amoresano Claudia
ISBN: 9788895122403
Category : Medical
Languages : en
Pages : 344
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Book Description
This book is designed to provide undergraduate and graduate students with practical strategies, methods and explanations to interpret the NMR spectra of small organic molecules. In particular, it is organized in a way that basic 1H- and 13iNMR concepts are introduced and immediately applied in a number of problems, solved and discussed in a step-by-step fashion. It contains almost exclusively real NMR data and it describes how to interpret the chemical shift, intensity and splitting pattern of the proton and carbon NMR signals (Chapters 1-5), paying attention to the effects of the magnetically non-equivalent nuclei (Chapter 4). The role of the solvent is also explained (Chapter 6), and a description of the interpretation of the most common two-dimensional NMR experiments is reported in Chapter 7. Chapter 8 is dedicated to the strategy for structural elucidation, while Chapter 9 contains exclusively summary problems.
Author: David Watson Mathieson
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 192
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Book Description
Contains seminar sessions of a summer school in organic spectrocopy 1964, held under the aegis of the Royal Institute of Chemistry.
