Synthesis and Characterization of Some Molybdenum Organophosphonates and Related Compounds PDF Download
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Author: Sylvia Tan
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ISBN:
Category : Molybdenum compounds
Languages : en
Pages : 422
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Author: Sylvia Tan
Publisher:
ISBN:
Category : Molybdenum compounds
Languages : en
Pages : 422
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Author: William Winder Beers
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Languages : en
Pages : 276
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Languages : en
Pages :
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Author: Nancy J. Christensen
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Category : Diolefins
Languages : en
Pages : 356
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Languages : en
Pages :
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Investigation into the direct synthesis of Mo4Cl(P(C2H5)3)4 from Mo2(OAc)4 led to a synthetic procedure that produces yields greater than 80%. The single-crystal structure disclosed a planar rectangular cluster of molybdenum atoms. Metal-metal bond distances suggest that the long edges of the rectangular cluster should be considered to be single bonds and the short metal-metal bonds to be triple bonds. This view is reinforced by an extended Hueckel calculation. Attempts to add a metal atom to Mo4Cl(PR3)4 to form Mo5Cl10(PR3)3 led instead to a compound with the composition Mo8Cl16(PR3)4. Solution and reflectance uv-visible spectra and x-ray photoelectron spectra suggest that tetranuclear molybdenum units are present. The facile reaction between Mo8Cl16(PR3)4 and PR3 imply that the linkage between tetrameric units is weak.
Author: Diana Rose Tomchick
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Category :
Languages : en
Pages : 542
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Author: Rabindranath Bissessur
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Category : Molybdenum compounds
Languages : en
Pages : 566
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Author: Deborah Ann Spink
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Category :
Languages : en
Pages : 152
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Author: Michele Lynn Mader
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Category :
Languages : en
Pages : 0
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Author: Brent Allen Aufdembrink
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Category :
Languages : en
Pages : 556
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