Development of Instrumentation Incorporating Solid State Sensors for Measurement of Oxygen Partial Pressure PDF Download
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Author: Mohieddine Benammar
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Languages : en
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Electronic instrumentation was developed for the measurement of the oxygen partial pressure, P1 (in a sample gas using fully-sealed zirconia pump-gauge oxygen sensors operated in an AC mode. These sensors, operated typically at 700?C, consisted of two discs of zirconia with porous platinum electrodes on each face separated by a gold seal and enclosing a small internal volume. One disc was operated as a pump enabling oxygen to be electrochemically transferred into and out of the enclosed volume; the other disc operated as a gauge, the Nernst EMF across the electrodes providing a measure of the ratio of the internal to the external oxygen partial pressure. By careful design of the circuitry it was possible to measure the oxygen partial pressure, P, without the need for a separate reference gas supply. Subsequently, a novel "tracking" mode of operation was proposed and implemented in which leakage effects generally associated with sealed pump-gauge devices were minimised: the sensor was operated in a feedback control-loop in order to adjust automatically the mean internal reference oxygen partial pressure, P0, so as to maintain the ratio (Px/P0) close to unity. The signal-to-noise ratio was markedly improved by using gauge EMFs with high amplitudes which inevitably display a distorted sinusoid due to the logarithmic term in the Nernst equation. Surprisingly, mathematical analysis predicted that the linearity of the output of the instrument using phase-sensitive detection should not be affected by the deviation from a sinusoid and this was confirmed experimentally: signal processing was practically implemented using simple analogue electronics. As anticipated there was a strong influence of sensor temperature on the output of the instrument: consequently, methods for temperature compensation were proposed and shown to be feasible with minimum hardware. The theory of Operation of leaky pump-gauge was also developed which indicated that a physical leak in the sensor should cause a phase shift and amplitude change in the sensor output. Experimental results were, in general, in agreement with the theory demonstrating the influences of the geometry and dimensions of the leak and of the operating frequency. Importantly, the theory predicted that, when operated in the AC mode, devices with major leakage may still be used for oxygen partial pressure measurement: again this was confirmed by experiment and the additional benefit of a concomitant substantial simplification of the electronic circuitry also realised. Interestingly an unexpected but small influence of oxygen concentration on the phase shift was observed: this requires additional study.
Author: Mohieddine Benammar
Publisher:
ISBN:
Category :
Languages : en
Pages :
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Book Description
Electronic instrumentation was developed for the measurement of the oxygen partial pressure, P1 (in a sample gas using fully-sealed zirconia pump-gauge oxygen sensors operated in an AC mode. These sensors, operated typically at 700?C, consisted of two discs of zirconia with porous platinum electrodes on each face separated by a gold seal and enclosing a small internal volume. One disc was operated as a pump enabling oxygen to be electrochemically transferred into and out of the enclosed volume; the other disc operated as a gauge, the Nernst EMF across the electrodes providing a measure of the ratio of the internal to the external oxygen partial pressure. By careful design of the circuitry it was possible to measure the oxygen partial pressure, P, without the need for a separate reference gas supply. Subsequently, a novel "tracking" mode of operation was proposed and implemented in which leakage effects generally associated with sealed pump-gauge devices were minimised: the sensor was operated in a feedback control-loop in order to adjust automatically the mean internal reference oxygen partial pressure, P0, so as to maintain the ratio (Px/P0) close to unity. The signal-to-noise ratio was markedly improved by using gauge EMFs with high amplitudes which inevitably display a distorted sinusoid due to the logarithmic term in the Nernst equation. Surprisingly, mathematical analysis predicted that the linearity of the output of the instrument using phase-sensitive detection should not be affected by the deviation from a sinusoid and this was confirmed experimentally: signal processing was practically implemented using simple analogue electronics. As anticipated there was a strong influence of sensor temperature on the output of the instrument: consequently, methods for temperature compensation were proposed and shown to be feasible with minimum hardware. The theory of Operation of leaky pump-gauge was also developed which indicated that a physical leak in the sensor should cause a phase shift and amplitude change in the sensor output. Experimental results were, in general, in agreement with the theory demonstrating the influences of the geometry and dimensions of the leak and of the operating frequency. Importantly, the theory predicted that, when operated in the AC mode, devices with major leakage may still be used for oxygen partial pressure measurement: again this was confirmed by experiment and the additional benefit of a concomitant substantial simplification of the electronic circuitry also realised. Interestingly an unexpected but small influence of oxygen concentration on the phase shift was observed: this requires additional study.
Author: Mohieddine Benammar
Publisher:
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Category :
Languages : en
Pages :
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Author: Donald L. Wise
Publisher: CRC Press
ISBN: 1482276933
Category : Medical
Languages : en
Pages : 823
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This reference text consists of contributed chapters by specialists directly carrying out research and development in this emerging field which joins advanced microelectronics with modern biotechnology. Chapters present novel biotechnology-based microelectronic instruments, such as those used for de
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Languages : en
Pages : 618
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Author: Carl A. Burtis
Publisher: Elsevier Health Sciences
ISBN: 1455759422
Category : Medical
Languages : en
Pages : 2259
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As the definitive reference for clinical chemistry, Tietz Textbook of Clinical Chemistry and Molecular Diagnostics, 5th Edition offers the most current and authoritative guidance on selecting, performing, and evaluating results of new and established laboratory tests. Up-to-date encyclopedic coverage details everything you need to know, including: analytical criteria for the medical usefulness of laboratory procedures; new approaches for establishing reference ranges; variables that affect tests and results; the impact of modern analytical tools on lab management and costs; and applications of statistical methods. In addition to updated content throughout, this two-color edition also features a new chapter on hemostasis and the latest advances in molecular diagnostics. Section on Molecular Diagnostics and Genetics contains nine expanded chapters that focus on emerging issues and techniques, written by experts in field, including Y.M. Dennis Lo, Rossa W.K. Chiu, Carl Wittwer, Noriko Kusukawa, Cindy Vnencak-Jones, Thomas Williams, Victor Weedn, Malek Kamoun, Howard Baum, Angela Caliendo, Aaron Bossler, Gwendolyn McMillin, and Kojo S.J. Elenitoba-Johnson. Highly-respected author team includes three editors who are well known in the clinical chemistry world. Reference values in the appendix give you one location for comparing and evaluating test results. NEW! Two-color design throughout highlights important features, illustrations, and content for a quick reference. NEW! Chapter on hemostasis provides you with all the information you need to accurately conduct this type of clinical testing. NEW! Six associate editors lend even more expertise and insight to the reference. NEW! Reorganized chapters ensure that only the most current information is included.
Author: Alexander P. Demchenko
Publisher: Springer Nature
ISBN: 3031190890
Category : Medical
Languages : en
Pages : 772
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Fluorescence is the most popular technique in chemical and biological sensing because of its ultimate sensitivity, high temporal and spatial resolution and versatility that enables imaging within the living cells. It develops rapidly in the directions of constructing new molecular recognition units, new fluorescence reporters and in improving sensitivity of response up to detection of single molecules. Its application areas range from control of industrial processes to environment monitoring and clinical diagnostics. This book provides systematic knowledge of basic principles in design of fluorescence sensing and imaging techniques together with critical analysis of recent developments. Being a guide for students and young researchers, it also addresses professionals involved in active basic and applied research. Making a strong link between education, research and product development, this book discusses prospects for future progress.
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Category : Aeronautics
Languages : en
Pages : 568
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Category : Dissertations, Academic
Languages : en
Pages : 526
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Theses on any subject submitted by the academic libraries in the UK and Ireland.
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Category : Automatic control
Languages : en
Pages : 392
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Category : Physics
Languages : en
Pages : 1248
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