Molten Metal Analysis by Laser Produced Plasmas PDF Download
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Author: Yong W. Kim
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Category :
Languages : en
Pages :
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Author: Yong W. Kim
Publisher:
ISBN:
Category :
Languages : en
Pages :
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Author:
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ISBN:
Category :
Languages : en
Pages : 42
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A new method of molten metal analysis, based on time- and space-resolved spectroscopy of a laser-produced plasma (LPP) plume of a molten metal surface, has been implemented in the form of a prototype LPP sensor-probe, allowing in-situ analysis in less than 1 minute. The research at Lehigh University has been structured in 3 phases: laboratory verification of concept, comparison of LPP method with conventional analysis of solid specimens and field trials of prototype sensor-probe in small-scale metal shops, and design/production/installation of two sensor-probes in metal production shops. Accomplishments in the first 2 phases are reported. 6 tabs, 3 figs.
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Category :
Languages : en
Pages : 56
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The radically new methodology of in-situ laser-produced plasma (LPP) analysis of molten metals, as developed at Lehigh University, has been implemented into an LPP sensor-probe system, ready for deployment at steelmaking facilities. The system consists of an LPP sensor-probe head, which is immersed into the molten metal bath for the short duration of measurement, a control console, an umbilical cord connecting the above two units, and a support console providing coolants and pneumatic supports to the control console. The Department of Energy funding has supported Phase III-A and -B of the project in a joint sponsorship with AISI, CTU 5-2 Consortium, and Lehigh University. The objectives have been to: (1) implement the molten metal calibration protocol for the LPP analysis methodology; (2) implement the methodology in the form of a second-generation LPP sensor-probe system, which facilitates real-time process control by in-situ determination of elemental composition of molten steel alloys; (3) deploy such developmental systems in steelmaking facilities; (4) upgrade the systems to a third-generation design; and (5) effect technology transfer by selecting a manufacturer of commercial LPP sensor-probe systems. Four of the five objectives have been fully met. The deployment objective has been partially realized at present. The full LPP sensor-probe system has been put through trial immersion runs at a foundry, but its deployment at steelmaking facilities has progressed to a stage where various issues of financial and legal nature are being codified into a formal agreement between a host site and Lehigh University.
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Category :
Languages : en
Pages : 18
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We have shown that a laser-produced plasma plume which is representative in composition of the condensed phase target can be reproducibly generated if the movement of the surface due to evaporation is kept in pace with the thermal diffusion front propagating into the bulk. The resulting mass loss is then strongly controlled by the thermal diffusivity of the target matter, and this relationship has been exploited to measure the thermal diffusivity of metallic alloys. We have developed a novel RF levitator-heater as a contamination-free molten metal source to be used as a target for LPP plume generation. In order to determine the mass loss due to LPP excitation, a new high sensitivity transducer has been constructed for measurement of the resulting impulse imparted on the specimen. The impulse transducer is built onto the specimen holder within the levitation-assisted molten metal source. The LPP method has been fully excercised for measurement of the thermal diffusivity of a molten specimen relative to the value for its room temperature solid. The results for SS304 and SS316 are presented together with a critique of the results. A numerical modeling of specimen heating in the molten metal source and the physical basis of the new hod are also presented.
Author: Nichola Walsh
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Category :
Languages : en
Pages : 0
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During the interaction of an intense laser pulse with a solid metal target, a high temperature, high density plasma is formed. Pulsed laser ablation has attracted much interest over the past fifty years with experimental and theoretical work largely focussed on the study of laser produced plasmas in vacuum. The study of pulsed laser ablation has been largely motivated from a materials processing perspective, with the characterisation of thin films using pulsed laser deposition of particular interest. Another application resulting from the study of laser produced plasmas is the use of laser-induced breakdown spectroscopy (LIBS) for elemental composition and quantitative analysis of samples. LIBS is now a widely used technique employed in various fields including environmental analysis, forensics and biomedical applications. While much work has been carried out on pulsed ablation of materials in vacuum and gas ambient, comparatively little research has been done on ablation in liquid media. As a result, the fundamental understanding of laser produced plasmas in liquids remains insufficient. Using techniques such as time resolved imaging and spectroscopy, a full characterisation of the plasma formed in air was undertaken as a comparison to the subsequent investigation of the plasma formed in water ambient. Single pulse studies revealed information on the dynamic evolution of a laser plasma formed in the liquid phase where strong confinement and broadband emission were the main observations. Shadowgraphy measurements were performed to examine the dynamic behaviour of the cavitation bubble that eventually forms post plasma ignition. The results of time resolved optical emission measurements from within the cavitation bubble using a second laser pulse reveal for the first time the full dynamic evolution of the plasma formed in such an environment.
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Category : Aeronautics
Languages : en
Pages : 652
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Lists citations with abstracts for aerospace related reports obtained from world wide sources and announces documents that have recently been entered into the NASA Scientific and Technical Information Database.
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Category : Power resources
Languages : en
Pages : 782
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Category : High temperature chemistry
Languages : en
Pages : 252
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Author: John W. Hastie
Publisher: Springer Science & Business Media
ISBN: 146120481X
Category : Science
Languages : en
Pages : 452
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Conference Overview and the Role of Chemistry in High-Temperature Materials Science and Technology LEO BREWER Department of ChemistIy, University of California, and Materials and Chemical Sciences Division, Lawrence Berkeley Laboratory, 1 Cyclotron Road, Berkeley, CA 94720 I don't want to compete with the fascinating historic account that John Drowart gave us, but I would like to go through the history of high don't get the reaction that I get from temperature symposia. I hope I some of my classes when I say, "Remember when such-and-such hap pened during the War?" And I get this blank look, and one of the students will say, "I wasn't born until after the Korean War. " Neverthe less, during World War II, many people in the high-temperature field had their first initiation. But there was one handicap. Owing to security measures, they were not able to interact with one another. Following the War, it was recognized that the high-temperature field was going to expand to meet the demands for materials with unique properties. To meet the demands for new fabrication techniques, it was important to establish better communications among various people. High-tempera ture symposia were established at that time and have continued very frequently, and I'd like to point out why they are especially important for this field. One problem is that it is not easy to work at high temperatures.
Author: Haydn N. G. Wadley
Publisher:
ISBN:
Category : Technology & Engineering
Languages : en
Pages : 280
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