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Author: Alessandro D'Ulivo
Publisher: Elsevier
ISBN: 0323858422
Category : Science
Languages : en
Pages : 477
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Book Description
Vapor Generation Techniques for Trace Element Analysis: Fundamental Aspects provides an overview and discussion of the fundamental aspects governing derivatization reactions of trace-level elements for analytical purposes. Vapor generation techniques coupled with atomic or mass spectrometry have been employed for over 50 years, but their popularity has dramatically increased in recent years, especially as alternative vapor generation approaches have been developed. This book bridges the knowledge gap of the derivatization mechanisms that yield volatile compounds and provides an update on recent developments in vapor generation techniques used for the determination and speciation of trace elements by atomic optical and mass spectrometry. It will serve as a comprehensive, single-source overview of recent developments, providing readers with an understanding of the correct implementation—and limitations—of applying vapor generation techniques to everyday analytical problems facing the trace element analyst. - Covers reaction mechanisms and fundamental processes of vapor generation in detail - Includes classical and alternative vapor generation approaches: alkylation, chelation, plasma, photochemical and electrochemical - Guides the interpretation of experimental results and implementation of vapor generation techniques in the laboratory
Author: Alessandro D'Ulivo
Publisher: Elsevier
ISBN: 0323858422
Category : Science
Languages : en
Pages : 477
Get Book Here
Book Description
Vapor Generation Techniques for Trace Element Analysis: Fundamental Aspects provides an overview and discussion of the fundamental aspects governing derivatization reactions of trace-level elements for analytical purposes. Vapor generation techniques coupled with atomic or mass spectrometry have been employed for over 50 years, but their popularity has dramatically increased in recent years, especially as alternative vapor generation approaches have been developed. This book bridges the knowledge gap of the derivatization mechanisms that yield volatile compounds and provides an update on recent developments in vapor generation techniques used for the determination and speciation of trace elements by atomic optical and mass spectrometry. It will serve as a comprehensive, single-source overview of recent developments, providing readers with an understanding of the correct implementation—and limitations—of applying vapor generation techniques to everyday analytical problems facing the trace element analyst. - Covers reaction mechanisms and fundamental processes of vapor generation in detail - Includes classical and alternative vapor generation approaches: alkylation, chelation, plasma, photochemical and electrochemical - Guides the interpretation of experimental results and implementation of vapor generation techniques in the laboratory
Author: Zoltan Mester
Publisher: Elsevier
ISBN: 0080545483
Category : Science
Languages : en
Pages : 1339
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Book Description
Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation.- First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.
Author: Zeev B. Alfassi
Publisher: Wiley-VCH
ISBN:
Category : Science
Languages : en
Pages : 632
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Book Description
Determination of Trace Elements Edited by Zeev B. Alfassi The best way to determine trace elements! This easy-to-use handbook guides the reader through the maze of all modern analytical operations. Each method is described by an expert in the field. The book highlights the advantages and disadvantages of individual techniques and enables pharmacologists, environmentalists, material scientists, and food industry to select a judicious procedure for their trace element analysis.
Author: de la Guardia
Publisher: John Wiley & Sons
ISBN: 111865434X
Category : Technology & Engineering
Languages : en
Pages : 792
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Book Description
Mineral elements are found in foods and drink of all differenttypes, from drinking water through to mothers’ milk. Thesearch for mineral elements has shown that many trace andultratrace-level elements presented in food are required for ahealthy life. By identifying and analysing these elements, it ispossible to evaluate them for their specific health-givingproperties, and conversely, to isolate their less desirableproperties with a view to reducing or removing them altogether fromsome foods. The analysis of mineral elements requires a number ofdifferent techniques – some methods may be suitable for onefood type yet completely unsuited to another. The Handbook of Mineral Elements in Food is the firstbook to bring together the analytical techniques, the regulatoryand legislative framework, and the widest possible range of foodtypes into one comprehensive handbook for food scientists andtechnologists. Much of the book is based on the authors’ owndata, most of which is previously unpublished, making theHandbook of Mineral Elements in Food a vital andup-to-the-minute reference for food scientists in industry andacademia alike. Analytical chemists, nutritionists and food policymakers will also find it an invaluable resource. Showcasing contributions from international researchers, andconstituting a major resource for our future understanding of thetopic, the Handbook of Mineral Elements in Food is anessential reference and should be found wherever food science andtechnology are researched and taught.
Author: Nelu Grinberg
Publisher: CRC Press
ISBN: 1482218682
Category : Medical
Languages : en
Pages : 991
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Book Description
This handbook is a guide for workers in analytical chemistry who need a starting place for information about a specific instrumental technique. It gives a basic introduction to the techniques and provides leading references on the theory and methodology for an instrumental technique. This edition thoroughly expands and updates the chapters to include concepts, applications, and key references from recent literature. It also contains a new chapter on process analytical technology.
Author: Henryk Matusiewicz
Publisher: Walter de Gruyter GmbH & Co KG
ISBN: 3110366738
Category : Science
Languages : en
Pages : 460
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Book Description
Highly accurate chemical speciation is of great importance in environmental, clinical, and food sciences, as well as in archaeometry. Trace analysis via atomic spectrometry, mass spectroscopy, gas chromatography, electron microprobing, or X-ray absorption spectroscopy provides detailed information on surface and sub-surface domain of samples. The book comprehensively presents modern techniques, timely application, and data modeling.
Author: Zeev Alfassi
Publisher: CRC Press
ISBN: 9780849352133
Category : Science
Languages : en
Pages : 490
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Book Description
Accurate determination of trace elements is critical in various fields of science and technology. Direct measurement of trace elements in samples with complex matrices is often impractical, either due to analytical sensitivity limitations or matrix interferences. Preconcentration procedures are generally needed to eliminate matrix interferences and/or enrich minute amounts of analytes to a level for reliable measurements. Preconcentration Techniques for Trace Elements provides up-to-date information on various preconcentration techniques and detailed discussions regarding such topics as the dissolution of matrices, coprecipitation, solvent extraction, electrochemical means, ion exchange, sorption, chromatographic methods, flotation, membranes, volatization, polymer foam sorbents, fire assay, isotachophoresis, and filter papers. This comprehensive volume, featuring contributions from 21 experts from nine countries, will provide valuable reference material for all scientists and technicians dealing with trace analysis of real-world samples.
Author: Tuan Vo-Dinh
Publisher: CRC Press
ISBN: 0203008995
Category : Medical
Languages : en
Pages : 1864
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Book Description
A wide variety of biomedical photonic technologies have been developed recently for clinical monitoring of early disease states; molecular diagnostics and imaging of physiological parameters; molecular and genetic biomarkers; and detection of the presence of pathological organisms or biochemical species of clinical importance. However, available in
Author: R. D. Reeves
Publisher: John Wiley & Sons
ISBN:
Category : Science
Languages : en
Pages : 440
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Book Description
Covers the entire sequence of processes necessary in the analysis of geological materials for trace elements. It provides: sampling techniques and physical and chemical methods of sample pretreatment; methods of chemical attack and of separation techniques including ion exchange, solvent extraction, coprecipitation, volatilization, and chromatographic methods; information on elemental abundance data and standard rock materials.
Author: Food and Agriculture Organization of the United Nations
Publisher: Food & Agriculture Org.
ISBN: 925134812X
Category : Technology & Engineering
Languages : en
Pages : 324
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Book Description
Food safety is an important global public health and trade matter, with chemical hazards occupying centre stage due to associated acute and chronic health outcomes. There is also an increasing need to address antimicrobial resistance concerns. While food remains a major vehicle for exposure to these hazards, related matrices cannot be ignored. Animal feed for instance may contain drug or pesticide residues as well as mycotoxins that could carry-over to food either as parent compounds or their metabolites of toxicological relevance. Contaminated water is also another medium of potential exposure to food hazards. A concerted effort is required to address the need for a safe food supply and one critical stakeholder is the testing laboratory. While this requires trained and capable analysts as well as reliable instrumentation, analytical methods are a major need. Development and validation – to ensure fitness of purpose – and availability of these methods is a necessity. This manual, consisting of several Standard Operating Procedures (SOPs), presents another opportunity for laboratories to address gaps in analytical methods and/or expand their options. The manual contains techniques for analyzing certain mycotoxins such as aflatoxins, fumonisin and ochratoxin in matrices that include milk, edible vegetable oil and animal feed etc. A range of veterinary drug residues including permitted and prohibited substances in animal matrices including fish, are also addressed. Several pesticide residues in cereals, fruits and vegetables are also covered. A couple of methods for analysis of selected metals are also presented.
