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Author: Oscar Núñez Burcio
Publisher: Nova Publishers
ISBN: 9781634850728
Category : Food
Languages : en
Pages : 0
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Book Description
Nowadays, there is a growing need for applications in food control and safety analysis to cope with the analysis of a large number of analytes in a very complex matrix. New analytical procedures are demanding sensitivity, robustness, effectiveness and high resolution within a reduced analysis time. Most of these requirements may be met to a certain extent by the total or partial automation of the conventional analytical methods, including sample preparation or sample pre-treatment coupled on-line to an analytical system. Despite the advances in chromatographic separations and mass spectrometry techniques, sample preparation is still one of the most important parts in any analytical method development and an effective sample preparation is essential for achieving good analytical results. Obviously, ideal sample preparation methods should be fast, accurate, precise and must keep sample integrity. For this reason, and over the last years, considerable efforts have been made to develop modern approaches in sample treatment techniques that enable the reduction of the analysis time without compromising the integrity of the extraction process. The aim of this book is to discuss new trends in sample preparation techniques applied to food analysis, and it will address not only the principles of each technique, but the most relevant applications in food control and safety analysis published over the few last years.
Author: Oscar Núñez Burcio
Publisher: Nova Publishers
ISBN: 9781634850728
Category : Food
Languages : en
Pages : 0
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Book Description
Nowadays, there is a growing need for applications in food control and safety analysis to cope with the analysis of a large number of analytes in a very complex matrix. New analytical procedures are demanding sensitivity, robustness, effectiveness and high resolution within a reduced analysis time. Most of these requirements may be met to a certain extent by the total or partial automation of the conventional analytical methods, including sample preparation or sample pre-treatment coupled on-line to an analytical system. Despite the advances in chromatographic separations and mass spectrometry techniques, sample preparation is still one of the most important parts in any analytical method development and an effective sample preparation is essential for achieving good analytical results. Obviously, ideal sample preparation methods should be fast, accurate, precise and must keep sample integrity. For this reason, and over the last years, considerable efforts have been made to develop modern approaches in sample treatment techniques that enable the reduction of the analysis time without compromising the integrity of the extraction process. The aim of this book is to discuss new trends in sample preparation techniques applied to food analysis, and it will address not only the principles of each technique, but the most relevant applications in food control and safety analysis published over the few last years.
Author: Marco Aurélio Zezzi Arruda
Publisher: Nova Publishers
ISBN: 9781600211188
Category : Science
Languages : en
Pages : 318
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Book Description
Micro Sampling for Solid and Slurries Analytical Methods; Microwave-assisted Procedures for Sample Preparation: Recent Developments; Trends in Sample Preparation using Combustion Techniques; Sample Preparation of Atmospheric Aerosols for Elemental Analysis and Fractionation Studies; Extraction and Pre-Concentration Techniques for Chromatographic Analysis; Strategies in Sample Preparation for Applications in Analytical Electrochemistry In-Line Sample Preparation in Flow Analysis; The Role of Vanguard-Rearguard Strategies in Sample Preparation in Routine AnaIytical Laboratories; Strategies for Sample Preparation Focusing on Biomolecules Determination/Characterization.
Author: Josep M. Bayona
Publisher: Academic Press
ISBN: 0123813743
Category : Science
Languages : en
Pages : 2998
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Book Description
Comprehensive Sampling and Sample Preparation is a complete treatment of the theory and methodology of sampling in all physical phases and the theory of sample preparation for all major extraction techniques. It is the perfect starting point for researchers and students to design and implement their experiments and support those experiments with quality-reviewed background information. In its four volumes, fundamentals of sampling and sample preparation are reinforced through broad and detailed sections dealing with Biological and Medical, Environmental and Forensic, and Food and Beverage applications. The contributions are organized to reflect the way in which analytical chemists approach a problem. It is intended for a broad audience of analytical chemists, both educators and practitioners of the art and can assist in the preparation of courses as well in the selection of sampling and sample preparation techniques to address the challenges at hand. Above all, it is designed to be helpful in learning more about these topics, as well as to encourage an interest in sampling and sample preparation by outlining the present practice of the technology and by indicating research opportunities. Sampling and Sample preparation is a large and well-defined field in Analytical Chemistry, relevant for many application areas such as medicine, environmental science, biochemistry, pharmacology, geology, and food science. This work covers all these aspects and will be extremely useful to researchers and students, who can use it as a starting point to design and implement their experiments and for quality-reviewed background information There are limited resources that Educators can use to effectively teach the fundamental aspects of modern sample preparation technology. Comprehensive Sampling and Sample Preparation addresses this need, but focuses on the common principles of new developments in extraction technologies rather than the differences between techniques thus facilitating a more thorough understanding Provides a complete overview of the field. Not only will help to save time, it will also help to make correct assessments and avoid costly mistakes in sampling in the process Sample and sample preparation are integral parts of the analytical process but are often less considered and sometimes even completely disregarded in the available literature. To fill this gap, leading scientists have contributed 130 chapters, organized in 4 volumes, covering all modern aspects of sampling and liquid, solid phase and membrane extractions, as well as the challenges associated with different types of matrices in relevant application areas
Author: Charis M. Galanakis
Publisher: Academic Press
ISBN: 0128231556
Category : Medical
Languages : en
Pages : 408
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Book Description
Innovative Food Analysis presents a modern perspective on the development of robust, effective and sensitive techniques to ensure safety, quality and traceability of foods to meet industry standards. Significant enhancements of analytical accuracy, precision, detection limits and sampling has expanded the practical range of food applications, hence this reference offers modern food analysis in view of new trends in analytical techniques and applications to support both the scientific community and industry professionals. This reference covers the latest topics across existing and new technologies, giving emphasis on food authenticity, traceability, food fraud, food quality, food contaminants, sensory and nutritional analytics, and more. - Covers the last ten years of applications across existing and new technologies of food analytics - Presents an emphasis on techniques in food authenticity, traceability and food fraud - Discusses bioavailability testing and product analysis of food allergens and foodomics
Author: Somenath Mitra
Publisher: John Wiley & Sons
ISBN: 0471457825
Category : Science
Languages : en
Pages : 480
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Book Description
The importance of accurate sample preparation techniques cannot be overstated--meticulous sample preparation is essential. Often overlooked, it is the midway point where the analytes from the sample matrix are transformed so they are suitable for analysis. Even the best analytical techniques cannot rectify problems generated by sloppy sample pretreatment. Devoted entirely to teaching and reinforcing these necessary pretreatment steps, Sample Preparation Techniques in Analytical Chemistry addresses diverse aspects of this important measurement step. These include: * State-of-the-art extraction techniques for organic and inorganic analytes * Sample preparation in biological measurements * Sample pretreatment in microscopy * Surface enhancement as a sample preparation tool in Raman and IR spectroscopy * Sample concentration and clean-up methods * Quality control steps Designed to serve as a text in an undergraduate or graduate level curriculum, Sample Preparation Techniques in Analytical Chemistry also provides an invaluable reference tool for analytical chemists in the chemical, biological, pharmaceutical, environmental, and materials sciences.
Author: Mark Stauffer
Publisher: BoD – Books on Demand
ISBN: 9535136852
Category : Technology & Engineering
Languages : en
Pages : 184
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Book Description
The goal of this book is to present an overview of applications and ideas toward sample preparation methods and techniques used in analysis of foods and beverages. This text is a compilation of selected research articles and reviews dealing with current efforts in the application of various methods and techniques of sample preparation to analysis of a variety of foods and beverages. The chapters in this book are divided into two broad sections. Section 1 deals with some ideas for methods and techniques that are applicable to problems that impact the analysis of foods and beverages and the food and beverage industries overall. Section 2 provides applications of sample preparation methods and techniques toward determination of specific analytes or classes of analytes in various foods and beverages. Overall, this book should serve as a source of scientific information for anyone involved in any aspect of analysis of foods and beverages.
Author: Colin F. Poole
Publisher: Elsevier
ISBN: 0128169079
Category : Science
Languages : en
Pages : 742
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Book Description
Solid Phase Extraction thoroughly presents both new and historic techniques for dealing with solid phase extraction. It provides all information laboratory scientists need for choosing and utilizing suitable sample preparation procedures for any kind of sample. In addition, the book showcases the contemporary uses of sample preparation techniques in the most important industrial and academic project environments, including solid-phase Microextraction, molecularly imprinted polymers, magnetic nanoparticles, and more. Written by recognized experts in their respective fields, this one-stop reference is ideal for those who need to know which technique to choose for solid phase extraction. Used in conjunction with a similar release, Liquid Phase Extraction, this book allows users to master this crucial aspect of sample preparation. - Defines the current state-of-the-art in extraction techniques and the methods and procedures for implementing them in laboratory practice - Includes extensive referencing that facilitates the identification of key information - Aimed at both entry-level scientists and those who want to explore new techniques and methods
Author: S.C. Moldoveanu
Publisher: Elsevier
ISBN: 0080540708
Category : Science
Languages : en
Pages : 949
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Book Description
Sample preparation is an essential step in many analyses. This book approaches the topic of sample preparation in chromatography in a methodical way, viewing it as a logical connection between sample collection and analytical chromatography. Providing a guide for choosing the appropriate sample preparation for a given analysis, this book describes various ways to process the sample, explaining the principle, discussing the advantages and disadvantages, describing the applicability to different types of samples, and showing the fitness to specific chromatographic determinations. The first part of the book contains an overview of sample preparation showing its relation to sample collection and to the core chromatographic analysis. The second part covers procedures that do not use chemical modifications of the analyte and includes methods for sample dissolution, concentration and cleanup designed mainly for modifying the initial matrix of the sample. This part starts with conventional separations such as filtration and distillation and finishes with more advanced techniques such as solid phase extraction and electroseparations. The third part gives a description of the chemical modifications that can be performed on a sample either for fractionation purposes or to improve a specific property of the analyte. This part includes derivatizations, polymer chemical degradations, and pyrolysis.
Author: Rosalind Wolstenholme
Publisher: John Wiley & Sons
ISBN: 1119978289
Category : Medical
Languages : en
Pages : 464
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Book Description
An in-depth text that explores the interface between analytical chemistry and trace evidence Analytical Techniques in Forensic Science is a comprehensive guide written in accessible terms that examines the interface between analytical chemistry and trace evidence in forensic science. With contributions from noted experts on the topic, the text features a detailed introduction analysis in forensic science and then subsequent chapters explore the laboratory techniques grouped by shared operating principles. For each technique, the authors incorporate specific theory, application to forensic analytics, interpretation, forensic specific developments, and illustrative case studies. Forensic techniques covered include UV-Vis and vibrational spectroscopy, mass spectrometry and gas and liquid chromatography. The applications reviewed include evidence types such as fibers, paint, drugs and explosives. The authors highlight data collection, subsequent analysis, what information has been obtained and what this means in the context of a case. The text shows how analytical chemistry and trace evidence can problem solve the nature of much of forensic analysis. This important text: Puts the focus on trace evidence and analytical science Contains case studies that illustrate theory in practice Includes contributions from experts on the topics of instrumentation, theory, and case examples Explores novel and future applications for analytical techniques Written for undergraduate and graduate students in forensic chemistry and forensic practitioners and researchers, Analytical Techniques in Forensic Science offers a text that bridges the gap between introductory textbooks and professional level literature.
Author: John Maclane
Publisher: Createspace Independent Publishing Platform
ISBN: 9781548034979
Category :
Languages : en
Pages : 250
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Book Description
One of the most important challenges in modernfood analysis is the research of new reliable sample preparationmethods. In fact, traditional and automated procedurescan ensure reliable results on condition that sample pretreatmentmethods are fast, accurate, precise, and able to maintainthe integrity of extraction processes. The book New trends insample preparation techniques for food analysis, editedby Oscar N��ez and Paolo Lucci, describes the currentstate of art of sample pretreatment systems in the fieldof food analysis.Contents The book is subdivided into seven chapters with afive-page detailed preface providing a preliminary discussionabout extraction procedures. The first chapter concerns newtrends in solid-phase extraction (SPE) analyses and innovativesorbent chemicals. The book considers new molecularlyimprinted polymers for SPE systems in Chap. 2, with relationto synthetic processes and practical examples. Chapter 3 isdedicated to turbulent flow chromatography and related applicationsfor food analyses (trace elements, contaminants).Subsequently, the discussion concerns new analytical applicationsfor food matrices: QuEChERS (Chap. 4) andmicroextraction methods for simple and inexpensive separations(Chap. 5). Chapter 6 is completely dedicated toionic liquids as an essential component of sample preparationfor the determination of metals and organicchemicals in food matrices. The final chapter discussesthe current state of art of supercritical fluid extractionfor different analytical purposes.
