Separation and Purification by Crystallization PDF Download
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Author: G. D. Botsaris
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 320
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Book Description
Covering a range of topics, this volume presents crystallization of polymorphs and the problems encountered in the separation of chiral compounds by selective crystallization, as well as aspects of the crystallization of amino acids, proteins, and pharmaceuticals. The introductory section includes state-of-the-art research on secondary nucleation, the mechanism for crystallization of proteins, kinetics of impurity effect on growth, and crystal morphology prediction. Other topics include the use of high-pressure crystallization in industrial processes, precipitation cases for organic and inorganic compounds, precipitation processes by antisolvents, fast reaction precipitation, and isoelectric precipitation.
Author: G. D. Botsaris
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 320
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Book Description
Covering a range of topics, this volume presents crystallization of polymorphs and the problems encountered in the separation of chiral compounds by selective crystallization, as well as aspects of the crystallization of amino acids, proteins, and pharmaceuticals. The introductory section includes state-of-the-art research on secondary nucleation, the mechanism for crystallization of proteins, kinetics of impurity effect on growth, and crystal morphology prediction. Other topics include the use of high-pressure crystallization in industrial processes, precipitation cases for organic and inorganic compounds, precipitation processes by antisolvents, fast reaction precipitation, and isoelectric precipitation.
Author: Allan Myerson
Publisher: Butterworth-Heinemann
ISBN: 0080533515
Category : Technology & Engineering
Languages : en
Pages : 329
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Book Description
Crystallization is an important separation and purification process used in industries ranging from bulk commodity chemicals to specialty chemicals and pharmaceuticals. In recent years, a number of environmental applications have also come to rely on crystallization in waste treatment and recycling processes.The authors provide an introduction to the field of newcomers and a reference to those involved in the various aspects of industrial crystallization. It is a complete volume covering all aspects of industrial crystallization, including material related to both fundamentals and applications. This new edition presents detailed material on crystallization of biomolecules, precipitation, impurity-crystal interactions, solubility, and design.Provides an ideal introduction for industrial crystallization newcomers Serves as a worthwhile reference to anyone involved in the fieldCovers all aspects of industrial crystallization in a single, complete volume
Author: Allan S. Myerson
Publisher: VCH
ISBN:
Category : Science
Languages : en
Pages : 440
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Book Description
Developed from a symposium sponsored by the International Chemical Congress of the Pacific Basin Societies, Honolulu, Hawaii, December 1989, this book presents the current research which will aid in the development, implementation, and improvement of crystallization as a separation and purification process. Sections cover basic studies, including crystal growth, nucleation, impurity-crystal interactions, and solution structure; crystallizer operation and control; crystallization of organic and biomolecules; and crystallization and precipitation of inorganic materials. Annotation copyrighted by Book News, Inc., Portland, OR
Author: Angelo Chianese
Publisher: John Wiley & Sons
ISBN: 3527645179
Category : Science
Languages : en
Pages : 253
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Book Description
Crystallization is an important technique for separation and purification of substances as well as for product design in chemical, pharmaceutical and biotechnological process industries. This ready reference and handbook draws on research work and industrial practice of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges. First the instrumentation and techniques used to measure the crystal size distribution, the nucleation and solubility points, and the chemical composition of the solid and liquid phase are outlined. Then the main techniques adopted to control industrial crystallizers, starting from fundamental approaches to the most advanced ones, including the multivariable predictive control are described. An overview of the main crystallizer types is given with details of the main control schemes adopted in industry as well as the more suitable sensors and actuators.
Author: Peter K'O-Chun Shen
Publisher:
ISBN:
Category : Crystallization
Languages : en
Pages : 266
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Book Description
Author: Hsien-Hsin Tung
Publisher: John Wiley & Sons
ISBN: 0470447788
Category : Science
Languages : en
Pages : 304
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Book Description
Filled with industrial examples emphasizing the practical applications of crystallization methodologies Based on the authors' hands-on experiences as process engineers at Merck, Crystallization of Organic Compounds guides readers through the practical aspects of crystallization. It uses plenty of case studies and examples of crystallization processes, ranging from development through manufacturing scale-up. The book not only emphasizes strategies that have been proven successful, it also helps readers avoid common pitfalls that can render standard procedures unsuccessful. The goal of this text is twofold: Build a deeper understanding of the fundamental properties of crystallization as well as the impact of these properties on crystallization process development. Improve readers' problem-solving abilities by using actual industrial examples with real process constraints. Crystallization of Organic Compounds begins with detailed discussions of fundamental thermodynamic properties, nucleation and crystal growth kinetics, process dynamics, and scale-up considerations. Next, it investigates modes of operation, including cooling, evaporation, anti-solvent, and reactive crystallization. The authors conclude with special applications such as ultrasound in crystallization and computational fluid dynamics in crystallization. Most chapters feature multiple examples that guide readers step by step through the crystallization of active pharmaceutical ingredients (APIs). With its focus on industrial applications, this book is recommended for chemical engineers and chemists who are involved with the development, scale-up, or operation of crystallization processes in the pharmaceutical and fine chemical industries.
Author: American Institute of Chemical Engineers
Publisher:
ISBN:
Category : Crystallization
Languages : en
Pages : 31
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Book Description
Author: W.L.F. Armarego
Publisher: Elsevier
ISBN: 0080515460
Category : Technology & Engineering
Languages : en
Pages : 627
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Book Description
Now in its fifth edition, the book has been updated to include more detailed descriptions of new or more commonly used techniques since the last edition as well as remove those that are no longer used, procedures which have been developed recently, ionization constants (pKa values) and also more detail about the trivial names of compounds.In addition to having two general chapters on purification procedures, this book provides details of the physical properties and purification procedures, taken from literature, of a very extensive number of organic, inorganic and biochemical compounds which are commercially available. This is the only complete source that covers the purification of laboratory chemicals that are commercially available in this manner and format.* Complete update of this valuable, well-known reference* Provides purification procedures of commercially available chemicals and biochemicals* Includes an extremely useful compilation of ionisation constants
Author: Angelo Chianese
Publisher: John Wiley & Sons
ISBN: 3527331735
Category : Science
Languages : en
Pages : 253
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Book Description
Crystallization is an important technique for separation and purification of substances as well as for product design in chemical, pharmaceutical and biotechnological process industries. This ready reference and handbook draws on research work and industrial practice of a large group of experts in the various areas of industrial crystallization processes, capturing the essence of current trends, the markets, design tools and technologies in this key field. Along the way, it outlines trouble free production, provides laboratory controls, analyses case studies and discusses new challenges. First the instrumentation and techniques used to measure the crystal size distribution, the nucleation and solubility points, and the chemical composition of the solid and liquid phase are outlined. Then the main techniques adopted to control industrial crystallizers, starting from fundamental approaches to the most advanced ones, including the multivariable predictive control are described. An overview of the main crystallizer types is given with details of the main control schemes adopted in industry as well as the more suitable sensors and actuators.
Author: Lesley Smart
Publisher: Royal Society of Chemistry
ISBN: 9780854046850
Category : Science
Languages : en
Pages : 126
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Book Description
This book looks at the common techniques used to prepare, purify and identify chemicals and concludes with a Case Study on Forensic Science.
