Reactions of Unsaturated Triosmium Carbonyl Clusters PDF Download
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Author: Mamoru Tachikawa
Publisher:
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Category :
Languages : en
Pages :
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Author: Mamoru Tachikawa
Publisher:
ISBN:
Category :
Languages : en
Pages :
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Author: Justin Mykietyn
Publisher:
ISBN:
Category : Carbonyl compounds
Languages : en
Pages : 142
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Author: S. W. Sankey
Publisher:
ISBN:
Category :
Languages : en
Pages : 0
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Author: Weng Kee Leong
Publisher:
ISBN:
Category : Chemical reactions
Languages : en
Pages : 430
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Author: David R. Moore
Publisher:
ISBN:
Category : Organoosmium compounds
Languages : en
Pages : 126
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Author: Susie C. Martins
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Category : Organoosmium compounds
Languages : en
Pages :
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Author: 李兆銘
Publisher: Open Dissertation Press
ISBN: 9781374810983
Category :
Languages : en
Pages :
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This dissertation, "The Chemistry of Triosmium Carbonyl Clusters Containing Oxygen and Sulphur Donor Ligands" by 李兆銘, Siu-ming, Lee, was obtained from The University of Hong Kong (Pokfulam, Hong Kong) and is being sold pursuant to Creative Commons: Attribution 3.0 Hong Kong License. The content of this dissertation has not been altered in any way. We have altered the formatting in order to facilitate the ease of printing and reading of the dissertation. All rights not granted by the above license are retained by the author. DOI: 10.5353/th_b4389375 Subjects: Carbonyl compounds Ligands
Author: P. A. Dolby
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Category :
Languages : en
Pages :
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Author: Robert Edward Sommerhalter
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Category : Metal clusters
Languages : en
Pages : 96
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With the goal of developing systematic syntheses of linked triosmium carbonyl clusters, we report the substitution reactions of the dibridged cluster Os3(CO)10(μ2-OEt)2 with the bifunctional ligand 1,5-pentanediol. Reaction of Os3(CO)10(μ2-OEt)2 with 1,5-pentanediol affords the cluster Os3(CO)10(μ2O(CH2)5OH)2 as the major product. Over extended reaction periods, quantitative conversion to the cluster H4Os4(CO)12 is observed. Linking of two triosmium carbonyl clusters via the 1,5-pentanediol bridging ligands has been achieved in the reaction of Os3(CO)10(μ2-O(CH2)5OH)2 with one molar equivalent of Os3(CO)10(μ2-OEt)2. A secondary product of this reaction has been characterized spectroscopically and is believed to be an intermediate in the formation of H4Os4(CO)12. A synthetic route to Os3(CO)10(μ2-OEt)2 via di-halogenated cluster intermediate Os3(CO)12X2 or Os3(CO)10(μ2-X)2 (X = Cl, Br, I) is also reported.
Author: 區逸貫
Publisher: Open Dissertation Press
ISBN: 9781374757295
Category :
Languages : en
Pages :
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This dissertation, "Chemical Reactivities of Triosmium Carbonyl Clusters With Nitrogen Heterocycles and Organomercurials" by 區逸貫, Yat-kun, Au, was obtained from The University of Hong Kong (Pokfulam, Hong Kong) and is being sold pursuant to Creative Commons: Attribution 3.0 Hong Kong License. The content of this dissertation has not been altered in any way. We have altered the formatting in order to facilitate the ease of printing and reading of the dissertation. All rights not granted by the above license are retained by the author. DOI: 10.5353/th_b3123460 Subjects: Carbonyl compounds Heterocyclic compounds Organomercury compounds
