Author: Mikhail A. Krivoglaz
Publisher: Springer Science & Business Media
ISBN: 3642742912
Category : Science
Languages : en
Pages : 483
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Book Description
Mikhail Alexandrovich Krivoglaz died unexpectedly when he was preparing the English edition of his two-volume monograph on diffraction and diffuse scatter ing of X-rays and neutrons in imperfect crystals. His death was a heavy blow to all who knew him, who had worked with him and to the world science community as a whole. The application of the diffraction techniques for the study of imperfections of crystal structures was the major field of Krivoglaz' work throughout his career in science. He started working in the field in the mid-fifties and since then made fundamental contributions to the theory of real crystals. His results have largely determined the current level of knowledge in this field for more than thirty years. Until the very last days of his life, Krivoglaz continued active studies in the physics of diffraction effects in real crystals. His interest in the theory aided in the explanation of the rapidly advancing experimental studies. The milestones marking important stages of his work were the first mono graph on the theory of X-ray and neutron scattering in real crystals which was published in Russian in 1967 (a revised English edition in 1969), and the two volume monograph published in Russian in 1983-84 (this edition is the revised translation of the latter).
Author: Izyumov
Publisher: Springer Science & Business Media
ISBN: 1461536588
Category : Science
Languages : en
Pages : 349
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Book Description
Detennination of the magnetic structure of magnetic materials is a fundamental problem that can be solved by magnetic neutron diffraction techniques. By magnetic structures we refer to the mutual alignment of the magnetic moments of the atoms in a crystal and their overall alignment relative to the crystallographic axes. Some indirect, tentative data on the magnetic structure of magnetic materials can be obtained from research on their magnetic, mechanical, thermal, and other properties. But only neutron diffraction is a unique direct method of detennining the magnetic structure of a crystal. The magnetic structure of more than one thousand crystals with magnetic order has been studied during 30 years of neutron diffraction research made on reactors in a large number of laboratories in the world. The results of this research work are extensively described in the handbook Magnetic Structures Determined by Neutron Diffraction [176]; in the present book, we will often refer to this handbook. The first extensive theoretical generalization of the principles of magnetic neutron diffraction and the results of research on magnetic structures appeared in the book by Yu. A. Izyumov and R. P. Ozerov Magnetic Neutron Diffraction [24, 134].
Author: Yurii A. Izyumov
Publisher: Springer Science & Business Media
ISBN: 1468407120
Category : Science
Languages : en
Pages : 607
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Book Description
The inter action between the magnetic field generated by the neutron and the magnetic moment of atoms containing unpaired electrons was experimentally demonstrated for the first time about twenty years ago. The basic theory describing such an in teraction had already been developed and the first nuclear reactors with large available thermal neutron fluxes had recently been con structed. The power of the magnetic neutron interaction for in vestigating the structure of magnetic materials was immediately recognized and put to use where possible. Neutron diffraction, however, was practicable only in countries with nuclear reactors. The earliest neutron determinations of magnetic ordering were hence primarily carried out at Oak Ridge and Brookhaven in the US, at Chalk River in Canada and at Harwell in England. Diffraction patterns from polycrystalline ferromagnets and antiferromagnets are interpretable if produced by simple spin arrays. More complex magnetic scattering patterns could often be unravelled, in terms of a three-dimensional array of atomic moments, if the specimen studied is a single crystal. The devel opment of sophisticated cryogenic equipment, with independently alignable magnetic fields, opened the way to greater complexity in the magnetic structures that could be successfully determined, as did also the introduction of polarized neutron beams. By the end of the 'sixties, many countries were contributing significantly to neutron diffraction studies of a wide variety of magnetic materials.
Author: Michael T. Hutchings
Publisher: Springer Science & Business Media
ISBN: 9780792318095
Category : Science
Languages : en
Pages : 622
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Book Description
The relevance of residual stresses in engineering components is being increasingly appreciated by modern engineers concerned with design and performance. The non-destructive evaluation of such stresses has provided a challenge which has been addressed by the use of X-ray diffraction to characterize near-surface stresses. The extension of diffraction stress measurements to include neutron diffraction represents a major advance. Use of the penetrating power of neutrons is ideally suited to the determination of macrostress variation through thick components and of microstresses in composites and multiphase alloys. This collection of papers on the subject is the first of its kind and represents a definitive summary of the field. With contributions by most of the world's experts, it gives a comprehensive treatment of the theory, practice and problems in the measurement of residual stresses using neutrons, with references to virtually all work currently in print. It provides state-of-the-art information about the uses and limitations of the method, with numerous examples. It is appropriate both for those currently using X-ray methods, and f
Author: M.T. Hutchings
Publisher: CRC Press
ISBN: 0203402812
Category : Science
Languages : en
Pages : 383
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Book Description
Over the past 25 years the field of neutron diffraction for residual stress characterization has grown tremendously, and has matured from the stage of trial demonstrations to provide a practical tool with widespread applications in materials science and engineering. While the literature on the subject has grown commensurately, it has also remained
Author: P. Chieux
Publisher: Springer
ISBN:
Category : Science
Languages : en
Pages : 384
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Book Description
Author: Chick C. Wilson
Publisher: World Scientific
ISBN: 9789810237769
Category : Science
Languages : en
Pages : 390
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Book Description
This important book presents a comprehensive account of the techniques & applications of single crystal neutron diffraction in the area of chemical crystallography & molecular structure. Beginning with a brief description of the general principles & the reasons for choosing the technique - the "why" - the book covers the methods for both the production of neutrons & the measurement of their scattering by molecular crystals - the "how" - followed by a detailed survey of past, present & future applications - the "what". The coverage of both steady state & pulsed neutron sources & instrumentation is extensive, while the survey of applications is the most comprehensive yet undertaken. The book endeavours to show why the technique is an essential method for studying areas as diverse as hydrogen bonding & weak interactions, organometallics, supramolecular chemistry & crystal engineering, metal hydrides, charge density & pharmaceuticals. It is an ideal reference source for the research worker interested in using neutron diffraction to study the structure of molecules. Contents: Crystallography & the Importance of Structural Information; Neutron Scattering; Neutron Diffractometers; Review of Applications I: The Accurate Location of Atoms; Review of Applications II: Hydrogen Bonding & Other Intermolecular Interactions; Review of Applications III: Probing Vibrations & Disorder; Impact on Material Properties & Design; The Future: New Instruments, New Sources, New Techniques. Readership: Students & researchers involved in structural science, especially chemical crystallography.
Author: André Authier
Publisher: Springer Science & Business Media
ISBN: 1461558794
Category : Science
Languages : en
Pages : 419
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Book Description
This volume collects the proceedings of the 23rd International Course of Crystallography, entitled "X-ray and Neutron Dynamical Diffraction, Theory and Applications," which took place in the fascinating setting of Erice in Sicily, Italy. It was run as a NATO Advanced Studies Institute with A. Authier (France) and S. Lagomarsino (Italy) as codirectors, and L. Riva di Sanseverino and P. Spadon (Italy) as local organizers, R. Colella (USA) and B. K. Tanner (UK) being the two other members of the organizing committee. It was attended by about one hundred participants from twenty four different countries. Two basic theories may be used to describe the diffraction of radiation by crystalline matter. The first one, the so-called geometrical, or kinematical theory, is approximate and is applicable to small, highly imperfect crystals. It is used for the determination of crystal structures and describes the diffraction of powders and polycrystalline materials. The other one, the so-called dynamical theory, is applicable to perfect or nearly perfect crystals. For that reason, dynamical diffraction of X-rays and neutrons constitutes the theoretical basis of a great variety of applications such as: • the techniques used for the characterization of nearly perfect high technology materials, semiconductors, piezoelectric, electrooptic, ferroelectric, magnetic crystals, • the X-ray optical devices used in all modem applications of Synchrotron Radiation (EXAFS, High Resolution X-ray Diffractometry, magnetic and nuclear resonant scattering, topography, etc. ), and • X-ray and neutron interferometry.
Author: Erich H. Kisi
Publisher: Oxford University Press
ISBN: 0199657424
Category : Science
Languages : en
Pages : 509
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Book Description
This is the first book covering the theory, practicalities, and the extensive applications of neutron powder diffraction in materials science, physics, chemistry, mineralogy, and engineering. The broad coverage should be accessible to graduate students and senior undergraduates in science and engineering, as well as lecturers and researchers.
Author:
Publisher: Academic Press
ISBN: 0128192143
Category : Science
Languages : en
Pages : 408
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Book Description
Neutron Crystallography in Structural Biology, Volume 634, the latest volume in the Methods in Enzymology series, continues the legacy of this premier serial with quality chapters authored by leaders in the field. Chapters in this updated release include Fundamentals of neutron crystallography in structural biology, Large crystal growth for neutron protein crystallography, Prospects for membrane protein crystals in NMX, IMAGINE: The neutron protein crystallography beamline at the high flux isotope reactor, The macromolecular neutron diffractometer at the spallation neutron source, Current status and near future plan of neutron protein crystallography at J-PARC, Neutron macromolecular crystallography at the European spallation source, and much more.
