Synthesis and Characterization of Compounds Containing Discrete Tetranuclear Clusters and Extended Arrays of Molybdenum Atoms PDF Download
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Author: Brent Allen Aufdembrink
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Languages : en
Pages : 556
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Author: Brent Allen Aufdembrink
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Category :
Languages : en
Pages : 556
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Category : Power resources
Languages : en
Pages : 760
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Languages : en
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Investigation into the direct synthesis of Mo4Cl(P(C2H5)3)4 from Mo2(OAc)4 led to a synthetic procedure that produces yields greater than 80%. The single-crystal structure disclosed a planar rectangular cluster of molybdenum atoms. Metal-metal bond distances suggest that the long edges of the rectangular cluster should be considered to be single bonds and the short metal-metal bonds to be triple bonds. This view is reinforced by an extended Hueckel calculation. Attempts to add a metal atom to Mo4Cl(PR3)4 to form Mo5Cl10(PR3)3 led instead to a compound with the composition Mo8Cl16(PR3)4. Solution and reflectance uv-visible spectra and x-ray photoelectron spectra suggest that tetranuclear molybdenum units are present. The facile reaction between Mo8Cl16(PR3)4 and PR3 imply that the linkage between tetrameric units is weak.
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Category : Dissertations, Academic
Languages : en
Pages : 670
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Category : Dissertation abstracts
Languages : en
Pages : 696
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Category : Government reports announcements & index
Languages : en
Pages : 964
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Author: Elizabeth Ann Fiore Vogel
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Languages : en
Pages : 104
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Category : Nuclear energy
Languages : en
Pages : 480
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Category : Dissertations, Academic
Languages : en
Pages : 754
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Author: Fabian Mohr
Publisher: John Wiley & Sons
ISBN: 3527320865
Category : Science
Languages : en
Pages : 425
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Written by world-class authors, this most recent major book on the topic highlights new and current trends as well as future directions. It is comprehensive in its scope, covering all aspects of gold chemistry -- from homogeneous to heterogeneous catalysis, from supramolecular assemblies to sensors and medicinal applications. The result is an invaluable work for both organic and inorganic chemists working in universities and industry, as well as material scientists.
