Analyse multi-classes et multi-résidus de pesticides dans les matrices alimentaires végétales

Analyse multi-classes et multi-résidus de pesticides dans les matrices alimentaires végétales PDF Author: Céline Jackiewicz
Publisher:
ISBN:
Category :
Languages : fr
Pages : 166

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Multiresidue Methods for the Analysis of Pesticide Residues in Food

Multiresidue Methods for the Analysis of Pesticide Residues in Food PDF Author: Horacio Heinzen
Publisher: CRC Press
ISBN: 1351644637
Category : Science
Languages : en
Pages : 531

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Book Description
In the last decades the public concern on the pesticide residues content in foods have been steadily rising. The global development of food trade implies that aliments from everywhere in the world can reach the consumer`s table. Therefore, the identification of agricultural practices that employ different pesticides combinations and application rates to protect produce must be characterized, as they left residues that could be noxious to human health. However, the possible number of pesticides (and its metabolites of toxicological relevance) to be found in a specific commodity is almost 1500, and the time needed to analyze them one by one, makes this analytical strategy a unrealistic task. To overcome this problem, the concept of Multi Residue Methods (MRM) for the analysis of pesticide traces have been developed. The advent of new and highly sensitive instrumentation, based in hyphenatedchromatographic systems to coupled mass analyzers (XC (MS/MS) or MSn) permitted simultaneously the identification and the determination of up to hundreds of pesticide residues in a single chromatographic run. Multiresidue Methods for the Analysis of Pesticide Residues in Food presents the analytical procedures developed in the literature, as well as those currently employed in the most advanced laboratories that perform routinely Pesticide Residue Analysis in foods. In addition to these points, the regulations, guidelines and recommendations from the most important regulatory agencies of the world on the topic will be commented and contrasted.

Analysis of Pesticides in Food and Environmental Samples

Analysis of Pesticides in Food and Environmental Samples PDF Author: Jose L. Tadeo
Publisher: CRC Press
ISBN: 1420007750
Category : Science
Languages : en
Pages : 382

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Book Description
Developing safety regulations for pesticides used around the world—in excess of 2.5 million tons annually—requires reliable analytical methods for assessing their impact in food and in the environment. Analysis of Pesticides in Food and Environmental Samples presents the most effective techniques for analyzing pesticide residues and other chemical contaminants in foods as well as in soil, water, and air. Renowned Scientists Report New Data and Advances in the Field The book introduces sample preparation, extraction, and analytical methods specific to each sample type, including foods from vegetal and animal origin. Other chapters discuss important aspects of quality assurance and the applicability of hyphenated analytical techniques. In addition to a practical chapter on the use of biosensors and immunoassays for monitoring and gathering exposure data, the book addresses regulatory aspects and presents current data on the levels of pesticides found in food and environmental matrices. Latest Methods Help Scientists Develop Safer, More Effective Pesticides Analysis of Pesticides in Food and Environmental Samples enables scientists to measure and predict the behavior and toxicity of pesticides with a higher degree of accuracy. The methodologies and insight in this timely work will contribute to the development of more effective, less toxic pesticides as well as better safety regulations.

Analyse des pesticides dans l'eau de surface, l'eau potable et les produits de consommation par chromatographie liquide couplée à la spectrométrie de masse

Analyse des pesticides dans l'eau de surface, l'eau potable et les produits de consommation par chromatographie liquide couplée à la spectrométrie de masse PDF Author: Juan Manuel Montiel León
Publisher:
ISBN:
Category :
Languages : fr
Pages :

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L'utilisation intensive de certains pesticides et leur relative persistance vont de pair avec la présence de résidus dans l'eau de surface et l'eau potable mais aussi dans les produits agricoles disponibles pour les consommateurs, y compris les denrées alimentaires. À l'heure actuelle, les effets des pesticides sur la vie aquatique et d'autres organismes non ciblés sont relativement bien connus, et la possibilité des effets sur l'être humain fait débat. Des normes de qualité ont été proposées pour l'eau, que ce soit des critères pour l'eau potable ou des critères de protection de la vie aquatique pour l'eau de surface. Des limites maximales de résidus (MRL) de pesticides ont également été établies pour certains produits, notamment les fruits et légumes. Un des défis pour les chercheurs est la mise en œuvre de nouvelles méthodes analytiques sensibles et robustes pour la quantification ultra-trace de ces composés, afin de déterminer si les différents échantillons sont conformes aux directives ou aux MRL. L'analyse des pesticides modérément polaires dans des matrices complexes repose tout d'abord sur la méthode d'extraction. Plusieurs options sont disponibles, telles que l'extraction liquide-liquide ou en phase solide (SPE, Solid Phase Extraction) pour les matrices aqueuses, ou encore dSPE de type QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) pour les matrices solides. Actuellement, la chromatographie en phase liquide couplée à la spectrométrie de masse en tandem représente un choix pertinent pour les analyses ultra-traces, mais sa mise en œuvre peut présenter certains défis. Dans ce contexte, les principaux objectifs de ce travail de recherche sont les suivants : i) proposer des méthodes analytiques rapides, sensibles et robustes pour déterminer des pesticides multi-classes aux niveaux d'exposition que l'on retrouve dans différentes matrices comme l'eau potable, les denrées alimentaires et l'urine comme matrice biologique, et ii) évaluer le lien entre les sources de contamination des divers pesticides et leur mobilité afin de documenter la distribution spatiale et temporelle dans l'eau de surface et l'eau potable au Québec. Pour les échantillons aqueux, une méthode SPE en ligne entièrement automatisée couplée à la chromatographie liquide haute performance et spectrométrie de masse en tandem a été développée. La méthode proposée est rapide (8 min par échantillon) avec des limites de détection comprises entre 0.1 et 5 ng L-1 pour les pesticides de la famille des néonicotinoïdes et l'atrazine. Pour les produits alimentaires tels que les fruits et légumes, l'optimisation d'une méthode de type QuEChERS a été réalisée. La méthode permet d'atteindre des niveaux de détection entre 0.05 ng g-1 et 2 ng g-1 pour une gamme de 22 pesticides couvrant 7 classes différentes, incluant les organophosphorés, les carbamates, les néonicotinoïdes et les triazines, entre autres. La robustesse des diverses méthodes a été démontrée par des expériences de contrôle qualité inter- et intra-journaliers afin de garantir l'exactitude, la précision et l'absence d'effets matriciels pour de longues séquences d'analyse. Les méthodes validées ont été appliquées à des échantillons réels, y compris des échantillons d'eau du robinet couvrant 52 villes de la province du Québec (Canada), 68 échantillons d'eau de surface (fleuve Saint-Laurent et tributaires), et 133 échantillons de laitue, pomme, raisin et tomates achetés sur les marchés locaux. Les résultats indiquent une forte occurrence de l'atrazine, la thiaméthoxame, la clothianidine et l'imidaclopride dans les échantillons d'eau et les quatre produits alimentaires.

Bioactive Molecules in Food

Bioactive Molecules in Food PDF Author: Jean-Michel Mérillon
Publisher: Springer Nature
ISBN: 3319780301
Category : Technology & Engineering
Languages : en
Pages : 2353

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Book Description
This reference work provides comprehensive information about the bioactive molecules presented in our daily food and their effect on the physical and mental state of our body. Although the concept of functional food is new, the consumption of selected food to attain a specific effect existed already in ancient civilizations, namely of China and India. Consumers are now more attentive to food quality, safety and health benefits, and the food industry is led to develop processed- and packaged-food, particularly in terms of calories, quality, nutritional value and bioactive molecules. This book covers the entire range of bioactive molecules presented in daily food, such as carbohydrates, proteins, lipids, isoflavonoids, carotenoids, vitamin C, polyphenols, bioactive molecules presented in wine, beer and cider. Concepts like French paradox, Mediterranean diet, healthy diet of eating fruits and vegetables, vegan and vegetarian diet, functional foods are described with suitable case studies. Readers will also discover a very timely compilation of methods for bioactive molecules analysis. Written by highly renowned scientists of the field, this reference work appeals to a wide readership, from graduate students, scholars, researchers in the field of botany, agriculture, pharmacy, biotechnology and food industry to those involved in manufacturing, processing and marketing of value-added food products.

Multi-scale Sustainability Evaluation

Multi-scale Sustainability Evaluation PDF Author: Santiago López-Ridaura
Publisher:
ISBN:
Category : Electronic books
Languages : en
Pages : 220

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Advances in Solid State Fermentation

Advances in Solid State Fermentation PDF Author: S. Roussos
Publisher: Springer Science & Business Media
ISBN: 9401706611
Category : Technology & Engineering
Languages : en
Pages : 641

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Book Description
G.HAINNAUX Departement Milieu et Activites Agricoles, Centre ORSTOM, 911 Avenue d' Agropolis, B.P. 5045, 34032 Montpellier Cedex , France. Solid state fermentation, popularly abbreviated as SSF, is currently investigated by many groups throughout the world. The study of this technique was largely neglected in the past in European and Western countries and there is now a high demand for SSF, meaning in food, environment, agricultural, phannaceutical and many other biotechnological applications. It gives me satisfaction to note that the importance of this technique was realised at my department way back in 1975 since then, our team has put concentrated efforts on developing this technique. xvii Foreword Advances in Solid State Fermentation Foreword M. PUYGRENIER Agropolis Valorisation, Avenue d' Agropolis, 34394 Montpellier Cedex 5, France. On the name of the Scientific Community, I would like to express the wish that this International Symposium on SSF should be successful. Solid State Fermentation is part of biotechnology research. It consists on seeding solid culture medium with bacteria or fungi (filamentous or higher) and on producing, in this medium (solid components and exudates) metabolites and high value products. In fact, this process is very old. In older industries such the food and agricultural, this technique has been extensively used. An example of this is the production of pork sausages and Roquefort cheese. Pharmaceutical industry could make extensive use of SSF in the production of secondary metabolites of many kinds and development in this direction is soon expected.

Hydrogen Cyanide and Cyanides

Hydrogen Cyanide and Cyanides PDF Author:
Publisher:
ISBN: 9789241530613
Category : Cyanides
Languages : en
Pages : 67

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Fungi and Food Spoilage

Fungi and Food Spoilage PDF Author: John I. Pitt
Publisher: Springer Science & Business Media
ISBN: 1461563917
Category : Technology & Engineering
Languages : en
Pages : 599

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Book Description
This book is designed as a laboratory guide for the food microbiologist, to assist in the isolation and identification of common food-borne fungi. We emphasise the fungi which cause food spoilage, but also devote space to the fungi commonly encountered in foods at harvest, and in the food factory. As far as possible, we have kept the text simple, although the need for clarity in the descriptions has necessitated the use of some specialised mycological terms. The identification keys have been designed for use by microbiologists with little or no prior knowledge of mycology. For identification to genus level, they are based primarily on the cultural and physiological characteristics of fungi grown under a standardised set of conditions. The microscopic features of the various fungi become more important when identifying isolates at the species level. Nearly all of the species treated have been illustrated with colony photographs, together with photomicrographs or line drawings. The photomicrographs were taken using a Zeiss WL microscope fitted with Nomarski interference contrast optics. We are indebted to Mr W. Rushton and Ms L. Burton, who printed the many hundreds of photographs used to make up the figures in this book. We also wish to express out appreciation to Dr D.L. Hawksworth, Dr A.H.S.

Life Cycle Assessment in the Agri-food Sector

Life Cycle Assessment in the Agri-food Sector PDF Author: Bruno Notarnicola
Publisher: Springer
ISBN: 3319119400
Category : Technology & Engineering
Languages : en
Pages : 408

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Book Description
The book presents an overview of the International practices and state-of-the-art of LCA studies in the agri-food sector, both in terms of adopted methodologies and application to particular products; the final purpose is to characterise and put order within the methodological issues connected to some important agri-food products (wine, olive oil, cereals and derived products, meat and fruit) and also defining practical guidelines for the implementation of LCAs in this particular sector. The first chapter entails an overview of the application of LCA to the food sector, the role of the different actors of the food supply chain and the methodological issues at a general level. The other chapters, each with a particular reference to the main foods of the five sectors under study, have a common structure which entails the review of LCA case studies of such agri-food products, the methodological issues, the ways with which they have been faced and the suggestion of practical guidelines.