Distillation: Equipment and Processes

Distillation: Equipment and Processes PDF Author: Andrzej Gorak
Publisher: Academic Press
ISBN: 0123868793
Category : Science
Languages : en
Pages : 373

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Book Description
Distillation: Equipment and Processes—winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers—is a single source of authoritative information on all aspects of the theory and practice of modern distillation, suitable for advanced students and professionals working in a laboratory, industrial plants, or a managerial capacity. It addresses the most important and current research on industrial distillation, including all steps in process design (feasibility study, modeling, and experimental validation), together with operation and control aspects. This volume features an extra focus on distillation equipment and processes. - Winner of the 2015 PROSE Award in Chemistry & Physics from the Association of American Publishers - Practical information on the newest development written by recognized experts - Coverage of a huge range of laboratory and industrial distillation approaches - Extensive references for each chapter facilitates further study

Distillation Tray Fundamentals

Distillation Tray Fundamentals PDF Author: M. J. Lockett
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 264

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Book Description
This book contains an in-depth treatment on distillation tray hydrodynamics and efficiency, with an emphasis on sieve and valve trays. Topics covered by the author include froth, foam and spray, dispersion height, pressure drop, flooding and weeping. Graduate students and research workers in chemical engineering will find it useful as well as chemical and process engineers in industry concerned with distillation and absorption.

Tray Efficiencies in Distillation Columns

Tray Efficiencies in Distillation Columns PDF Author: American Institute of Chemical Engineers. Research Committee
Publisher:
ISBN:
Category : Distillation
Languages : en
Pages : 152

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Book Description


Tray Distillation Columns

Tray Distillation Columns PDF Author: American Institute of Chemical Engineers
Publisher:
ISBN:
Category :
Languages : en
Pages : 26

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Book Description


Distillation Operation

Distillation Operation PDF Author: Henry Z. Kister
Publisher: McGraw Hill Professional
ISBN: 9780070349100
Category : Technology & Engineering
Languages : en
Pages : 754

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Book Description
Discussing distillation, this book gives readers guidelines for operation, troubleshooting and control. It offers a compendium of Do's and Don'ts, good practices, and guidelines for trouble-free design; operation and troubleshooting for inlets and outlets; avoiding tray damage; installation; commissioning and startup techniques; and more.

Distillation Design

Distillation Design PDF Author: Henry Z. Kister
Publisher: McGraw-Hill Companies
ISBN:
Category : Science
Languages : en
Pages : 750

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Book Description
Providing coverage of design principles for distillation processes, this text contains a presentation of process and equipment design procedures. It also highlights limitations of some design methods, and offers guidance on how to overcome them.

Distillation Engineering

Distillation Engineering PDF Author: Reinhard Billet
Publisher:
ISBN:
Category : Cooking
Languages : en
Pages : 544

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Book Description
Partial Table of Contents I. The Thermal Separation of Liquids II. Thermodynamics of Mixtures 1. Definitions and Relationships A. Separability of a Liquid Mixture B. Partial Pressures in Vapor Mixtures C. Evaporation of Liquid Mixtures 2. Types of Mixtures A. Ideal Binary Mixtures B. Nonideal Binary Mixtures C. Ideal Multicomponent Mixtures D. Nonideal Multicomponent Mixtures III. Continuous Rectifiers 1. Mode of Operations 2. Operating Lines A. Enrichment Line B. The Stripping Line 3. Stepwise Separation in Rectifiers A. Theoretical Plates for Separation of Binaries B. The Reflux Ratio in the Separation of Binaries C. Multicomponent Mixtures 4. Column Diameter and Column Throughput 5. Heat Requirements IV. The Batch Still 1. Operation 2. Operating Line and Separation Steps 3. Column Diameter, Column Throughput, and Heat Requirements 4. Time for Separation and Related Variables at Constant Product Concentration A. Molar Vapor Load Constant in Time B. Heat Requirement Constant in Time 5. Separation Time for Variable Heating Area V. The Semicontinuous Still 1. Operation 2. Finding the Operating Lines, the Separation Steps, the Column Load, the Column: Size, and the Heat Demand VI. Engineering Data, Optimization of Costs, and Selection of Column Internals 1. General A. Packing Types B. Plates and Trays 2. Designs and Functions A. Packed Towers B. Plate Columns 3. Evaluation of Rectifying Columns and Best Mode of Operation A. Evaluating and Calculations, Separating Effect, Pressure Loss, Load, Specific Column Volume, and Specific Column Cost B. Numerical Evaluation for Packed Towers C. Quantitative Evaluation for Plate-Type Columns D. Packed Columns versus Tray Columns-Operational Features and Cost E. Special Designs for Vacuum Operation 4. Tests of Full-Size Tower Internals VII. Optimum Separation 1. Optimization of Simple Columns A. The Theory and Its Application B. Quantitative Evaluation 2. Optimization of Multiple Columns A. Duplex Columns: Number of Theoretical Steps, Reflux Ratios, and Vapor Loads B. Vapor Loads of Multiple Columns Subdivided Because of Limited Height C. Optimizing Duplex Rectifiers for Minimum Pressure Loss 3. Optimum Operation of Combined Columns of Different Types Under Special Consideration A. Parallel Arrangement B. Series Arrangement 4. Specialized Operations A. Specialized Hookups and their Calculation B. Rectification in Straight Stripping Columns C. Rectification in Straight Enriching Columns D. Direct Heating of Columns E. Saving Heat in Rectification VIII. Detail Planning of Separating Columns 1. General Viewpoints in the Selection of Column Types 2. Packed Columns Columns 3. Special Packings 4. Plate-Type Columns 5. Pressure Losses in Rectification Columns IX. Partial Distillation 1. Separation of Liquids by Continuous Partial Distillation 2. Separation of Liquids by Discontinuous Partial Distillation X. Partial Condensation 1. Partial Condensation in Dephlegmators 2. Partial Countercurrent Direct Condensation in Columns XI. Laboratory Columns and Pilot Plants 1. Distillation Columns with Miniature Size Packing 2. Transferring Data Gained From Semi-industrial Units to Full-Scale XII. Distillation in Fine and High Vacuum 1. Molecular Distillation 2. Thin-Film Distillation 3. Mechanism of Separation XIII. Components of a Separation Plant 1. Internal Components 2. Heat Exchangers 3. Pumps 4. Measuring and Controls XIV. Use of Computers XV. Distillation and Environmental Protection XVI. Outlook Bibliography Symbols and Units Glossary Index

Distillation Tray Fundamentals

Distillation Tray Fundamentals PDF Author: M. J. Lockett
Publisher: Cambridge University Press
ISBN: 9780521105873
Category : Technology & Engineering
Languages : en
Pages : 0

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Book Description
First published in 1986, this book contains an in-depth treatment on distillation tray hydrodynamics and efficiency, with an emphasis on sieve and valve trays. As distillation lies at the heart of the petroleum and chemical industries, so at the heart of most distillation columns are the trays used to effect the separation. Topics covered by the author include froth, foam and spray, dispersion height, pressure drop, flooding and weeping. Procedures for predicting tray efficiency are outlined including the effects of entrainment, weeping and flow maldistribution. Methods for multicomponent efficiency are also covered with examples. Although distillation tray hydrodynamics is probably one of the most well-researched areas of chemical engineering, few books cover the subject other than on an elementary level. The present volume will be used by graduate students and research workers in chemical engineering, and by chemical and process engineers in industry concerned with distillation and absorption.

Practical Distillation Control

Practical Distillation Control PDF Author: W.L. Luyben
Publisher: Springer Science & Business Media
ISBN: 1475702779
Category : Science
Languages : en
Pages : 547

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Book Description
Distillation column control has been the the "Lehigh inquisition" and survived! So it subject of many, many papers over the last has been tested by the fire of both actual half century. Several books have been de review by a hard-nosed plant experience and voted to various aspects of the subject. The group of practically oriented skeptics. technology is quite extensive and diffuse. In selecting the authors and the topics, There are also many conflicting opinions the emphasis has been on keeping the ma about some of the important questions. terial practical and useful, so some subjects We hope that the collection under one that are currently of mathematical and the cover of contributions from many of the oretical interest, but have not been demon leading authorities in the field of distillation strated to have practical importance, have control will help to consolidate, unify, and not been included. clarify some of this vast technology. The The book is divided about half and half contributing authors of this book represent between methodology and specific applica tion examples. Chapters 3 through 14 dis both industrial and academic perspectives, and their cumulative experience in the area cuss techniques and methods that have of distillation control adds up to over 400 proven themselves to be useful tools in at tacking distillation control problems.

Distillation Troubleshooting

Distillation Troubleshooting PDF Author: Henry Z. Kister
Publisher: John Wiley & Sons
ISBN: 1118216350
Category : Technology & Engineering
Languages : en
Pages : 758

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Book Description
THE FIRST BOOK OF ITS KIND ON DISTILLATION TECHNOLOGY The last half-century of research on distillation has tremendously improved our understanding and design of industrial distillation equipment and systems. High-speed computers have taken over the design, control, and operation of towers. Invention and innovation in tower internals have greatly enhanced tower capacity and efficiency. With all these advances, one would expect the failure rate in distillation towers to be on the decline. In fact, the opposite is the case: the tower failure rate is on the rise and accelerating. Distillation Troubleshooting collects invaluable hands-on experiences acquired in dealing with distillation and absorption malfunctions, making them readily accessible for those engaged in solving today's problems and avoiding tomorrow's. The first book of its kind on the distillation industry, the practical lessons it offers are a must for those seeking the elusive path to trouble-free distillation. Distillation Troubleshooting covers over 1,200 case histories of problems, diagnoses, solutions, and key lessons. Coverage includes: * Successful and unsuccessful struggles with plugging, fouling, and coking * Histories and prevention of tray, packing, and internals damage * Lessons taught by incidents and accidents during shutdowns, commissioning, and abnormal operation * Troubleshooting distillation simulations to match the real world * Making packing liquid distributors work * Plant bottlenecks from intermediate draws, chimney trays, and feed points * Histories of and key lessons from explosions and fires in distillation towers * Prevention of flaws that impair reboiler and condenser performance * Destabilization of tower control systems and how to correct it * Discoveries from shutdown inspections * Suppression of foam and accumulation incidents A unique resource for improving the foremost industrial separation process, Distillation Troubleshooting transforms decades of hands-on experiences into a handy reference for professionals and students involved in the operation, design, study, improvement, and management of large-scale distillation.