Thin-Layer Chromatography for Binding Media Analysis PDF Download
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Author: Mary F. Striegel
Publisher: Getty Publications
ISBN: 0892363908
Category : Art
Languages : en
Pages : 188
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Book Description
In the study and conservation of art and artifacts, natural organic materials are frequently encountered in components such as coatings, binders, and adhesives. The identification of these materials is often crucial to the attempt to characterize the technologies employed by artists or craftspeople, understand the processes and causes of deterioration, and plan appropriate conservation treatments. Yet the limited resources of many conservation laboratories put many analysis techniques beyond their reach. Thin-layer chromatography can help fill this gap. The volume consists of a handbook, protocols, and guide to reference materials. The handbook serves as a primer for the basic application of thin-layer chromatography to the analysis of binding media, adhesives, and coatings found on cultural objects; the protocols provide step-by-step instructions for the laboratory procedures involved in typical analyses; and the guide to reference materials aids in the understanding of the types of materials and documentation needed for accurate analyses by thin-layer chromatography.
Author: Mary F. Striegel
Publisher: Getty Publications
ISBN: 0892363908
Category : Art
Languages : en
Pages : 188
Get Book Here
Book Description
In the study and conservation of art and artifacts, natural organic materials are frequently encountered in components such as coatings, binders, and adhesives. The identification of these materials is often crucial to the attempt to characterize the technologies employed by artists or craftspeople, understand the processes and causes of deterioration, and plan appropriate conservation treatments. Yet the limited resources of many conservation laboratories put many analysis techniques beyond their reach. Thin-layer chromatography can help fill this gap. The volume consists of a handbook, protocols, and guide to reference materials. The handbook serves as a primer for the basic application of thin-layer chromatography to the analysis of binding media, adhesives, and coatings found on cultural objects; the protocols provide step-by-step instructions for the laboratory procedures involved in typical analyses; and the guide to reference materials aids in the understanding of the types of materials and documentation needed for accurate analyses by thin-layer chromatography.
Author: Bernd Spangenberg
Publisher: Springer Science & Business Media
ISBN: 364210729X
Category : Science
Languages : en
Pages : 399
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Book Description
Thin-layer chromatography (TLC) is widely used particularly for pharmaceutical and food analysis. While there are a number of books on the qualitative identification of chemical substances by TLC, the unique focus here is on quantitative analysis. The authors describe all steps of the analytical procedure, beginning with the basics and equipment for quantitative TLC followed by sample pretreatment and sample application, development and staining, scanning, and finally statistical and chemometric data evaluation and validation. An important feature is the coverage of effect-directed biological detection methods. Chapters are organized in a modular fashion facilitating the easy location of information about individual procedural steps.
Author: Lukasz Komsta
Publisher: CRC Press
ISBN: 1466507152
Category : Medical
Languages : en
Pages : 1070
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Book Description
Used routinely in drug control laboratories, forensic laboratories, and as a research tool, thin layer chromatography (TLC) plays an important role in pharmaceutical drug analyses. It requires less complicated or expensive equipment than other techniques, and has the ability to be performed under field conditions. Filling the need for an up-to-date, complete reference, Thin Layer Chromatography in Drug Analysis covers the most important methods in pharmaceutical applications of TLC, namely, analysis of bulk drug material and pharmaceutical formulations, degradation studies, analysis of biological samples, optimization of the separation of drug classes, and lipophilicity estimation. The book is divided into two parts. Part I is devoted to general topics related to TLC in the context of drug analysis, including the chemical basis of TLC, sample pleparation, the optimization of layers and mobile phases, detection and quantification, analysis of ionic compounds, and separation and analysis of chiral substances. The text addresses the newest advances in TLC instrumentation, two-dimensional TLC, quantification by slit scanning densitometry and image analysis, statistical processing of data, and various detection and identification methods. It also describes the use of TLC for solving a key issue in the drug market—the presence of substandard and counterfeit pharmaceutical products. Part II provides an in-depth overview of a wide range of TLC applications for separation and analysis of particular drug groups. Each chapter contains an introduction about the structures and medicinal actions of the described substances and a literature review of their TLC analysis. A useful resource for chromatographers, pharmacists, analytical chemists, students, and R&D, clinical, and forensic laboratories, this book can be utilized as a manual, reference, and teaching source.
Author: Juan Manuel Madariaga
Publisher: Royal Society of Chemistry
ISBN: 178801524X
Category : Art
Languages : en
Pages : 319
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Book Description
Reviewing the analytical strategies used in the study of cultural heritage assets, this book pays particular attention to analytical methodology and ensuring reliable results are obtained for those working in conservation practice.
Author: Iva Rezić
Publisher: Cambridge Scholars Publishing
ISBN: 1527579352
Category : Art
Languages : en
Pages : 215
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Book Description
This book utilizes current scientific advances to better understand the principles of degradation of historical textile materials (including ancient mummies, dresses, jewellery and musical instruments) and their characterisation. Moreover, it highlights the importance of multidisciplinary procedures as a part of complex task when only a relatively low amount of materials are available for analysis. In such cases, only sensitive, selective and reliable analytical procedures, such as microscopy, spectroscopy and chromatography, can be applied in the characterization of precious materials. As this book explores current scientific advances to better understand the principles of materials characterisation, it is of broad general interest to the general public, but also to the chemical, anthropological and conservation-restoration communities. Moreover, it also offers particular support to a global audience interested in the preservation of historical materials.
Author: Joyce Hill Stoner
Publisher: Routledge
ISBN: 1136000410
Category : Antiques & Collectibles
Languages : en
Pages : 917
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Book Description
Conservation of Easel Paintings is the first comprehensive text on the history, philosophy, and methods of treatment of easel paintings that combines both theory with practice. With contributions from an international group of experts and interviews with important artists, this volume provides an all-encompassing guide to necessary background knowledge in technical art history, artists' materials, scientific methods of examination and documentation, with sections that present varying approaches and methods for treatment, including consolidation, lining, cleaning, retouching, and varnishing. The book concludes with a section featuring issues of preventive conservation, storage, shipping, exhibition, lighting, safety issues, and public outreach. Conservation of Easel Paintings is a crucial resource in the training of conservation students and will provide generations of practicing paintings conservators and interested art historians, curators, directors, collectors, dealers, artists, and students of art and art history with invaluable information and guidance.
Author: Colin Poole
Publisher: Elsevier
ISBN: 0323983014
Category : Science
Languages : en
Pages : 692
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Book Description
Instrumental Thin-Layer Chromatography, Second Edition offers a comprehensive source of authoritative information on all aspects of instrumental thin-layer chromatography. The use of short, topic-focused chapters facilitates identifying information of immediate interest for familiar or emerging uses of thin-layer chromatography. The book gives those working in both academia and industry the opportunity to learn, refresh, or deepen their understanding of fundamental and instrumental aspects of thin-layer chromatography, as well as the tools to interpret and manage chromatographic data. The book serves as a practical consolidated guide to the selection of separation conditions and the use of auxiliary techniques. This fully updated new edition restores the contemporary character of the book for those involved in advancing the technology, analyzing data produced, or applying the technique to new application areas. Some chapters have been consolidated to make room for topics not covered in the first edition, reflecting general changes in the field of thin-layer chromatography, especially in effects-directed detection, convenient interfaces for advanced spectroscopic detection, and greater automation possibilities. This book is a valuable reference for anyone who needs to acquire fundamental and practical information to facilitate progress in research and management functions utilizing information acquired by thin-layer chromatography. - Features individual chapters written by recognized authoritative and visionary experts in the field - Provides an overview and focused treatment of a single topic - Provides tables and diagrams with commonly used data to facilitate practical work, comparison of results, and decision-making - Places modern developments in the research literature into a general context not always apparent to inexperienced users of the technique - Offers comprehensive updates to all chapters - Includes new chapters on instrument platforms, effects-directed detection, data analysis tools, small-scale and microfluidic planar separation systems, and applications to the separation of amino acids and peptides, the analysis of saccharides and lipids, and forensic analysis
Author: Paul Garside
Publisher: Royal Society of Chemistry
ISBN: 1788010930
Category : Art
Languages : en
Pages : 503
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Book Description
With contributions by scientists working in the museum and heritage sector, this textbook provides an overview of the analytical techniques and data processing methods used in modern conservation science.
Author: Ingo Klöckl
Publisher: Walter de Gruyter GmbH & Co KG
ISBN: 3110777282
Category : Science
Languages : en
Pages : 923
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Book Description
Volume 1 of the Handbook of Colorants Chemistry comprehensively covers the fundamentals of color as well as the underlying scientifi c principles, via the presentation of molecular compositions of inorganic and organic pigments. The author explains the chemical and physical production of color and the infl uence of the physical-geometric pigment parameters on the color shade. This volume also deals with historical and modern pigments, dyes, and binders, as well as their mode of action. The complementary “Volume 2: in Painting, Art and Inks” (ISBN 978-3-11-077700-0) focuses on paints, painting and drawing systems used by the painter and craftsman. The book is supplemented by a comprehensive bibliography with references to standard works, monographs, and original papers. The reader is provided with a unique overview of the fi eld of color chemistry.
Author: John Mills
Publisher: Routledge
ISBN: 113600002X
Category : Antiques & Collectibles
Languages : en
Pages : 222
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Book Description
'The Organic Chemistry of Museum Objects' makes available in a single volume, a survey of the chemical composition, properties and analysis of the whole range of organic materials incorporated into objects and artworks found in museum collections. The authors cover the fundamental chemistry of the bulk materials such as wood, paper, natural fibres and skin products, as well as that of the relatively minor components incorporated as paint, media, varnishes, adhesives and dyes. This expanded second edition, now in paperback, follows the structure of the first, though it has been extensively updated. In addition to chapters on basic organic chemistry, analytical methods, analytical findings and fundamental aspects of deterioration, the subject matter is grouped as far as possible by broad chemical class - oils and fats, waxes, bitumens, carbohydrates, proteins, natural resins, dyestuffs and synthetic polymers. This is an essential purchase for all practising and student conservators, restorers, museum scientists, curators and organic chemists.
