The Separation and Determination of Polynuclear Aromatic Hydrocarbons by High-performance Liquid Chromatography

The Separation and Determination of Polynuclear Aromatic Hydrocarbons by High-performance Liquid Chromatography PDF Author: British Carbonization Research Association
Publisher:
ISBN:
Category : Hydrocarbons
Languages : en
Pages :

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The Separation and Determination of Polynuclear Aromatic Hydrocarbons by High-performance Liquid Chromatography

The Separation and Determination of Polynuclear Aromatic Hydrocarbons by High-performance Liquid Chromatography PDF Author: British Carbonization Research Association
Publisher:
ISBN:
Category : Hydrocarbons
Languages : en
Pages :

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The Separation and Determination of Polynuclear Aromatic Hydrocarbons by High-performance Liquid Chromatography

The Separation and Determination of Polynuclear Aromatic Hydrocarbons by High-performance Liquid Chromatography PDF Author: British Carbonization Research Association
Publisher:
ISBN:
Category :
Languages : en
Pages : 19

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Handbook of Chromatography

Handbook of Chromatography PDF Author: Hamir S. Rathore
Publisher: CRC Press
ISBN: 9780849330056
Category : Science
Languages : en
Pages : 442

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Book Description
Handbook of Chromatography provides a detailed description of significant aspects of polycyclic aromatic hydrocarbons (PAHs). The sources, occurrence, nomenclature, and carcinogenicity of PAHs are covered, and a comprehensive record of data of sample preparation, detection, separation, determination, and characterization of PAHs by liquid chromatography is presented. The book also summarizes extraction and enrichment procedures (e.g., Soxhlet extraction, ultrasonic extraction, liquid-liquid partitioning); presents data from paper chromatography, thin-layer chromatography, high-performance thin-layer chromatography, and electrophoresis of PAHs; and discusses the methodology and applications of extrography in analyzing complex aromatic materials. Handbook of Chromatography also provides a PAHs book directory and a list of suppliers of PAHs and HPLC columns. The volume will be an essential reference for analytical chemists, environmental toxicologists, organic chemists, biomedical specialists, and biotechnicians.

High Pressure Liquid Chromatography for the Measurement of Polynuclear Aromatic Hydrocarbons in Water

High Pressure Liquid Chromatography for the Measurement of Polynuclear Aromatic Hydrocarbons in Water PDF Author: R. Kent Sorrell
Publisher:
ISBN:
Category : Liquid chromatography
Languages : en
Pages : 44

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Method Development and Monitoring of Polynuclear Aromatic Hydrocarbons in Selected U.S. Waters

Method Development and Monitoring of Polynuclear Aromatic Hydrocarbons in Selected U.S. Waters PDF Author: Jitendra Saxena
Publisher:
ISBN:
Category : Water
Languages : en
Pages : 100

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Polycyclic Aromatic Hydrocarbons in Work Atmospheres

Polycyclic Aromatic Hydrocarbons in Work Atmospheres PDF Author: Alf Bjorseth
Publisher: CRC Press
ISBN: 1351092219
Category : Technology & Engineering
Languages : en
Pages : 190

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Book Description
This book deals with the sources, distribution, analytical methods, and monitoring of Polycyclic aromatic hydrocarbons (PAH) in the occupational environment. It is hoped that this book will make a contribution to understanding the formation and determination of PAH in work atmosphere and that it will make a particular contribution to occupational health projects. Much of the information given in this book has been generating in studies carried out in cooperation with the Norwegian aluminium industry.

A Developmental Investigation of Separation and Analysis of Molecular Mass 302 Da Polyaromatic Hydrocarbons Using High Performance Liquid Chromatography and Chiral Stationary Phase

A Developmental Investigation of Separation and Analysis of Molecular Mass 302 Da Polyaromatic Hydrocarbons Using High Performance Liquid Chromatography and Chiral Stationary Phase PDF Author: James Janesko
Publisher:
ISBN:
Category :
Languages : en
Pages : 0

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Book Description
High molecular weight -- polycyclic aromatic hydrocarbons (HMW-PAH) are often found where air, water, and soil are subject to higher levels of industrial pollutants. These molecules are environmentally concerning due to their carcinogenic, mutagenic, and tumorigenic propensities. Furthermore, the isomers in this family are challenging to separate due to similar retention parameters, spectroscopic fingerprints, and mass spectral patterns.

Analytical Chemistry of Polycyclic Aromatic Compounds

Analytical Chemistry of Polycyclic Aromatic Compounds PDF Author: Milton Lee
Publisher: Elsevier
ISBN: 0323149030
Category : Science
Languages : en
Pages : 475

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Book Description
Analytical Chemistry of Polycyclic Aromatic Compounds focuses on the chemical and physical properties of the polycyclic aromatic compounds, critically evaluating various chromatographic and spectroscopic methods. This book discusses how gas chromatography and high-performance liquid chromatography can be both competitive and complementary analytical methods. Ancillary techniques of both are emphasized for the structural elucidation of individual polycyclic aromatic compounds in complex mixtures. The merits of spectroscopic methods in both structural work and quantitation are also described. This text likewise provides background information concerning the chemistry, occurrence, and toxicology of polycyclic aromatic compounds, including the isolation of polycyclic aromatic compounds from a wide variety of materials and matrices. This publication is recommended to scientists involved with the study of polycyclic aromatic compounds, analysts who need to acquire routine data, and individuals charged with formulating environmental policies and drafting regulations.

Separation and Determination of Polycyclic Aromatic Hydrocarbons and Nitrogen Heterocycles Pertaining to Coal Gasification, Tar Sands, Shale Oil, Coal Liquids, and Related Samples. Final Technical Progress Report, January 1978-December 1979

Separation and Determination of Polycyclic Aromatic Hydrocarbons and Nitrogen Heterocycles Pertaining to Coal Gasification, Tar Sands, Shale Oil, Coal Liquids, and Related Samples. Final Technical Progress Report, January 1978-December 1979 PDF Author:
Publisher:
ISBN:
Category :
Languages : en
Pages :

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A method was developed for identifying and determining benzo(a)pyrene in a filtered retort water sample from an in situ oil shale process by employing liquid-liquid extraction, dry-column chromatography, thin-layer chromatography and fluorescence spectrometry. The accuracy and precision of the method were good, and the limit of detection was approximately 0.08 ppB. Irreproducible results were obtained with unfiltered retort water samples. Programmed multiple development was used to a limited extent in the separation of polycyclic aromatic hydrocarbons from a shale oil sample. However, results indicated that this separation technique should be investigated further in the separation of polycyclic aromatic hydrocarbons. Benzo(a)pyrene was determined in several shale oil samples by methods developed previously. Polycyclic aromatic hydrocarbons were characterized in several shale oil samples using open-column, dry-column and thin-layer chromatography as separation steps. Visible fluorescence from the separated components on chromatoplates was measured directly to obtain fluorescence profiles of the components on the chromatoplates. Several comparisons were made among the shale oil samples as to the relative amounts of 6-, 5-, 4- and 3-ring polycyclic aromatic hydrocarbons. The theoretical and practical analytical aspects of the room temperature phosphorescence of nitrogen heterocycles were investigated. Intense room temperature phosphorescence was obtained from several nitrogen heterocycles when these compounds were absorbed on silica gel. Theoretical explanations were given for the intense phosphorescence. Benzo(f)quinoline and phenanthridine were separated from a shale oil sample by open-column and high performance liquid chromatography, and then identified by room temperature phosphorescence.

Handbook of Polycyclic Aromatic Hydrocarbons

Handbook of Polycyclic Aromatic Hydrocarbons PDF Author: Bjorseth
Publisher: CRC Press
ISBN: 9780824774424
Category : Science
Languages : en
Pages : 434

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Book Description
This volume concerns sources of polycyclic aromatic hydrocarbons (PAH), their emission factors, and relative importance. It deals with exposure, uptake, metabolism, and detection of PAH in the human body. The volume contains an update of information in environmental and biochemical studies of PAH.