Microanalysis of Solids

Microanalysis of Solids PDF Author: B.G. Yacobi
Publisher: Springer Science & Business Media
ISBN: 1489914927
Category : Science
Languages : en
Pages : 459

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Book Description
The main objective of this book is to systematically describe the basic principles of the most widely used techniques for the analysis of physical, structural, and compositional properties of solids with a spatial resolution of approxi mately 1 ~m or less. Many books and reviews on a wide variety of microanalysis techniques have appeared in recent years, and the purpose of this book is not to replace them. Rather, the motivation for combining the descriptions of various mi croanalysis techniques in one comprehensive volume is the need for a reference source to help identify microanalysis techniques, and their capabilities, for obtaining particular information on solid-state materials. In principle, there are several possible ways to group the various micro analysis techniques. They can be distinguished by the means of excitation, or the emitted species, or whether they are surface or bulk-sensitive techniques, or on the basis of the information obtained. We have chosen to group them according to the means of excitation. Thus, the major parts of the book are: Electron Beam Techniques, Ion Beam Techniques, Photon Beam Techniques, Acoustic Wave Excitation, and Tunneling of Electrons and Scanning Probe Microscopies. We hope that this book will be useful to students (final year undergrad uates and graduates) and researchers, such as physicists, material scientists, electrical engineers, and chemists, working in a wide variety of fields in solid state sciences.

Microanalysis of Solids

Microanalysis of Solids PDF Author: B.G. Yacobi
Publisher: Springer Science & Business Media
ISBN: 1489914927
Category : Science
Languages : en
Pages : 459

Get Book Here

Book Description
The main objective of this book is to systematically describe the basic principles of the most widely used techniques for the analysis of physical, structural, and compositional properties of solids with a spatial resolution of approxi mately 1 ~m or less. Many books and reviews on a wide variety of microanalysis techniques have appeared in recent years, and the purpose of this book is not to replace them. Rather, the motivation for combining the descriptions of various mi croanalysis techniques in one comprehensive volume is the need for a reference source to help identify microanalysis techniques, and their capabilities, for obtaining particular information on solid-state materials. In principle, there are several possible ways to group the various micro analysis techniques. They can be distinguished by the means of excitation, or the emitted species, or whether they are surface or bulk-sensitive techniques, or on the basis of the information obtained. We have chosen to group them according to the means of excitation. Thus, the major parts of the book are: Electron Beam Techniques, Ion Beam Techniques, Photon Beam Techniques, Acoustic Wave Excitation, and Tunneling of Electrons and Scanning Probe Microscopies. We hope that this book will be useful to students (final year undergrad uates and graduates) and researchers, such as physicists, material scientists, electrical engineers, and chemists, working in a wide variety of fields in solid state sciences.

Laser Microanalysis

Laser Microanalysis PDF Author: Lieselotte Moenke-Blankenburg
Publisher: Wiley-Interscience
ISBN:
Category : Science
Languages : en
Pages : 312

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Book Description
Examines the state-of-the-art in laser microanalysis. First three chapters deal with analytical applications when a laser is a radiation source, effects of laser-target interactions, studies of microplasma generation, and laser microanalysis of solids. Second part of the book focuses on special techniques, methodical treatments, and the applications of laser microanalysis to chemistry, mineralogy, metallurgy, biology, medicine, archeology, environmental research, and forensic science.

Cathodoluminescence Microscopy of Inorganic Solids

Cathodoluminescence Microscopy of Inorganic Solids PDF Author: B.G. Yacobi
Publisher: Springer Science & Business Media
ISBN: 1475795955
Category : Science
Languages : en
Pages : 294

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Book Description
Microcharacterization of materials is a rapidly advancing field. Among the many electron and ion probe techniques, the cathodoluminescence mode of an electron probe instrument has reached a certain maturity, which is reflected by an increas ing number of publications in this field. The rapid rate of progress in applications of cathodoluminescence techniques in characterizing inorganic solids has been especially noticeable in recent years. The main purpose of the book is to outline the applications of cath odoluminescence techniques in the assessment of optical and electronic proper ties of inorganic solids, such as semiconductors, phosphors, ceramics, and min erals. The assessment provides, for example, information on impurity levels derived from cathodoluminescence spectroscopy, analysis of dopant concentra tions at a level that, in some cases, is several orders of magnitude lower than that attainable by x-ray microanalysis, the mapping of defects, and the determination of carrier lifetimes and the charge carrier capture cross sections of impurities. In order to make the book self-contained, some basic concepts of solid-state phys ics, as well as various cathodoluminescence techniques and the processes leading to luminescence phenomena in inorganic solids, are also described. We hope that this book will be useful to both scientists and graduate students interested in microcharacterization of inorganic solids. This book, however, was not intended as a definitive account of cathodoluminescence analysis of in organic solids. In considering the results presented here, readers should re member that many materials have properties that vary widely as a function of preparation conditions.

Scanning Electron Microscopy and X-Ray Microanalysis

Scanning Electron Microscopy and X-Ray Microanalysis PDF Author: Joseph Goldstein
Publisher: Springer Science & Business Media
ISBN: 1461332737
Category : Science
Languages : en
Pages : 679

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Book Description
This book has evolved by processes of selection and expansion from its predecessor, Practical Scanning Electron Microscopy (PSEM), published by Plenum Press in 1975. The interaction of the authors with students at the Short Course on Scanning Electron Microscopy and X-Ray Microanalysis held annually at Lehigh University has helped greatly in developing this textbook. The material has been chosen to provide a student with a general introduction to the techniques of scanning electron microscopy and x-ray microanalysis suitable for application in such fields as biology, geology, solid state physics, and materials science. Following the format of PSEM, this book gives the student a basic knowledge of (1) the user-controlled functions of the electron optics of the scanning electron microscope and electron microprobe, (2) the characteristics of electron-beam-sample inter actions, (3) image formation and interpretation, (4) x-ray spectrometry, and (5) quantitative x-ray microanalysis. Each of these topics has been updated and in most cases expanded over the material presented in PSEM in order to give the reader sufficient coverage to understand these topics and apply the information in the laboratory. Throughout the text, we have attempted to emphasize practical aspects of the techniques, describing those instru ment parameters which the microscopist can and must manipulate to obtain optimum information from the specimen. Certain areas in particular have been expanded in response to their increasing importance in the SEM field. Thus energy-dispersive x-ray spectrometry, which has undergone a tremendous surge in growth, is treated in substantial detail.

The Physics of Solids

The Physics of Solids PDF Author: J. B. Ketterson
Publisher: Oxford University Press
ISBN: 0191060550
Category : Science
Languages : en
Pages : 1053

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Book Description
This comprehensive text covers the basic physics of the solid state starting at an elementary level suitable for undergraduates but then advancing, in stages, to a graduate and advanced graduate level. In addition to treating the fundamental elastic, electrical, thermal, magnetic, structural, electronic, transport, optical, mechanical and compositional properties, we also discuss topics like superfluidity and superconductivity along with special topics such as strongly correlated systems, high-temperature superconductors, the quantum Hall effects, and graphene. Particular emphasis is given to so-called first principles calculations utilizing modern density functional theory which for many systems now allow accurate calculations of the electronic, magnetic, and thermal properties.

Mechanics of Solids

Mechanics of Solids PDF Author: Carl Ross
Publisher: Routledge
ISBN: 1317189388
Category : Technology & Engineering
Languages : en
Pages : 1510

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Book Description
An introduction to the fundamental concepts of solid materials and their properties The primary recommended text of the Council of Engineering Institutions for university undergraduates studying the mechanics of solids New chapters covering revisionary mathematics, geometrical properties of symmetrical sections, bending stresses in beams, composites and the finite element method Free electronic resources and web downloads support the material contained within this book Mechanics of Solids provides an introduction to the behaviour of solid materials and their properties, focusing upon the fundamental concepts and principles of statics and stress analysis. Essential reading for first year undergraduates, the mathematics in this book has been kept as straightforward as possible and worked examples are used to reinforce key concepts. Practical stress and strain scenarios are also covered including stress and torsion, elastic failure, buckling, bending, as well as examples of solids such as thin-walled structures, beams, struts and composites. This new edition includes new chapters on revisionary mathematics, geometrical properties of symmetrical sections, bending stresses in beams, composites, the finite element method, and Ross’s computer programs for smartphones, tablets and computers.

Scanning Electron Microscopy

Scanning Electron Microscopy PDF Author: Ludwig Reimer
Publisher: Springer
ISBN: 3540389679
Category : Science
Languages : en
Pages : 538

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Book Description
Scanning Electron Microscopy provides a description of the physics of electron-probe formation and of electron-specimen interactions. The different imaging and analytical modes using secondary and backscattered electrons, electron-beam-induced currents, X-ray and Auger electrons, electron channelling effects, and cathodoluminescence are discussed to evaluate specific contrasts and to obtain quantitative information.

Electron and Ion Microscopy and Microanalysis

Electron and Ion Microscopy and Microanalysis PDF Author: Lawrence E Murr
Publisher: CRC Press
ISBN: 1482293358
Category : Technology & Engineering
Languages : en
Pages : 856

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Book Description
The publication date of the first edition is not stated, but the new edition is apparently considerably revised and expanded. It was written to serve as a multi-purpose text at the senior or graduate level and as a reference for the practicing scientist or engineer. Readers should have a math backgr

Electron Beam Interactions with Solids for Microscopy, Microanalysis & Microlithography

Electron Beam Interactions with Solids for Microscopy, Microanalysis & Microlithography PDF Author: David F. Kyser
Publisher: Scanning Electron Microscopy
ISBN:
Category : Science
Languages : en
Pages : 392

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Book Description


Handbook of Sample Preparation for Scanning Electron Microscopy and X-Ray Microanalysis

Handbook of Sample Preparation for Scanning Electron Microscopy and X-Ray Microanalysis PDF Author: Patrick Echlin
Publisher: Springer Science & Business Media
ISBN: 0387857311
Category : Technology & Engineering
Languages : en
Pages : 329

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Book Description
Scanning electr on microscopy (SEM) and x-ray microanalysis can produce magnified images and in situ chemical information from virtually any type of specimen. The two instruments generally operate in a high vacuum and a very dry environment in order to produce the high energy beam of electrons needed for imaging and analysis. With a few notable exceptions, most specimens destined for study in the SEM are poor conductors and composed of beam sensitive light elements containing variable amounts of water. In the SEM, the imaging system depends on the specimen being sufficiently electrically conductive to ensure that the bulk of the incoming electrons go to ground. The formation of the image depends on collecting the different signals that are scattered as a consequence of the high energy beam interacting with the sample. Backscattered electrons and secondary electrons are generated within the primary beam-sample interactive volume and are the two principal signals used to form images. The backscattered electron coefficient ( ? ) increases with increasing atomic number of the specimen, whereas the secondary electron coefficient ( ? ) is relatively insensitive to atomic number. This fundamental diff- ence in the two signals can have an important effect on the way samples may need to be prepared. The analytical system depends on collecting the x-ray photons that are generated within the sample as a consequence of interaction with the same high energy beam of primary electrons used to produce images.