Author:
Publisher:
ISBN: 9789201269195
Category : Sample preparation (Chemistry)
Languages : en
Pages :

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Author: International Atomic Energy Agency
Publisher: IAEA Tecdoc Series No. 1783
ISBN: 9789201004161
Category : Technology & Engineering
Languages : en
Pages : 0

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Book Description
Nuclear and related techniques can help develop climate-smart agricultural practices by optimizing water and nutrient use efficiency, assessing organic carbon sequestration in soil, and assisting in the evaluation of soil erosion control measures. Knowledge on the behaviour of radioactive materials in soil, water and foodstuffs is also essential in enhancing nuclear emergency preparedness and response. Appropriate sampling and sample preparation are the first steps to ensure the quality and effective use of the measurements and this publication provides comprehensive detail on the necessary steps.

Author: International Atomic Energy Agency
Publisher:
ISBN: 9789201050182
Category : Technology & Engineering
Languages : en
Pages : 70

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Book Description
Stable isotope techniques can help identify the sources of water pollution associated with agricultural activities. Knowing the origin of nutrients or contaminants is essential to improve agricultural practices. To ensure the quality of stable isotope analysis, appropriate sampling and sample preparation are crucial. This publication presents methods for surface water sampling and sample processing through micro-diffusion and bacterial denitrification combined with laser spectroscopy. Information on such methods is often described in a very summarized and non-comprehensive way without proper illustration of every step. This publication aims to bridge this gap for scientists, technicians and students. It presents a selection of standard operating procedures providing guidance in water sampling and sample preparation that are mandatory when conducting reliable isotope analysis on water.

Author: Dercon, G., Lee Zhi Yi, A., Fesenko, S., Heng, L.
Publisher: Food & Agriculture Org.
ISBN: 925135975X
Category : Technology & Engineering
Languages : en
Pages : 136

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Book Description
The evaluation of radioactive releases to the environment is important for the support of sustainable development of agriculture, due to the potential for released radioactivity to enter food chain. The impact of radionuclides on the food chains are normally assessed by means of measurements of radioactivity in environmental samples, which include soils, feedstuffs, foodstuffs, and water. Sampling of agricultural soils and food, as well as measurement of various radionuclides for radioactivity requires efficient, cheap, effective and easily implemented techniques. The lack of such techniques may prevent the development of national infrastructures in providing the required level of food safety. This document provides the standard operating procedures (SOPs) for sampling and measurements of radionuclides in agriculture. It also includes an overview of the techniques relevant for agricultural soil and crops. Supplementary techniques such as the assessment of radiocaesium mobility in soils are also presented. The document is intended for individuals and authorities dealing with sampling and measurement of radionuclides in agricultural environments, and answered the many request for assistance from the IAEA Members in radionuclide measurements in agricultural soils and food items.

Author: International Atomic Energy Agency
Publisher:
ISBN: 9789201020192
Category : Technology & Engineering
Languages : en
Pages : 48

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Book Description
Stable isotope techniques can help improve soil management and crop nutrition. To ensure the quality of stable isotope analysis through isotope ratio mass spectrometry (IRMS), appropriate sample preparation is crucial. This publication presents methods for proper plant and soil sample processing for IRMS analysis. The information on such methods is often described in a summarized and non-comprehensive way without illustration of every step. This publication fills this gap and presents a selection of standard operating procedures and provides highly detailed guidance on sample preparation that will support practitioners in conducting reliable isotope analysis on plant and soil materials.

Author: Joseph Adu-Gyamfi
Publisher: Springer Nature
ISBN: 3030974979
Category : Agriculture
Languages : en
Pages : 67

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Book Description
This open access book distinguished itself from other publications by offering step-by-step instructions on how to extract, purify, provide modifications, and major issues to be encountered during the process. For the 18OP method to progress, further fundamental research as well as field and laboratory studies need to be conducted for a better understanding of P cycling in the environment. Chapter 1 outlines the background and examples of 18Op studies in sediments, soils, fresh water, mineral fertilizers, and plants. Chapters 2 and 3 examine the stepwise extraction and purification protocols including reagents, equipment and consumables and preparations for analyses. Chapter 4 examines some of the challenges and modifications during the purification process. Chapter 5 discusses planning and designing of a study using 18Op, external quality assurance with an example of an inter-laboratory study. Chapter 6 outlines the conclusions, future trends, and opportunities, the scaling out of the method from laboratory to field studies. It is expected that the 18OP would be extensively applied in research geared to understand phosphorus dynamics in different agro-environments. .

Author: Josep M. Bayona
Publisher: Academic Press
ISBN: 0123813743
Category : Science
Languages : en
Pages : 2998

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Book Description
Comprehensive Sampling and Sample Preparation is a complete treatment of the theory and methodology of sampling in all physical phases and the theory of sample preparation for all major extraction techniques. It is the perfect starting point for researchers and students to design and implement their experiments and support those experiments with quality-reviewed background information. In its four volumes, fundamentals of sampling and sample preparation are reinforced through broad and detailed sections dealing with Biological and Medical, Environmental and Forensic, and Food and Beverage applications. The contributions are organized to reflect the way in which analytical chemists approach a problem. It is intended for a broad audience of analytical chemists, both educators and practitioners of the art and can assist in the preparation of courses as well in the selection of sampling and sample preparation techniques to address the challenges at hand. Above all, it is designed to be helpful in learning more about these topics, as well as to encourage an interest in sampling and sample preparation by outlining the present practice of the technology and by indicating research opportunities. Sampling and Sample preparation is a large and well-defined field in Analytical Chemistry, relevant for many application areas such as medicine, environmental science, biochemistry, pharmacology, geology, and food science. This work covers all these aspects and will be extremely useful to researchers and students, who can use it as a starting point to design and implement their experiments and for quality-reviewed background information There are limited resources that Educators can use to effectively teach the fundamental aspects of modern sample preparation technology. Comprehensive Sampling and Sample Preparation addresses this need, but focuses on the common principles of new developments in extraction technologies rather than the differences between techniques thus facilitating a more thorough understanding Provides a complete overview of the field. Not only will help to save time, it will also help to make correct assessments and avoid costly mistakes in sampling in the process Sample and sample preparation are integral parts of the analytical process but are often less considered and sometimes even completely disregarded in the available literature. To fill this gap, leading scientists have contributed 130 chapters, organized in 4 volumes, covering all modern aspects of sampling and liquid, solid phase and membrane extractions, as well as the challenges associated with different types of matrices in relevant application areas

Author:
Publisher: IAEA
ISBN:
Category : Business & Economics
Languages : en
Pages : 224

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Book Description
The IAEA has compiled this overview of current applications of nuclear analytical techniques (NATs). The contributions included in this book describe a variety of nuclear techniques and applications, such as those in the fields of environment and health, industrial processes, non-destructive testing, forensic and archaeological investigations, cosmochemistry and method validation. The techniques covered range from classical instrumental neutron activation analysis (INAA), its radiochemical derivative RNAA, in-beam methods such as prompt y neutron activation analysis (PGNAA) and accelerator mass spectrometry (AMS), to X ray fluorescence (XRF) and proton induced X ray emission (PIXE) spectroscopy. Isotopic techniques to investigate element behaviour in biology and medicine, and also to validate other non-nuclear analytical techniques, are described. Destructive and non-destructiveapproaches are presented, along with their use to investigate very small and very large samples, archaeological samples and extraterrestrial samples. Several nuclear analytical applications in industry are described that have considerable socioeconomic impact wherever they can be implemented.

Author: International Atomic Energy Agency
Publisher:
ISBN: 9789201189103
Category : Environmental sampling
Languages : en
Pages : 146

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Book Description
The 1990s saw significant developments in the global non-proliferation landscape, resulting in a new period of safeguards development. The current publication, which is the second revision and update of IAEA/NVS/1, is intended to give a full and balanced description of the safeguards techniques and equipment used for nuclear material accountancy, containment and surveillance measures, environmental sampling, and data security. New features include a section on new and novel technologies. As new verification measures continue to be developed, the material in this book will be reviewed periodically and updated versions issued.

Author: Zoltan Mester
Publisher: Elsevier
ISBN: 0080545483
Category : Science
Languages : en
Pages : 1339

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Book Description
Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation.- First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.