Oxidation of Ultra High Temperature Ceramics in Water Vapor PDF Download
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Author: National Aeronautics and Space Administration (NASA)
Publisher: Createspace Independent Publishing Platform
ISBN: 9781721650033
Category :
Languages : en
Pages : 34
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Book Description
Ultra High Temperature Ceramics (UHTCs) including HfB2 + 20v/0 SiC (HS), ZrB2 + 20v/0 SiC (ZS), and ZrB2 + 30v/0 C + 14v/0 SiC (ZCS) have been investigated for use as potential aeropropulsion engine materials. These materials were oxidized in water vapor (90 percent) using a cyclic vertical furnace at 1 atm. The total exposure time was 10 h at temperatures of 1200, 1300, and 1400 C. CVD SiC was also evaluated as a baseline for comparison. Weight change, X-ray diffraction analyses, surface and cross-sectional SEM and EDS were performed. These results are compared with tests ran in a stagnant air furnace at temperatures of 1327 C for 100 min, and with high pressure burner rig (HPBR) results at 1100 and 1300 C at 6 atm for 50 h. Low velocity water vapor does not make a significant contribution to the oxidation rates of UHTCs when compared to stagnant air. The parabolic rate constants at 1300 C, range from 0.29 to 16.0 mg(sup 2)cm(sup 4)/h for HS and ZCS, respectively, with ZS results between these two values. Comparison of results for UHTCs tested in the furnace in 90 percent water vapor with HPBR results was difficult due to significant sample loss caused by spallation in the increased velocity of the HPBR. Total recession measurements are also reported for the two test environments. Nguyen, QuynhGiao N. and Opila, Elizabeth J. and Robinson, Raymond C. Glenn Research Center NASA/TM-2004-212923, E-14363
Author: National Aeronautics and Space Administration (NASA)
Publisher: Createspace Independent Publishing Platform
ISBN: 9781721650033
Category :
Languages : en
Pages : 34
Get Book Here
Book Description
Ultra High Temperature Ceramics (UHTCs) including HfB2 + 20v/0 SiC (HS), ZrB2 + 20v/0 SiC (ZS), and ZrB2 + 30v/0 C + 14v/0 SiC (ZCS) have been investigated for use as potential aeropropulsion engine materials. These materials were oxidized in water vapor (90 percent) using a cyclic vertical furnace at 1 atm. The total exposure time was 10 h at temperatures of 1200, 1300, and 1400 C. CVD SiC was also evaluated as a baseline for comparison. Weight change, X-ray diffraction analyses, surface and cross-sectional SEM and EDS were performed. These results are compared with tests ran in a stagnant air furnace at temperatures of 1327 C for 100 min, and with high pressure burner rig (HPBR) results at 1100 and 1300 C at 6 atm for 50 h. Low velocity water vapor does not make a significant contribution to the oxidation rates of UHTCs when compared to stagnant air. The parabolic rate constants at 1300 C, range from 0.29 to 16.0 mg(sup 2)cm(sup 4)/h for HS and ZCS, respectively, with ZS results between these two values. Comparison of results for UHTCs tested in the furnace in 90 percent water vapor with HPBR results was difficult due to significant sample loss caused by spallation in the increased velocity of the HPBR. Total recession measurements are also reported for the two test environments. Nguyen, QuynhGiao N. and Opila, Elizabeth J. and Robinson, Raymond C. Glenn Research Center NASA/TM-2004-212923, E-14363
Author: Nasa Technical Reports Server (Ntrs)
Publisher: BiblioGov
ISBN: 9781289263522
Category :
Languages : en
Pages : 24
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Book Description
Ultra High Temperature Ceramics (UHTCs) including HfB2 + 20v/0 SiC (HS), ZrB2 + 20v/0 SiC (ZS), and ZrB2 + 30v/0 C + 14v/0 SiC (ZCS) have been investigated for use as potential aeropropulsion engine materials. These materials were oxidized in water vapor (90 percent) using a cyclic vertical furnace at 1 atm. The total exposure time was 10 h at temperatures of 1200, 1300, and 1400 C. CVD SiC was also evaluated as a baseline for comparison. Weight change, X-ray diffraction analyses, surface and cross-sectional SEM and EDS were performed. These results are compared with tests ran in a stagnant air furnace at temperatures of 1327 C for 100 min, and with high pressure burner rig (HPBR) results at 1100 and 1300 C at 6 atm for 50 h. Low velocity water vapor does not make a significant contribution to the oxidation rates of UHTCs when compared to stagnant air. The parabolic rate constants at 1300 C, range from 0.29 to 16.0 mg(sup 2)cm(sup 4)/h for HS and ZCS, respectively, with ZS results between these two values. Comparison of results for UHTCs tested in the furnace in 90 percent water vapor with HPBR results was difficult due to significant sample loss caused by spallation in the increased velocity of the HPBR. Total recession measurements are also reported for the two test environments.
Author: T. Sato
Publisher:
ISBN:
Category :
Languages : en
Pages : 12
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Book Description
Author: Elizabeth J. Opila
Publisher: The Electrochemical Society
ISBN: 9781566773997
Category : Science
Languages : en
Pages : 588
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Book Description
" ... papers presented at the Fourth International Symposium on High Temperature Corrosion and Materials Chemistry, held at the 203rd meeting of the Electrochemical Society, Inc., in Paris, France, April 30- May 2, 2003"--Preface.
Author: Low, I. M.
Publisher: IGI Global
ISBN: 1466640677
Category : Technology & Engineering
Languages : en
Pages : 679
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Book Description
Ceramics are a versatile material, more so than is widely known. They are thermal resistant, poor electrical conductors, insulators against nuclear radiation, and not easily damaged, making ceramics a key component in many industrial processes. MAX Phases and Ultra-High Temperature Ceramics for Extreme Environments investigates a new class of ultra-durable ceramic materials, which exhibit characteristics of both ceramics and metals. Readers will explore recent advances in the manufacturing of ceramic materials that improve their durability and other physical properties, enhancing their overall usability and cost-effectiveness. This book will be of primary use to researchers, academics, and practitioners in chemical, mechanical, and electrical engineering. This book is part of the Research Essentials collection.
Author: William G. Fahrenholtz
Publisher: John Wiley & Sons
ISBN: 111892441X
Category : Technology & Engineering
Languages : en
Pages : 601
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Book Description
The first comprehensive book to focus on ultra-high temperature ceramic materials in more than 20 years Ultra-High Temperature Ceramics are a family of compounds that display an unusual combination of properties, including extremely high melting temperatures (>3000°C), high hardness, and good chemical stability and strength at high temperatures. Typical UHTC materials are the carbides, nitrides, and borides of transition metals, but the Group IV compounds (Ti, Zr, Hf) plus TaC are generally considered to be the main focus of research due to the superior melting temperatures and stable high-melting temperature oxide that forms in situ. Rather than focusing on the latest scientific results, Ultra-High Temperature Ceramics: Materials for Extreme Environment Applications broadly and critically combines the historical aspects and the state-of-the-art on the processing, densification, properties, and performance of boride and carbide ceramics. In reviewing the historic studies and recent progress in the field, Ultra-High Temperature Ceramics: Materials for Extreme Environment Applications provides: Original reviews of research conducted in the 1960s and 70s Content on electronic structure, synthesis, powder processing, densification, property measurement, and characterization of boride and carbide ceramics. Emphasis on materials for hypersonic aerospace applications such as wing leading edges and propulsion components for vehicles traveling faster than Mach 5 Information on materials used in the extreme environments associated with high speed cutting tools and nuclear power generation Contributions are based on presentations by leading research groups at the conference "Ultra-High Temperature Ceramics: Materials for Extreme Environment Applications II" held May 13-19, 2012 in Hernstein, Austria. Bringing together disparate researchers from academia, government, and industry in a singular forum, the meeting cultivated didactic discussions and efforts between bench researchers, designers and engineers in assaying results in a broader context and moving the technology forward toward near- and long-term use. This book is useful for furnace manufacturers, aerospace manufacturers that may be pursuing hypersonic technology, researchers studying any aspect of boride and carbide ceramics, and practitioners of high-temperature structural ceramics.
Author:
Publisher:
ISBN:
Category : Corrosion and anti-corrosives
Languages : en
Pages : 592
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Book Description
Author: T Sato
Publisher:
ISBN:
Category :
Languages : en
Pages : 13
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Book Description
Author: R. Naslain
Publisher: Woodhead Publishing Limited
ISBN:
Category : Reference
Languages : en
Pages : 864
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Book Description
Author: HT. Lin
Publisher:
ISBN:
Category : Ceramic
Languages : en
Pages : 15
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Book Description
This paper provides a review of two recent studies undertaken to examine the oxidation behavior of monolithic SiC and SiC-SiC composites in simulated and actual gas turbine environments. In the first study, a high-pressure and high-temperature test facility was used to expose a variety of structural ceramics and ceramic matrix composites to 15% water vapor carried in an air environment at 10 atm of total pressure and 1204°C. The second study involved the exposure of a SiC-SiC combustor liner in an industrial gas turbine for approximately 2300 h at a total pressure of 10 atm and peak liner temperature of 1150°C.
