Handbook of Derivatization Reactions for HPLC PDF Download
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Author: George Lunn
Publisher: Wiley-Interscience
ISBN: 9780471238881
Category : Science
Languages : en
Pages : 1832
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Book Description
Thousands of derivatization procedures for HPLC and CE-an essential tool for today's analytical chemist. This valuable reference offers fast and convenient access to derivatization reactions for both HPLC and capillary electrophoresis (CE). Covering a wide variety of compounds from pharmaceutical drugs and biological products to industrial contaminants, it is organized first by functional group and then by individual reagents. Techniques for each functional group are described in sufficient detail that the researcher can replicate procedures without reference to the original publications-saving hours of tedious library research. And because detailed procedures for the same reagent are listed together, it is easy to combine features of different methods and tailor them to fit specific individual requirements. Also available on CD-ROM, Handbook of Derivatization Reactions for HPLC contains fully abstracted and evaluated procedures from more than 1,900 papers, with descriptions of hundreds of reagents. A further 3,000 papers are referenced in bibliographies that are clearly annotated to help analysts identify those sources likely to be most useful. This important new resource will be welcomed by chemists working in pharmaceutical, biomedical, and environmental analysis. Also available on CD-ROM System requirements . . . IBM-compatible PC 486 or better and Windows(r) 3.0 or higher, or Macintosh 68030 processor and System 7 or higher * CD-ROM drive and 8 MB RAM minimum * 5 MB free hard disk space minimum, 30 MB recommended for full installation.
Author: George Lunn
Publisher: Wiley-Interscience
ISBN: 9780471238881
Category : Science
Languages : en
Pages : 1832
Get Book Here
Book Description
Thousands of derivatization procedures for HPLC and CE-an essential tool for today's analytical chemist. This valuable reference offers fast and convenient access to derivatization reactions for both HPLC and capillary electrophoresis (CE). Covering a wide variety of compounds from pharmaceutical drugs and biological products to industrial contaminants, it is organized first by functional group and then by individual reagents. Techniques for each functional group are described in sufficient detail that the researcher can replicate procedures without reference to the original publications-saving hours of tedious library research. And because detailed procedures for the same reagent are listed together, it is easy to combine features of different methods and tailor them to fit specific individual requirements. Also available on CD-ROM, Handbook of Derivatization Reactions for HPLC contains fully abstracted and evaluated procedures from more than 1,900 papers, with descriptions of hundreds of reagents. A further 3,000 papers are referenced in bibliographies that are clearly annotated to help analysts identify those sources likely to be most useful. This important new resource will be welcomed by chemists working in pharmaceutical, biomedical, and environmental analysis. Also available on CD-ROM System requirements . . . IBM-compatible PC 486 or better and Windows(r) 3.0 or higher, or Macintosh 68030 processor and System 7 or higher * CD-ROM drive and 8 MB RAM minimum * 5 MB free hard disk space minimum, 30 MB recommended for full installation.
Author: Daniel R. Knapp
Publisher: John Wiley & Sons
ISBN: 9780471034698
Category : Science
Languages : en
Pages : 772
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Book Description
Brings together practical information previously available only innumerous separate sources. Handbook of Analytical DerivationReactions begins with an overview of analytical derivatizationwith a section on apparatus. Describes analytical derivatizationmethods organized according to the sample to be derivatized.Discussion of methods includes derivative type, reagent, sampletype, reaction, and typical procedure with comments and referencesfor each.
Author: George Lunn
Publisher: John Wiley & Sons
ISBN: 0471711675
Category : Science
Languages : en
Pages : 743
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Book Description
An indispensable resource for busy researchers Your time is valuable-too valuable to spend hunting through the technical literature in search of the right HPLC assay techniques for your projects. With HPLC Methods for Recently Approved Pharmaceuticals, you'll quickly identify and replicate the ideal procedures for your project needs, without having to refer to original source publications. More of your time can then be spent in the lab, not the library. Covering the relevant world literature through 2003, this book picks up where Dr. Lunn's acclaimed HPLC Methods for Pharmaceutical Analysis left off. It arms you with established HPLC assay techniques for hundreds of newly approved drugs, as well as drugs for which assay methods were only recently developed. Combining detailed descriptions of procedures with specially annotated references, this practical handbook gives you: * HPLC methods for 390 commonly prescribed pharmaceutical compounds * Various procedures for each drug listed together-making it easy to mix and match for customized approaches * Methods for drugs in biological fluids and for bulk and formulated drugs * Chemical structures, molecular weights and formulas, and CAS Registry Numbers * Cross-references to The Merck Index * Retention times of other drugs that can be assayed using the same methods
Author: Henryk Lamparczyk
Publisher: CRC Press
ISBN: 9780849330087
Category : Science
Languages : en
Pages : 178
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Book Description
CRC Handbook of Analysis and Characterization of Steroids provides a comprehensive review of chromatographic methods used in steroid analysis, including gas chromatography, high-performance liquid chromatography, thin-layer chromatography, and supercritical fluid chromatography. The book discusses principles, applications, and apparatus required for the chromatographic analysis of steroids. Classes of steroids covered include anabolic-androgenic steroids, bile acids, cardenolides, ecdysteroids, estrogens, corticoids, sterols, and Vitamin D. A chapter is devoted to each class of steroids and features nomenclature, structures, and descriptions for sample preparations and chromatographic data. CRC Handbook of Analysis and Characterization of Steroids provides essential information and techniques for professional analytical chemists in academia, clinical chemists in pharmaceutical and food quality control labs, and researchers and technicians in forensic and drug analysis facilities.
Author: Danilo Corradini
Publisher: CRC Press
ISBN: 9780203909751
Category : Science
Languages : en
Pages : 1018
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Book Description
Delineating its usage in separation, purification and detection processes across a variety of disciplines, from industry to applied research, this work discusses the principles, techniques and instrumentation involving HPLC within a detailed framework. Over 100 tables present previously scattered experimental data.
Author: S. Blackburn
Publisher: CRC Press
ISBN: 9780849330667
Category : Science
Languages : en
Pages : 444
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Book Description
An in-depth analysis of chromatography literature and procedures since 1981 is presented in this publication. Featured is a compre-hensive range of tables relating to the chromatographic separation and determination of amino acids, amines, and their derivatives. Methods of sample preparation and derivatization and methods of detection are described. Included are techniques for the liquid and gas chro-matographic separation of free amino acids and their derivatives, including o-phthalaldehyde, dansyl, and phenylthiolaydantoin deriva-tives. The separation of amino acid enantiomers is also described. This book will be invaluable to chemists, biochemists, and analysts involved in the separation and determination of amino acids or amines and their derivatives.
Author: S. Blackburn
Publisher: CRC Press
ISBN: 1000443337
Category : Science
Languages : en
Pages : 427
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Book Description
An in-depth analysis of chromatography literature and procedures since 1981 is presented in this publication. Featured is a compre-hensive range of tables relating to the chromatographic separation and determination of amino acids, amines, and their derivatives. Methods of sample preparation and derivatization and methods of detection are described. Included are techniques for the liquid and gas chro-matographic separation of free amino acids and their derivatives, including o-phthalaldehyde, dansyl, and phenylthiolaydantoin deriva-tives. The separation of amino acid enantiomers is also described. This book will be invaluable to chemists, biochemists, and analysts involved in the separation and determination of amino acids or amines and their derivatives.
Author: Haleem J. Issaq
Publisher: CRC Press
ISBN: 9780824705763
Category : Science
Languages : en
Pages : 782
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Book Description
A Century of Separation Science presents an extensive overview of the critical developments in separation science since 1900, covering recent advances in chromatography, electrophoresis, field-flow fractionation, countercurrent chromatography, and supercritical fluid chromatography for high-speed and high-throughput analysis.
Author: Serban C. Moldoveanu
Publisher: Elsevier
ISBN: 0323898203
Category : Science
Languages : en
Pages : 698
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Book Description
Modern Sample Preparation for Chromatography, Second Edition explains the principles of sample preparation for chromatographic analysis. A variety of procedures are applied to make real-world samples amenable for chromatographic analysis and to improve results. This book's authors discuss each procedure's advantages, disadvantages and their applicability to different types of samples, along with their fit for different types of chromatographic analysis. The book contains numerous literature references and examples of sample preparation for different matrices and new sections on green approaches in sample preparation, progress in automation of sample preparation, non-conventional solvents for LLE (ionic liquids, deep eutectic mixtures, and others), and more. - Presents numerous techniques applied for sample preparation for chromatographic analysis - Provides an up-to-date source of information regarding the progress made in sample preparation for chromatography - Describes examples for specific types of matrices, providing a guide for choosing the appropriate sample preparation method for a given analysis
Author: Ibolya Molnár-Perl
Publisher: Elsevier
ISBN: 0080458459
Category : Science
Languages : en
Pages : 669
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Book Description
Quantitation of Amino Acids and Amines by Chromatography: Methods and Protocols is intended to serve as a ready-to-use guide for the identification and quantification of amino acids and amines in various matrices, providing an overview on the theory and protocol of available methods. It presents chromatograms with exact elution programs enabling visual analysis and compares the advantages-disadvantages of various chromatographic techniques. In accordance with the chronological order of the development of chromatographic methods, different techniques are discussed: The possibilities of gas chromatography (GC), followed by those of the high performance liquid chromatography (HPLC) and the most recent techniques capillary electrophoresis (CE), capillary, electrochromatography (CEC).The characteristics of the given chromatographic procedure, relating to the topic in question, are classified according to the preliminary preparation/derivatization process(es), which means the simple methods, suitable for the analysis of the selected compound(s) in natural form, are followed by various derivatization proposals. Detailed protocols provide the reader with guidance in beginning tasks and on how to improve current methods. This book appeals to a wide audience and is recommended for those looking towards the wider reaches of identification and quantification of amino acids and amines.* Provides a systematic, and comprehensive summary of chromatographic techniques and derivatization processes* Compares advantages/disadvantages of various chromatographic techniques* Readers can undertake practical tasks using detailed protocols given in the book
