The Application of Centrifugation to Polymer Fractionation PDF Download
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Author: Andrew James Manning
Publisher:
ISBN:
Category : Centrifugation
Languages : en
Pages : 360
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Book Description
Author: Andrew James Manning
Publisher:
ISBN:
Category : Centrifugation
Languages : en
Pages : 360
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Book Description
Author: Frieder Francuskiewicz
Publisher: Springer Science & Business Media
ISBN: 3642787045
Category : Science
Languages : en
Pages : 230
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Book Description
Fractionation of polymers via solubility has been a well known method in polymer characterization for a long time. The original object of analytical fractionations, the determination of the molecular weight distribution, is nowadays achieved more efficiently and conveniently by chromatographic methods. However, fractionation procedures, which were developed in great diversity, remain up~to-date and essential for obtaining preparative fractions with narrow distributions. Such fractions are wanted increasingly for the investigation of true structure-property relationships which are mostly influ~ enced by distributions of molecular weight or other parameters such as branching or chemical composition. Literature on the field of polymer fractionation is extensive and several reviews exist. However, there is a lack of systematically methodical instruc tions for carrying-out of diverse fractionation procedures. This volume repre sents an attempt to reduce this deficiency and is focussed on practical aspects of fractionation procedures. This laboratory manual is intended for polymer chemists, physicists, and technicians, for students of polymer science, and skilled laboratory assistants, all of whom are not dealing directly with fractionation but are in need of fractions to carry out further investigations.
Author: Manfred J. R. Cantow
Publisher: Elsevier
ISBN: 1483271706
Category : Science
Languages : en
Pages : 540
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Book Description
Polymer Fractionation focuses on the processes, reactions, and transformations involved in polymer fractionation, including chromatography, titration, and sedimentation. The selection first offers information on theoretical considerations and fractional precipitation. Topics include polydispersity of high polymers, phase relations for polydisperse systems, fractionation theory and efficiency, and fractionation by solvent evaporation. The manuscript then takes a look at fractional solution, chromatographic fractionation, and gel permeation chromatography. The book elaborates on thermal diffusion and turbidimetric titration, as well as methods of fractionation, studies of the variables, outline of the method and range of application, and elaboration of the method. The text then ponders on sedimentation, isothermal diffusion, and summative fractionation. Discussions focus on mathematical interpretation of summative data, experimental methods for the determination of diffusion constants, and methods for the determination of the diffusion coefficient distribution. The selection is a valuable source of information for readers interested in polymer fractionation.
Author: Walter Maechtle
Publisher: Springer Science & Business Media
ISBN: 3540262180
Category : Technology & Engineering
Languages : en
Pages : 249
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Book Description
This book is divided into chapters covering instrumentation, sedimentation velocity runs, density gradient runs, application examples and future developments. In particular, the detailed application chapter demonstrates the versatility and power of AUC by means of many interesting and important industrial examples. Thus the book concentrates on practical aspects rather than details of centrifugation theory.
Author: John M. Graham
Publisher: Oxford University Press
ISBN: 0199634947
Category : Medical
Languages : en
Pages : 360
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Book Description
In the fast changing world of cell biology it is often required that particular membranes or subcellular organisms be isolated from the structure for investigative purposes. This book shows how to do this in a practical, hands-on way.
Author: G.D. Birnie
Publisher: Butterworth-Heinemann
ISBN: 1483278417
Category : Science
Languages : en
Pages : 340
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Book Description
Centrifugal Separations in Molecular and Cell Biology focuses on the application of modern centrifugation technology in molecular and cell biology, including the separation and fractionation of biological particles by centrifugation on the preparative and analytical scales. The selection first covers the principles and practices of centrifugation and the bases of centrifugal separations. Discussions focus on the basic concepts of sedimentation theory, centrifugation methods, designing centrifugation experiments, care of centrifuges and rotors, and statistical estimation of molecular parameters. The book also ponders on the practical aspects of rate-zonal centrifugation, including gradient materials, density and viscosity of glycerol solutions, and resolution and gradient shape. The publication examines fractionations in zonal rotors and the quantitative aspects of rate-zonal centrifugation. The text then reviews isopycnic centrifugation in ionic media and analytical centrifugation. Topics include separation by isopycnic banding, large-scale preparative procedures, and density-gradient solutes. The selection is a valuable reference for readers interested in centrifugation technology.
Author: Martin E. Schimpf
Publisher: John Wiley & Sons
ISBN: 9780471184300
Category : Science
Languages : en
Pages : 618
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Book Description
Field flow fractionation (FFF) is an emerging separation technique, which has been proven successful in the analysis of pharmaceuticals, biotechnology products, polymers, soils, and foods, among others. In this book, Martin Schimpf joins forces with Karin Caldwell and J. Calvin Giddings, two of the primary developers of this technique, to bring you the first comprehensive, one-stop reference on the technique.
Author:
Publisher:
ISBN:
Category : Rubber
Languages : en
Pages : 504
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Book Description
Author: Wallace Woon-Fong Leung
Publisher: Butterworth-Heinemann
ISBN: 0081026358
Category : Technology & Engineering
Languages : en
Pages : 503
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Book Description
Centrifugal Separations in Biotechnology, Second Edition, is the only book on the market devoted to centrifugal separation in biotechnology. Key topics covered include a full introduction to centrifugation, sedimentation and separation; detailed coverage of centrifuge types, including batch and semi-batch centrifuges, disk-stack and tubular decanter centrifuges; methods for increasing solids concentration; laboratory and pilot testing of centrifuges; selection and sizing centrifuges; scale-up of equipment, performance prediction and analysis of test results using numerical simulation. Centrifugal Separations in Biotechnology, Second Edition, provides guidance on troubleshooting and optimizing centrifuges, and then goes on to explore the commercial applications of centrifuges in biotechnology. It gives detailed process information and data to assist in the development of particular processes from existing systems. It is of value to professionals in the chemical, bioprocess, and biotech sectors, and all those concerned with bioseparation, bioprocessing, unit-operations and process engineering. Provides a comprehensive guide to centrifuges, their optimal development, and their operation in the biotechnology industry Updated throughout based on developments in industrial applications and advances in our understanding of centrifugal separations in biotechnology Discusses applications for the separation of proteins, DNA, mitochondria, ribosomes, lysosomes and other cellular elements Includes new sections on use of optimal polymer dosage in waste treatment, new centrifuge designs for applications in algae processing, biopharma, and more
Author: Serban C. Moldoveanu
Publisher: Elsevier
ISBN: 0323898203
Category : Science
Languages : en
Pages : 698
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Book Description
Modern Sample Preparation for Chromatography, Second Edition explains the principles of sample preparation for chromatographic analysis. A variety of procedures are applied to make real-world samples amenable for chromatographic analysis and to improve results. This book's authors discuss each procedure’s advantages, disadvantages and their applicability to different types of samples, along with their fit for different types of chromatographic analysis. The book contains numerous literature references and examples of sample preparation for different matrices and new sections on green approaches in sample preparation, progress in automation of sample preparation, non-conventional solvents for LLE (ionic liquids, deep eutectic mixtures, and others), and more. Presents numerous techniques applied for sample preparation for chromatographic analysis Provides an up-to-date source of information regarding the progress made in sample preparation for chromatography Describes examples for specific types of matrices, providing a guide for choosing the appropriate sample preparation method for a given analysis
