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Author: Marcello Locatelli
Publisher: MDPI
ISBN: 303921084X
Category : Technology & Engineering
Languages : en
Pages : 308
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Book Description
The present Special Issue, “Innovative Extraction Techniques and Hyphenated Instrument Configuration for Complex Matrices Analysis”, aims to collect and to disseminate some of the most significant and recent contributions in the interdisciplinary area of innovative extraction procedures from complex matrices followed by validated analytical methods using hyphenated instrument configurations to support the optimization of the whole process and the scale-up possibility
Author: Marcello Locatelli
Publisher: MDPI
ISBN: 303921084X
Category : Technology & Engineering
Languages : en
Pages : 308
Get Book Here
Book Description
The present Special Issue, “Innovative Extraction Techniques and Hyphenated Instrument Configuration for Complex Matrices Analysis”, aims to collect and to disseminate some of the most significant and recent contributions in the interdisciplinary area of innovative extraction procedures from complex matrices followed by validated analytical methods using hyphenated instrument configurations to support the optimization of the whole process and the scale-up possibility
Author: Marcello Locatelli
Publisher:
ISBN: 9783039210855
Category : Chemical engineering
Languages : en
Pages : 308
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Book Description
The present Special Issue, “Innovative Extraction Techniques and Hyphenated Instrument Configuration for Complex Matrices Analysis”, aims to collect and to disseminate some of the most significant and recent contributions in the interdisciplinary area of innovative extraction procedures from complex matrices followed by validated analytical methods using hyphenated instrument configurations to support the optimization of the whole process and the scale-up possibility.
Author: Marcello Locatelli
Publisher: MDPI
ISBN: 3039365770
Category : Medical
Languages : en
Pages : 162
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Book Description
The availability (and the development) of innovative approaches to quantitative analyses and the data processing are often mandatory to deeply characterize a sample and to correctly highlight the analytical target. These objectives are carried out either by simply improving a single aspect of the analytical protocol or by developing a synergy of steps (from extraction to instrumental configuration to chemometric approaches) to obtain the maximum analytical information sought. Examples are innovative extraction protocols (also following the recent guidelines on green analytical chemistry) or new materials for the selective extraction of target compounds, multi-analytes screening methods, and "untargeted" approaches for food applications. In this text, the various articles are attributable to these elements, in particular, we start with a multi-analyte method for the determination of 10 different cannabinoids from Cannabis sativa L. by means of conventional techniques (Mandrioli and coworkers), to then see the application of techniques hyphenated "ultra-fast" by UPLC-MS for the authentication of food products (Xue and coworkers). The work of Song and coworkers on these applications in food products is also interesting, as it highlights how the collection process (and the timing of this passage) can affect the chemical profile and, consequently, the biological activity of Panax ginseng. Mocan and coworkers, applying an innovative extraction technique based on microwaves and applying well-known, robust, and easy-to-use instrumentation, have demonstrated how it is possible to discriminate between various species of Galium and how the chemical profiles obtained can support the biological activities observed. Similarly, but with the aim of developing new sample pretreatment procedures, Maggira and collaborators have developed graphene oxide-based materials for the selective extraction of sulfonamides in milk. Shen and coworkers apply a different type of approach, the "untargeted" one, for the geographical characterization of the Gentian Rigescens for which they combine chemometric techniques for the processing of raw chemical profile data. Wang and coworkers report a multiclass screening of drugs with high-resolution mass spectrometry through which they manage to obtain a high-scale, fast screening method for pesticides in fishery drugs based on ultrahigh-performance liquid chromatography tandem quadrupole-orbitrap high-resolution mass spectrometer.
Author: Roberto Romero-González
Publisher: Elsevier
ISBN: 0128096489
Category : Science
Languages : en
Pages : 362
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Book Description
Applications of High Resolution Mass Spectrometry: Food Safety and Pesticide Residue Analysis is the first book to offer complete coverage of all aspects of high resolution mass spectrometry (HRMS) used for the analysis of pesticide residue in food. Aimed at researchers and graduate students in food safety, toxicology, and analytical chemistry, the book equips readers with foundational knowledge of HRMS, including established and state-of-the-art principles and analysis strategies. Additionally, it provides a roadmap for implementation, including discussions of the latest instrumentation and software available. Detailed coverage is given to the application of HRMS coupled to ultra high-performance liquid chromatography (UHPLC-HRMS) in the analysis of pesticide residue in fruits and vegetables and food from animal origin. The book also discusses extraction procedures and the challenges of sample preparation, gas chromatography coupled to high resolution mass spectrometry, flow injection-HRMS, ambient ionization, and identification of pesticide transformation products in food. Responding to the fast development and application of these new procedures, this book is an essential resource in the food safety field. - Arms researchers with an in-depth resource devoted to the rapid advances in HRMS tools and strategies for pesticide residue analysis in food - Provides a complete overview of analytical methodologies and applications of HRMS, including UHPLC-HRMS, HRMS coupled with time of flight (TOF) and/or GC-Orbitrap, and flow injection-HRMS - Discusses the current international regulations and legislation related to the use of HRMS in pesticide residue analysis - Features a chapter on the hardware and software available for HRMS implementation - Offers separate chapters on HRMS applied to pesticide residue analysis in fruits and vegetables and in food from animal origin
Author: I. Mikšík
Publisher: Elsevier
ISBN: 0080858686
Category : Science
Languages : en
Pages : 1149
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Book Description
This book deals with chromatographic and electrophoretic methods applied for the separation (quantitation and identification) of biologically relevant compounds. It is assumed that the potential reader is familiar with the basics of chromatographic and electromigration methods. Individual separation modes are dealt with to an extent which follows their applicability for biomedical purposes: liquid chromatography and electromigration methods are therefore highlighted.Each chapter is completed with a list of recent literature covering the 1987-1997 period, which can be used for further guidance of the reader in his/her own field. The chapters have been written by specialists in a particular area and with an emphasis on applications to the biomedical field. This implies that theoretical and instrumental aspects are kept to a minimum which allows the reader to understand the text. Considerable attention is paid to method selection, detection and derivatization procedures and troubleshooting. The majority of examples given represent the analyses of typical naturally-occurring mixtures. Adequate attention is paid to the role of the biological matrix and sample pretreatment, and special attention is given to forensic, toxicological and clinical applications. The book is completed with an extensive Index of Compounds Separated.
Author: Mustafa Soylak
Publisher: Elsevier
ISBN: 0128185708
Category : Science
Languages : en
Pages : 482
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Book Description
New Generation Green Solvents for Separation and Preconcentration of Organic and Inorganic Species is designed to help researchers and students understand the production and application of new generation green solvents in separation- and preconcentration-based analytical methods. Beginning with the historical background and milestones in the development of analytical instrumentation, the book goes on to give a detailed overview of the most up-to-date uses of green solvents in sample preparation. Using a wealth of examples, it compares old and new extraction procedures and explores the many applications of new generation green solvents. Practical, easy-to-follow experiments are used to illustrate the key concepts. This practical guide helps to promote the use of safer, more sustainable solvents in analytical chemistry and beyond for environmental scientists, researchers in pharmaceutical and biotech industries, and students in analytical chemistry. - Covers the basic analytical theory essential for understanding extraction- and microextraction-based separation and preconcentration methods - Explains combination use of new generation solvents with various detection systems, including UV-VIS, ICP-MS, HPLC, LC-MS, GC-MS, and LC-MS/MS - Emphasizes trace chemical component separation, preconcentration and analysis
Author: Sivasankar,
Publisher: OUP India
ISBN: 9780198073918
Category : Technology & Engineering
Languages : en
Pages : 0
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Book Description
Instrumental Methods of Analysis is a textbook designed to introduce various analytical and chemical methods, their underlying principles and applications to the undergraduate engineering students of biotechnology and chemical engineering. This book would also be of interest to students who pursue their B. Sc / M. Sc degree programs in biotechnology and chemistry.
Author: Josep M. Bayona
Publisher: Academic Press
ISBN: 0123813743
Category : Science
Languages : en
Pages : 2998
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Book Description
Comprehensive Sampling and Sample Preparation is a complete treatment of the theory and methodology of sampling in all physical phases and the theory of sample preparation for all major extraction techniques. It is the perfect starting point for researchers and students to design and implement their experiments and support those experiments with quality-reviewed background information. In its four volumes, fundamentals of sampling and sample preparation are reinforced through broad and detailed sections dealing with Biological and Medical, Environmental and Forensic, and Food and Beverage applications. The contributions are organized to reflect the way in which analytical chemists approach a problem. It is intended for a broad audience of analytical chemists, both educators and practitioners of the art and can assist in the preparation of courses as well in the selection of sampling and sample preparation techniques to address the challenges at hand. Above all, it is designed to be helpful in learning more about these topics, as well as to encourage an interest in sampling and sample preparation by outlining the present practice of the technology and by indicating research opportunities. Sampling and Sample preparation is a large and well-defined field in Analytical Chemistry, relevant for many application areas such as medicine, environmental science, biochemistry, pharmacology, geology, and food science. This work covers all these aspects and will be extremely useful to researchers and students, who can use it as a starting point to design and implement their experiments and for quality-reviewed background information There are limited resources that Educators can use to effectively teach the fundamental aspects of modern sample preparation technology. Comprehensive Sampling and Sample Preparation addresses this need, but focuses on the common principles of new developments in extraction technologies rather than the differences between techniques thus facilitating a more thorough understanding Provides a complete overview of the field. Not only will help to save time, it will also help to make correct assessments and avoid costly mistakes in sampling in the process Sample and sample preparation are integral parts of the analytical process but are often less considered and sometimes even completely disregarded in the available literature. To fill this gap, leading scientists have contributed 130 chapters, organized in 4 volumes, covering all modern aspects of sampling and liquid, solid phase and membrane extractions, as well as the challenges associated with different types of matrices in relevant application areas
Author: Colin Poole
Publisher: Elsevier
ISBN: 0323983014
Category : Science
Languages : en
Pages : 692
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Book Description
Instrumental Thin-Layer Chromatography, Second Edition offers a comprehensive source of authoritative information on all aspects of instrumental thin-layer chromatography. The use of short, topic-focused chapters facilitates identifying information of immediate interest for familiar or emerging uses of thin-layer chromatography. The book gives those working in both academia and industry the opportunity to learn, refresh, or deepen their understanding of fundamental and instrumental aspects of thin-layer chromatography, as well as the tools to interpret and manage chromatographic data. The book serves as a practical consolidated guide to the selection of separation conditions and the use of auxiliary techniques. This fully updated new edition restores the contemporary character of the book for those involved in advancing the technology, analyzing data produced, or applying the technique to new application areas. Some chapters have been consolidated to make room for topics not covered in the first edition, reflecting general changes in the field of thin-layer chromatography, especially in effects-directed detection, convenient interfaces for advanced spectroscopic detection, and greater automation possibilities. This book is a valuable reference for anyone who needs to acquire fundamental and practical information to facilitate progress in research and management functions utilizing information acquired by thin-layer chromatography. - Features individual chapters written by recognized authoritative and visionary experts in the field - Provides an overview and focused treatment of a single topic - Provides tables and diagrams with commonly used data to facilitate practical work, comparison of results, and decision-making - Places modern developments in the research literature into a general context not always apparent to inexperienced users of the technique - Offers comprehensive updates to all chapters - Includes new chapters on instrument platforms, effects-directed detection, data analysis tools, small-scale and microfluidic planar separation systems, and applications to the separation of amino acids and peptides, the analysis of saccharides and lipids, and forensic analysis
Author: Alexandre A. Shvartsburg
Publisher: CRC Press
ISBN: 9781420051070
Category : Science
Languages : en
Pages : 322
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Book Description
Over the last decade, scientific and engineering interests have been shifting from conventional ion mobility spectrometry (IMS) to field asymmetric waveform ion mobility spectrometry (FAIMS). Differential Ion Mobility Spectrometry: Nonlinear Ion Transport and Fundamentals of FAIMS explores this new analytical technology that separates and characterizes ions by the difference between their mobility in gases at high and low electric fields. It also covers the novel topics of higher-order differential IMS and IMS with alignment of dipole direction. The book relates the fundamentals of FAIMS and other nonlinear IMS methods to the physics of gas-phase ion transport. It begins with the basics of ion diffusion and mobility in gases, covering the main attributes of conventional IMS that are relevant to all IMS approaches. Building on this foundation, the author reviews diverse high-field transport phenomena that underlie differential IMS. He discusses the conceptual implementation and first-principles optimization of FAIMS as a filtering technique, emphasizing the dependence of FAIMS performance metrics on instrumental parameters and properties of ion species. He also explores ion reactions in FAIMS caused by field heating and the effects of inhomogeneous electric field in curved FAIMS gaps. Written by an accomplished scientist in the field, this state-of-the-art book supplies the foundation to understand the new technology of nonlinear IMS methods.
