Gas Chromatography of Organometallic Compounds

Gas Chromatography of Organometallic Compounds PDF Author: T. R. Crompton
Publisher: Springer Science & Business Media
ISBN: 1468442260
Category : Science
Languages : en
Pages : 597

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Book Description
Since its introduction into the armoury of the analytical chemist approximately two decades ago the technique of gas chroma tography has found very extensive applications in the analysis of most types of organic compounds. One of the few remaining limitations of the technique when applied to such compounds, namely the analysis of very highly boiling and or thermally unstable substances, has been overcome in many instances by the introduction of techniques such as silation for the conversion of sample components to lower boiling or more stable substances which can be gas chromatographed at reasonably low temperatures. All of this has been extensively dealt with in many books published during recent years dealing with the theory and practice of applying gas chromatography to the analysis and preparative separation of organic compounds. In parallel with these developments there has occurred, particu larly over the past decade, a growing interest in the application of gas chromatography to the analysis of organometallic compounds. Indeed, for many types of organometallic compounds, gas chromatography is the analytical method of choice particularly, as so often happens, when the sample is a mixture. To the author's knowledge no complete review exists of the published work in this very interesting new field; a situation it is hoped the present volume will rectify.

Gas Chromatography of Organometallic Compounds

Gas Chromatography of Organometallic Compounds PDF Author: T. R. Crompton
Publisher: Springer Science & Business Media
ISBN: 1468442260
Category : Science
Languages : en
Pages : 597

Get Book Here

Book Description
Since its introduction into the armoury of the analytical chemist approximately two decades ago the technique of gas chroma tography has found very extensive applications in the analysis of most types of organic compounds. One of the few remaining limitations of the technique when applied to such compounds, namely the analysis of very highly boiling and or thermally unstable substances, has been overcome in many instances by the introduction of techniques such as silation for the conversion of sample components to lower boiling or more stable substances which can be gas chromatographed at reasonably low temperatures. All of this has been extensively dealt with in many books published during recent years dealing with the theory and practice of applying gas chromatography to the analysis and preparative separation of organic compounds. In parallel with these developments there has occurred, particu larly over the past decade, a growing interest in the application of gas chromatography to the analysis of organometallic compounds. Indeed, for many types of organometallic compounds, gas chromatography is the analytical method of choice particularly, as so often happens, when the sample is a mixture. To the author's knowledge no complete review exists of the published work in this very interesting new field; a situation it is hoped the present volume will rectify.

Gas Chromatography of Organometallic Compounds

Gas Chromatography of Organometallic Compounds PDF Author: 3Island Press
Publisher:
ISBN: 9781468442274
Category :
Languages : en
Pages : 600

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Book Description


Gas Chromatography of Organometallic Compounds

Gas Chromatography of Organometallic Compounds PDF Author: TR. CROMPTON
Publisher:
ISBN:
Category :
Languages : en
Pages : 0

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Book Description


Advanced Gas Chromatography

Advanced Gas Chromatography PDF Author: Mustafa Ali Mohd
Publisher: BoD – Books on Demand
ISBN: 9535102982
Category : Science
Languages : en
Pages : 474

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Book Description
Progress in agricultural, biomedical and industrial applications' is a compilation of recent advances and developments in gas chromatography and its applications. The chapters cover various aspects of applications ranging from basic biological, biomedical applications to industrial applications. Book chapters analyze new developments in chromatographic columns, microextraction techniques, derivatisation techniques and pyrolysis techniques. The book also includes several aspects of basic chromatography techniques and is suitable for both young and advanced chromatographers. It includes some new developments in chromatography such as multidimensional chromatography, inverse chromatography and some discussions on two-dimensional chromatography. The topics covered include analysis of volatiles, toxicants, indoor air, petroleum hydrocarbons, organometallic compounds and natural products. The chapters were written by experts from various fields and clearly assisted by simple diagrams and tables. This book is highly recommended for chemists as well as non-chemists working in gas chromatography.

Columns for Gas Chromatography

Columns for Gas Chromatography PDF Author: Eugene F. Barry
Publisher: John Wiley & Sons
ISBN: 0470114177
Category : Science
Languages : en
Pages : 315

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Book Description
Choosing the right column is key in Gas Chromatography Gas Chromatography (GC) is the most widely used method for separating and analyzing a wide variety of organic compounds and gases. There have been many recent advancements in both packed column and capillary column GC. With numerous options and considerations, selecting the right column can be complicated. This resource provides essential guidance for scientists and technicians, including: Methods of choosing both capillary and packed columns Selection of dimensions (column length, I.D., film thickness, etc.) and type of column Guidelines for proper connections of the column to the injector and detector United States Pharmacopeia and National Formulary chromatographic methods ASTM, EPA, NIOSH, and OSHA column selection specifications Information on the advantages of computer assistance in GC and multidimensional GC Comprehensive information on column oven temperature control Columns for Gas Chromatography: Performance and Selection is a hands-on reference for scientists and technicians using GC.

Gas Chromatography

Gas Chromatography PDF Author: Peter Kusch
Publisher: BoD – Books on Demand
ISBN: 1838818650
Category : Science
Languages : en
Pages : 144

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Book Description
Gas chromatography (GC) is one of the most important types of chromatography used in analytical chemistry for separating and analyzing chemical organic compounds. Today, gas chromatography is one of the most widespread investigation methods of instrumental analysis. This technique is used in the laboratories of chemical, petrochemical, and pharmaceutical industries, in research institutes, and also in clinical, environmental, and food and beverage analysis. This book is the outcome of contributions by experts in the field of gas chromatography and includes a short history of gas chromatography, an overview of derivatization methods and sample preparation techniques, a comprehensive study on pyrazole mass spectrometric fragmentation, and a GC/MS/MS method for the determination and quantification of pesticide residues in grape samples.

Gas Chromatography in Inorganics and Organometallics

Gas Chromatography in Inorganics and Organometallics PDF Author: Georges Guiochon
Publisher:
ISBN:
Category : Chemistry, Inorganic
Languages : en
Pages : 354

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Book Description


Comprehensive Organometallic Analysis

Comprehensive Organometallic Analysis PDF Author: T.R. Crompton
Publisher: Springer Science & Business Media
ISBN: 1461594987
Category : Science
Languages : en
Pages : 907

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Book Description
It is now some sixteen years since the author's first series of books on the analysis of organometallic compounds. Many developments in the subject have occurred since that time and a new book on the subject is now overdue. The present book aims to provide a comprehensive review of the subject. It covers not only all aspects of the analysis of organometallic compounds but also contains two additional chapters, dealing with environmental analysis and the use of chelates of metals in the determination of very low concentrations of organic metals. Whilst reviewing the literature for the present book, it was observed that whereas papers published prior to 1973 dealt almost exclusively with various forms of analysis, a high proportion of those published during the past ten years were concerned with the application of proven or newly developed methods to the determination of organometallic compounds in environmental samples such as water, air, soil, river and ocean sediments, fish life and biota samples. An increasing range of elements including mercury, lead, arsenic, tin, antimony, selenium and manganese are now being found in organically bound forms in the environment, some resulting from pollution, others formed in nature by bacterial processes. As many of these substances have appreciable implications to human and animal health and the ecosystem as a whole, it was considered that it would be timely to include a separate chapter in the book devoted entirely to this subject.

Practical Gas Chromatography

Practical Gas Chromatography PDF Author: Katja Dettmer-Wilde
Publisher: Springer
ISBN: 3642546404
Category : Science
Languages : en
Pages : 904

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Book Description
Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.

Occurrence and Analysis of Organometallic Compounds in the Environment

Occurrence and Analysis of Organometallic Compounds in the Environment PDF Author: T. R. Crompton
Publisher: John Wiley & Sons
ISBN: 9780471976073
Category : Science
Languages : en
Pages : 254

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Book Description
Unter besonderer Berücksichtigung der wichtigsten Schadstoffe - Quecksilber, Blei, Zinn und Arsen - werden hier alle Aspekte des Vorkommens, der Toxizität und der Analytik organometallischer Verbindungen in Umweltproben systematisch erläutert. Ausführlich wird auch auf Phänomene wie die Bioakkumulation und die Verteilung der Xenobiotika im Ökosystem eingegangen. (02/98)