Specimen Handling, Preparation, and Treatments in Surface Characterization

Specimen Handling, Preparation, and Treatments in Surface Characterization PDF Author: Alvin W. Czanderna
Publisher: Springer Science & Business Media
ISBN: 0306469138
Category : Science
Languages : en
Pages : 302

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Book Description
With the development in the 1960s of ultrahigh vacuum equipment and techniques and electron, X-ray, and ion beam techniques to determine the structure and composition of interfaces, activities in the field of surface science grew nearly exponentially. Today surface science impacts all major fields of study from physical to biological sciences, from physics to chemistry, and all engineering disciplines. The materials and phenomena characterized by surface science range from se- conductors, where the impact of surface science has been critical to progress, to metals and ceramics, where selected contributions have been important, to bio- terials, where contributions are just beginning to impact the field, to textiles, where the impact has been marginal. With such a range of fields and applications, questions about sample selection, preparation, treatment, and handling are difficult to cover completely in one review article or one chapter. Therefore, the editors of this book have assembled a range of experts with experience in the major fields impacted by surface characterization. It is the only book which treats the subject of sample handling, preparation, and treatment for surface characterization. It is full of tricks, cautions, and handy tips to make the laboratory scientist’s life easier. With respect to organization of the book, the topics range from discussion of vacuum to discussion of biological, organic, elemental or compound samples, to samples prepared ex situ or in situ to the vacuum, to deposition ofthin films. Generic considerations of sample preparation are also given.

Specimen Handling, Preparation, and Treatments in Surface Characterization

Specimen Handling, Preparation, and Treatments in Surface Characterization PDF Author: Alvin W. Czanderna
Publisher: Springer Science & Business Media
ISBN: 0306469138
Category : Science
Languages : en
Pages : 302

Get Book

Book Description
With the development in the 1960s of ultrahigh vacuum equipment and techniques and electron, X-ray, and ion beam techniques to determine the structure and composition of interfaces, activities in the field of surface science grew nearly exponentially. Today surface science impacts all major fields of study from physical to biological sciences, from physics to chemistry, and all engineering disciplines. The materials and phenomena characterized by surface science range from se- conductors, where the impact of surface science has been critical to progress, to metals and ceramics, where selected contributions have been important, to bio- terials, where contributions are just beginning to impact the field, to textiles, where the impact has been marginal. With such a range of fields and applications, questions about sample selection, preparation, treatment, and handling are difficult to cover completely in one review article or one chapter. Therefore, the editors of this book have assembled a range of experts with experience in the major fields impacted by surface characterization. It is the only book which treats the subject of sample handling, preparation, and treatment for surface characterization. It is full of tricks, cautions, and handy tips to make the laboratory scientist’s life easier. With respect to organization of the book, the topics range from discussion of vacuum to discussion of biological, organic, elemental or compound samples, to samples prepared ex situ or in situ to the vacuum, to deposition ofthin films. Generic considerations of sample preparation are also given.

Catalysis with Supported Size-selected Pt Clusters

Catalysis with Supported Size-selected Pt Clusters PDF Author: Florian Frank Schweinberger
Publisher: Springer Science & Business Media
ISBN: 3319014994
Category : Science
Languages : en
Pages : 222

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Book Description
In his thesis, Florian Schweinberger investigates the influence of the precise size of catalytically active species on reactivity. In order to do this he carries out studies both in UHV and under ambient conditions for supported, size-selected Platium clusters (8-68 atoms). Schweinberger probed the electronic structure, adsorption properties and reactivity of two olefins on surfaces and Pt clusters in the submonolayer range. With adsorbed trichloroethene (TCE) a possible cluster-adsorbate induced change in the electronic structure, and for ethene a low-temperature, size-dependent self-/hydrogenation was observed.In a collaborative approach, Schweinberger and colleagues investigated Pt clusters under ambient pressure conditions. They characterised the clusters at at the local and integral level and tested for temperature stability. Experiments in gas phase ?-reactors and in liquid, as part of a hybrid photocatalytic system, revealed size-dependent reactivity.Overall this thesis is not only of interest for those who want to perform similar experiments but also provides superb scientific insights for researchers in the field.

Thermal Barrier Coatings: Failure Theory and Evaluation Technology

Thermal Barrier Coatings: Failure Theory and Evaluation Technology PDF Author: Yichun Zhou
Publisher: Springer Nature
ISBN: 9811927235
Category : Science
Languages : en
Pages : 943

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Book Description
This book highlights the failure theories and evaluation techniques of thermal barrier coatings, covering the thermal-mechanical–chemical coupling theories, performance and damage characterization techniques, and related evaluations. Thermal barrier coatings are the key thermal protection materials for high-temperature components in advanced aeroengines. Coating spallation is a major technical bottleneck faced by researchers. The extremely complex microstructure, diverse service environments, and failure behaviors bring challenges to the spallation analysis in terms of the selective use of mechanical theories, experimental methods, and testing platforms. In the book, the authors provide a systematic summary of the latest research and technological advances and present their insights and findings in the past couple of decades. This book is not only suitable for researchers and engineers in thermal barrier coatings and related fields but also a good reference for upper-undergraduate and postgraduate students of materials science and mechanics majors.

Sample Preparation Techniques for Chemical Analysis

Sample Preparation Techniques for Chemical Analysis PDF Author: Massoud Kaykhaii
Publisher: BoD – Books on Demand
ISBN: 1839692146
Category : Science
Languages : en
Pages : 109

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Book Description
Despite having powerful software, microchips, and solid-state detectors that enable analytical chemists to achieve fast, stable, and accurate signals from their instruments, sample preparation is the most important step in chemical analysis. Issues can arise at this step for various reasons, including a low concentration of analytes, incompatibility of the sample with the analytical instrument, and matrix interferences. This volume discusses the basics of sample preparation and examines modern techniques that can be used by both novice and expert analytical chemists. Chapters review microextraction, surface spectroscopy analysis, and techniques for particle, tissue, and cellular separation.

Indium Phosphide Negative Electron Affinity Photocathodes

Indium Phosphide Negative Electron Affinity Photocathodes PDF Author: Yun Sun
Publisher:
ISBN:
Category :
Languages : en
Pages : 500

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Book Description


Characterization of Metals and Alloys

Characterization of Metals and Alloys PDF Author: Paul Holloway
Publisher: Momentum Press
ISBN: 1606500473
Category : Science
Languages : en
Pages : 330

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Book Description
A better understanding of the microstructure of metals and alloys has led to great advances in the performance and useful applications of these, the oldest of mankind's engineered materials. This book in the Materials Characterizations series focuses on the particular molecular and atomistic properties of metals insofar as how they affect the different techniques for measuring and analyzing internal structure, surface structure, and chemical/physical properties. It provides a vital connection between commonly used characterization techniques like Scanning Electron Microscopy and how such can be used in the various ways that metals are processed, machined, and used. Review of relevant mechanical and chemical properties of metals and how they affect characterization techniques Characterization techniques used for melting and casting, machining, and metallic thin films processes Concise summaries of major characterization technologies for metals and alloys, including Auger Electron Spectroscopy, Energy-Dispersive X-Ray Spectroscopy, Neutron Activation Analysis, Scanning Electron Microscopy, and Transmission Electron Spectroscopy

Metallographic and Materialographic Specimen Preparation, Light Microscopy, Image Analysis, and Hardness Testing

Metallographic and Materialographic Specimen Preparation, Light Microscopy, Image Analysis, and Hardness Testing PDF Author:
Publisher: ASTM International
ISBN:
Category :
Languages : en
Pages : 761

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Book Description


Chemical Abstracts Service Source Index

Chemical Abstracts Service Source Index PDF Author: American Chemical Society. Chemical Abstracts Service
Publisher:
ISBN:
Category : Chemistry
Languages : en
Pages : 2064

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Book Description
A key source to journal and conference abbreviations in the sciences. Although it focuses on chemistry, other scientific and engineering disciplines are also well represented. In addition to the abbreviation and full title, each entry also contains publishing info, title changes, language and frequency of publication, and libraries owning that title. Over 130,000 entries representing more than 70,000 publications dating back to 1907 are included.

Auger- and X-Ray Photoelectron Spectroscopy in Materials Science

Auger- and X-Ray Photoelectron Spectroscopy in Materials Science PDF Author: Siegfried Hofmann
Publisher: Springer Science & Business Media
ISBN: 3642273815
Category : Science
Languages : en
Pages : 528

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Book Description
To anyone who is interested in surface chemical analysis of materials on the nanometer scale, this book is prepared to give appropriate information. Based on typical application examples in materials science, a concise approach to all aspects of quantitative analysis of surfaces and thin films with AES and XPS is provided. Starting from basic principles which are step by step developed into practically useful equations, extensive guidance is given to graduate students as well as to experienced researchers. Key chapters are those on quantitative surface analysis and on quantitative depth profiling, including recent developments in topics such as surface excitation parameter and backscattering correction factor. Basic relations are derived for emission and excitation angle dependencies in the analysis of bulk material and of fractional nano-layer structures, and for both smooth and rough surfaces. It is shown how to optimize the analytical strategy, signal-to-noise ratio, certainty and detection limit. Worked examples for quantification of alloys and of layer structures in practical cases (e.g. contamination, evaporation, segregation and oxidation) are used to critically review different approaches to quantification with respect to average matrix correction factors and matrix relative sensitivity factors. State-of-the-art issues in quantitative, destructive and non-destructive depth profiling are discussed with emphasis on sputter depth profiling and on angle resolved XPS and AES. Taking into account preferential sputtering and electron backscattering corrections, an introduction to the mixing-roughness-information depth (MRI) model and its extensions is presented.

Forthcoming Books

Forthcoming Books PDF Author: Rose Arny
Publisher:
ISBN:
Category : American literature
Languages : en
Pages : 976

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Book Description