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Author: Ralph Lloyd Shriner
Publisher:
ISBN:
Category : Chemistry, Organic
Languages : en
Pages : 334
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Book Description
Author: Ralph Lloyd Shriner
Publisher:
ISBN:
Category : Chemistry, Organic
Languages : en
Pages : 334
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Book Description
Author: Christine K. F. Hermann
Publisher: John Wiley & Sons
ISBN: 1119799686
Category : Science
Languages : en
Pages : 709
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Book Description
The Systematic Identification of Organic Compounds A comprehensive introduction to the identification of unknown organic compounds Identifying unknown compounds is one of the most important parts of the study of chemistry. From basic characteristics such as melting and/or boiling point to more complex data generated through cutting-edge techniques, the range of possible methods for identifying unknown organic compounds is substantial. The utility of a research reference which compiles known techniques and characteristics of possible compounds is clear. The Systematic Identification of Organic Compounds provides such a reference, designed to teach a hands-on approach in the chemistry lab. It takes readers step-by-step through the process of identifying an unknown compound and elucidating its structure from infrared, nuclear magnetic resonance, and mass spectra in addition to solubility characteristics, melting point, boiling point, and classification tests. The result is an essential overview for advanced chemistry students looking to understand this exciting area of laboratory work. Readers of the ninth edition of The Systematic Identification of Organic Compounds will also find: A detailed chapter on safety, personal protection equipment, chemical storage, safety data sheets, and other safety concerns New NMR, IR, and mass spectra with detailed explanations on interpretation Questions at the end of each chapter designed to facilitate and reinforce progression, keyed to a companion website for instructors Tables of known compounds including data relevant for identification Companion website with structural problems from experimental data for students to practice how to reason and solve The Systematic Identification of Organic Compounds is a useful reference for advanced undergraduates and graduate students studying organic chemistry, organic spectroscopy, and related subjects.
Author: Ralph Lloyd Shriner
Publisher: John Wiley & Sons
ISBN:
Category : Science
Languages : en
Pages : 626
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Book Description
Step-by-step instructions on identifying organic compounds. The steps described include elemental analysis, solubility, infrared spectra, nuclear magnetic resonance spectra, mass spectra, classification tests, and preparation of a derivative. Most directions for experiments are described in a micro or mini scale and clean up directions are given at the end of each procedure. Emphasizes the systematic approach to identifying unknowns. -- Offers a review of spectroscopy. -- Discusses infrared, nuclear magnetic resonance, and mass spectroscopy and includes examples of spectra. -- Discusses chromatography, distillations, and the separation of mixtures.
Author: Yong-Cheng Ning
Publisher: Wiley-VCH
ISBN:
Category : Science
Languages : en
Pages : 480
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Book Description
Clearly structured, easy to read and optimal to understand, this extensive compendium fills the gap between textbooks devoted to either spectra interpretation or basic physical principles. The original Chinese editions have already sold over 18,500 copies, and the material is taken from the latest literature from around the world, plus technical information provided by the manufacturers of spectroscopic instruments. Alongside basic methods, Professor Ning presents up-to-date developments in NMR, MS, IR and Raman spectroscopy, such as pulsed-field gradient technique, LC-NMR, and DOSY. He stresses the application of spectroscopic methods, interpreting them in great detail and depth since most of the selected spectra may be applied to practical work, as well as summarizing the rules for their interpretation. He also incorporates his original ideas, including a comparison of the common points in different spectroscopic techniques. This monograph features a unique structure, a typical example being the discussion of 2D NMR starting from pulse sequence units, which construct various pulse sequences for related 2D NMR. A complete chapter deals with the determination of configurations and conformations of organic compounds and even biological molecules from the viewpoint of spectroscopic methodologies, while one whole section is dedicated to the interpretation of mass spectra produced by soft ionization techniques. The principles of mass analyzers, especially the ion trap, are discussed in great depth, together with a concise summary of the MS fragmentation and rearrangement of common compounds, allowing readers to easily predict related mass spectrometric reactions. All the three kinds of library retrieval of mass spectra are presented in detail, together with recent developments in molecular vibration spectroscopy. The whole is rounded off with several appendices, including a subject index for rapid reference. With a foreword by the Nobel prizewinner, Richard R. Ernst.
Author: Ralph L. Shriner
Publisher: John Wiley & Sons
ISBN: 0471215031
Category : Science
Languages : en
Pages : 735
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Book Description
First written in 1935, Shriner remains a classic text in the field. Coauthor Christine Hermann has introduced modern methods and topics and completely updated the illustration and photo program. The book is ideal for the Advanced Organic Lab and for Spectroscopy courses.
Author: Louis Frederick Fieser
Publisher:
ISBN:
Category : Chemistry, Organic
Languages : en
Pages : 369
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Book Description
Author: W.L.F. Armarego
Publisher: Elsevier
ISBN: 0080515460
Category : Technology & Engineering
Languages : en
Pages : 627
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Book Description
Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.* Complete update of this valuable, well-known reference* Provides purification procedures of commercially available chemicals and biochemicals* Includes an extremely useful compilation of ionisation constants
Author: Robert Milton Silverstein
Publisher:
ISBN: 9780471429135
Category : Organic compounds
Languages : en
Pages : 0
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Book Description
Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book: Uses a problem-solving approach with extensive reference charts and tables. Offers an extensive set of real-data problems offers a challenge to the practicing chemist
Author: Mr. Sushant Sudhir Pande
Publisher: Trinity Publishing House, Satara
ISBN: 8196977948
Category : Medical
Languages : en
Pages : 124
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Book Description
We are pleased to put forth the "Laboratory Manual of Pharmaceutical Organic Chemistry I." This manual, prepared according to the PCI B. Pharm course regulations 2014, is divided into three sections: systematic qualitative analysis, preparation of suitable solid derivatives and construction of molecular models. The methods of all the experiments are drawn from the latest editions of official books of pharmaceutical organic chemistry and research papers, ensuring the inclusion of the latest advancements in methodologies or apparatus. This manual is designed for outcome-based education. Each experiment follows a uniform format, with sections for practical significance, practical outcomes (PrOs), mapping with course outcomes, theory, resources used, procedure, precautions, observations, results, conclusion, references, and synopsis questions. Each experiment offers an opportunity for students to perform practical work, developing proficiency in effectively managing equipment, handling glassware, chemicals, reagents, and writing analytical reports. In addition, the questions at the end of the experiments help to enhance students' knowledge, benefiting them as they pursue higher studies. During the laboratory period, you will have to multiple tasks while performing the experiment. It is essential to document your actions and observations thoroughly as you proceed. Always plan your work ahead, considering what you are doing, why you are doing it, what is happening, and what conclusions you can draw from your experiment. We acknowledge the help and cooperation of various individuals in bringing out this manual. We are highly indebted to the authors of the books and articles mentioned in the references, which were a major source of information for this manual. We also thank the publishers, designers, and printers who worked hard to publish this manual in a timely manner. We hope that this manual will be helpful to students in understanding concepts, principles, and performing procedures. We wish you all the best!
Author: United States. Environmental Protection Agency. Library Systems Branch
Publisher:
ISBN:
Category : Environmental protection
Languages : en
Pages : 702
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Book Description
