Application of Mass Spectrometry to the Analysis of Polycyclic Aromatic Hydrocarbons and Related Compounds in the Environment

Application of Mass Spectrometry to the Analysis of Polycyclic Aromatic Hydrocarbons and Related Compounds in the Environment PDF Author: Takeo Sakuma
Publisher:
ISBN:
Category : Gas chromatography
Languages : en
Pages : 650

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Application of Mass Spectrometry to the Analysis of Polycyclic Aromatic Hydrocarbons and Related Compounds in the Environment

Application of Mass Spectrometry to the Analysis of Polycyclic Aromatic Hydrocarbons and Related Compounds in the Environment PDF Author: Takeo Sakuma
Publisher:
ISBN:
Category : Gas chromatography
Languages : en
Pages : 650

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Book Description


Toxicological Profile for Polycyclic Aromatic Hydrocarbons

Toxicological Profile for Polycyclic Aromatic Hydrocarbons PDF Author:
Publisher:
ISBN:
Category : Polycyclic aromatic hydrocarbons
Languages : en
Pages : 500

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Development and Application of Comprehensive Chemical Analytical Methods for the Analysis of Polyaromatic Compounds

Development and Application of Comprehensive Chemical Analytical Methods for the Analysis of Polyaromatic Compounds PDF Author:
Publisher:
ISBN: 9789464230765
Category :
Languages : en
Pages : 190

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Book Description
Polycyclic aromatic hydrocarbons (PAHs) and numerous related polyaromatic compounds (PACs), like substituted PAHs or heterocyclic polyaromatics, are a widespread class of organic compounds originating from natural and anthropogenic sources. During the last century the impact of anthropogenic sources on the emission of PACs has been growing substantially. Nowadays, a rising number of man-made chemicals and unintentionally produced compounds enter the environment. Identification of potentially harmful compounds poses a serious challenge because environmental samples are very complex. Additionally, the „chemical picture” of our environment is changing rapidly. Analysis of complex environmental samples with a rich matrix requires efficient and robust extraction, clean-up and/or fractionation procedures followed by gas- or liquid chromatographic analysis. Gas chromatography in combination with mass spectrometry was the method of choice in my research. The study presented here focuses on the developments in the environmental analysis of PACs with the emphasis on the contaminants of emerging concern (CECs), whereas the standard analysis of PAHs still concentrates on the set of so called 16 EPA PAHs, set in 1976. My research concentrated on the analysis of PACs in complex matrices like sediment and recycled rubber. The developed methods combine target analysis, based on a predefined list of analytes, and screening analysis, aiming at the identification of unrecognized or novel contaminants. These procedures allowed to isolate, identify and quantify a suite of non-priority pollutants, predominantly PACs, present as complex mixtures. The compounds positively identified (with injection of standards) or tentatively identified (with library search) included inter alia a variety of alkylated PAHs, NSO-heterocycles, NSO-substituted PAHs, halogenated-PAHs, and others. Environmental samples, like polluted sediments, contain thousands of compounds that cannot be chromatographically r

Large (C> = 24) Polycyclic Aromatic Hydrocarbons

Large (C> = 24) Polycyclic Aromatic Hydrocarbons PDF Author: John C. Fetzer
Publisher: John Wiley & Sons
ISBN: 9780471363545
Category : Science
Languages : en
Pages : 308

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Book Description
Polycyclische aromatische Kohlenwasserstoffe (PAHs) gehören zu den ersten Chemikalien, die als krebserregend für den Menschen erkannt wurden. Erstmals werden in diesem Buch PAHs mit mehr als sieben Ringen auf modernem Stand systematisch abgehandelt. Spezielle Kapitel beschäftigen sich mit Probenvorbereitung und -handling; auch ein Vergleich verschiedener Analyseverfahren ist enthalten. Besonders nützlich für den Laboralltag ist ein ausführlicher Anhang mit Strukturformeln sowie UV-Absorptions- und Fluoreszenz-Emissionsspektren von fast 50 Verbindungen.

Chromatographic Analysis of the Environment

Chromatographic Analysis of the Environment PDF Author: Leo M.L. Nollet
Publisher: CRC Press
ISBN: 1315316196
Category : Technology & Engineering
Languages : en
Pages : 650

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Book Description
This detailed handbook covers different chromatographic analysis techniques and chromatographic data for compounds found in air, water, and soil, and sludge. The new edition outlines developments relevant to environmental analysis, especially when using chromatographic mass spectrometric techniques. It addresses new issues, new lines of discussion, and new findings, and develops in greater detail the aspects related to chromatographic analysis in the environment. It also includes different analytical methodologies, addresses instrumental aspects, and outlines conclusions and perspectives for the future.

PAHs and Related Compounds

PAHs and Related Compounds PDF Author: Alasdair H. Neilson
Publisher: Springer Science & Business Media
ISBN: 9783540634225
Category : Medical
Languages : en
Pages : 420

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Book Description
The volumes 3/I and 3/J present a modern account of polycyclic aromatic hydrocarbons (PAHs) and their heterocyclic analogs in the environment. The authors are internationally well recognized scientists belonging to those working presently in the frontline of the different subfields of this interdisciplinary area of environmental science; they give an integrated thorough overview on this hot topic. Extensive cross-referencing between chapters provides the readers with an easy access to all major areas. Due to the huge amount of material the text is published in two volumes (3/I and 3/J). It is expected that both volumes will soon become a major source of information and inspiration for all researchers actively working in PAH environmental chemistry or ecology.

Petrogenic Polycyclic Aromatic Hydrocarbons in the Aquatic Environment: Analysis, Synthesis, Toxicity and Environmental Impact

Petrogenic Polycyclic Aromatic Hydrocarbons in the Aquatic Environment: Analysis, Synthesis, Toxicity and Environmental Impact PDF Author: Daniela M. Pampanin
Publisher: Bentham Science Publishers
ISBN: 1681084279
Category : Science
Languages : en
Pages : 245

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Book Description
Although a lot is known about the influence of Polycyclic Aromatic Hydrocarbons (PAHs) on the marine environment, there are still many unanswered questions. Petrogenic Polycyclic Aromatic Hydrocarbons in the Aquatic Environment is a monograph that sums up basic knowledge about this topic while highlighting current research practices useful in studying the aquatic environment. It starts with an introduction to effect of PAH in the marine environment. It then proceeds to provide information on techniques to monitor PAH levels and investigate the affected environment in order to control the subsequent negative effects. Chapters also detail the carcinogenic and endocrine effects of PAHs on fish as well as the degradation of PAHs by microorganisms. This monograph is a useful reference for environmental science students and professionals learning about the role of PAH in the marine environment.

Mass Spectrometry of Priority Pollutants

Mass Spectrometry of Priority Pollutants PDF Author: Brian Middleditch
Publisher: Springer Science & Business Media
ISBN: 1468437887
Category : Science
Languages : en
Pages : 316

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Book Description
When the list of organic priority pollutants was first published, many mass spec troscopists went scrambling to their reference books. GC-MS was mandated for the analysis of 114 compounds, yet the spectra of many of them, if they had been recorded at all, were scattered throughout the literature. Moreover, it soon became apparent that, even if a sufficient number of instruments could be made available to undertake the task of monitoring 114 substances in the effluents of 21 categories of industry, the personnel could not be trained to perform the analyses and interpret the results. The solution to this problem has been the development of highly automated mass spectrometers which can be operated by personnel without the traditional research training. This book is for the new breed of mass spectroscopist who is not interested in the esoteric details of mass spectral fragmentation, but who merely wishes to identify specific pollutants in effluents. Our inclusion of com prehensive lists of synonyms and bibliographic data should make the book of even greater value to the reader who is not too familiar with the idiosyncrasies of chemical nomenclature and the scientific literature. The experienced mass spectroscopist should also benefit from having all of the data collected together in one volume. This is a book to be used, rather than deposited in a library distant from the laboratory: we would hope that it will fmd a place on top of every mass spectrometer used for the analysis of priority pollutants.

Analytical Chemistry of Polycyclic Aromatic Compounds

Analytical Chemistry of Polycyclic Aromatic Compounds PDF Author: Milton Lee
Publisher: Elsevier
ISBN: 0323149030
Category : Science
Languages : en
Pages : 475

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Book Description
Analytical Chemistry of Polycyclic Aromatic Compounds focuses on the chemical and physical properties of the polycyclic aromatic compounds, critically evaluating various chromatographic and spectroscopic methods. This book discusses how gas chromatography and high-performance liquid chromatography can be both competitive and complementary analytical methods. Ancillary techniques of both are emphasized for the structural elucidation of individual polycyclic aromatic compounds in complex mixtures. The merits of spectroscopic methods in both structural work and quantitation are also described. This text likewise provides background information concerning the chemistry, occurrence, and toxicology of polycyclic aromatic compounds, including the isolation of polycyclic aromatic compounds from a wide variety of materials and matrices. This publication is recommended to scientists involved with the study of polycyclic aromatic compounds, analysts who need to acquire routine data, and individuals charged with formulating environmental policies and drafting regulations.

PAHs and Related Compounds

PAHs and Related Compounds PDF Author: Alasdair N. Neilson
Publisher: Springer
ISBN: 3540496971
Category : Medical
Languages : en
Pages : 431

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Book Description
Environmental Chemistry is a relatively young science. Interest in this subject, however, is growing very rapidly and, although no agreement has been reached as yet about the exact content and limits of this interdisciplinary discipline, there appears to be increasing interest in seeing environmental topics which are based on chemistry embodied in this subject. One of the first objectives of Environ mental Chemistry must be the study of the environment and of natural chemical processes which occur in the environment. A major purpose of this series on Environmental Chemistry, therefore, is to present a reasonably uniform view of various aspects of the chemistry of the environment and chemical reactions occurring in the environment. The industrial activities of man have given a new dimension to Environ mental Chemistry. We have now synthesized and described over five million chemical compounds and chemical industry produces about hundred and fifty million tons of synthetic chemicals annually. We ship billions of tons of oil per year and through mining operations and other geophysical modifications, large quantities of inorganic and organic materials are released from their natural deposits. Cities and metropolitan areas of up to 15 million inhabitants produce large quantities of waste in relatively small and confined areas. Much of the chemical products and waste products of modern society are released into the environment either during production, storage, transport, use or ultimate disposal. These released materials participate in natural cycles and reactions and frequently lead to interference and disturbance of natural systems.