Photoelectron Spectroscopy of Some Inorganic and Organometallic Compounds PDF Download
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Languages : en
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Core electron binding energies were measured for a variety of inorganic and organometallic compounds using gas-phase X-ray photoelectron spectroscopy (XPS). The atomic charge distributions in these molecules are deduced from the binding energies, often leading to a better understanding of the bonding in these compounds. The XPS spectra of fifteen volatile tin compounds were recorded. The data suggest that the metal d orbitals are not significantly involved in the bonding. The oxygen ls XPS spectra of gaseous CH3Mn(CO)5, (.pi.-C5H5Fe(CO)2)2, and Co4(CO)12 can be readily resolved into separate peaks due to bridging and terminal carbonyl groups. The C ls spectrum of Fe(CO)5 consists of a single symmetric peak. The carbonyl ligand core binding energies of transition-metal carbonyl complexes are sensitive to differences in the metal-to-CO ligand bonding. Both C ls and O ls carbonyl binding energies correlate well with average C-O stretching force constants or average C-O stretching frequencies. The metal and carbonyl binding energies in a series of pentacarbonylmanganese complexes LMn(CO)5 are a good measure of the relative electronegativities of the ligands L. High-quality X-ray photoelectron spectra have been obtained for compounds dissolved in glycerin solutions, and aqueous solutions were converted into glycerin solutions which gave good XRSspectra of the solutes. The technique appears promising as a future analytical application of X-ray photoelectron spectroscopy. The shifts in the binding energies of oxygen, chlorine, and carbon atoms in some isoelectronic isostructural compounds can be explained in terms of simple trends in atomic charges.
Author: Jack Yarwood
Publisher: Royal Society of Chemistry
ISBN: 1849732833
Category : Science
Languages : en
Pages : 279
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This series provides an unequalled source of information on an area of chemistry that continues to grow in importance. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in the field, researchers will find this an invaluable source of information on current methods and applications.
Author: Fu Chung Chang
Publisher:
ISBN:
Category : Photoelectron spectroscopy
Languages : en
Pages : 340
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Author: Grant Allan Von Wald
Publisher:
ISBN:
Category :
Languages : en
Pages : 584
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![Photoelectron Spectroscopy of Organometallic Compounds [microform] PDF](https://books.google.com/books/content/images/frontcover/YQYovwEACAAJ?fife=w80-h100)
Author: Jingcun Wu
Publisher: National Library of Canada = Bibliothèque nationale du Canada
ISBN: 9780612286917
Category : Organometallic compounds
Languages : en
Pages : 228
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High resolution gas phase photoelectron spectra are reported for a series of trimethylphosphine substituted tungsten carbonyls and cyclopentadienyl derivatives of indium (CpIn) and thallium (CpTl). The advantages of using monochromatic synchrotron radiation PES for studying the electronic structure of organometallic molecules are demonstrated.
Author: P Day
Publisher: Royal Society of Chemistry
ISBN: 1847555969
Category : Science
Languages : en
Pages : 326
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Specialist Periodical Reports provide systematic and detailed review coverage of progress in the major areas of chemical research. Written by experts in their specialist fields the series creates a unique service for the active research chemist, supplying regular critical in-depth accounts of progress in particular areas of chemistry. For over 80 years the Royal Society of Chemistry and its predecessor, the Chemical Society, have been publishing reports charting developments in chemistry, which originally took the form of Annual Reports. However, by 1967 the whole spectrum of chemistry could no longer be contained within one volume and the series Specialist Periodical Reports was born. The Annual Reports themselves still existed but were divided into two, and subsequently three, volumes covering Inorganic, Organic and Physical Chemistry. For more general coverage of the highlights in chemistry they remain a 'must'. Since that time the SPR series has altered according to the fluctuating degree of activity in various fields of chemistry. Some titles have remained unchanged, while others have altered their emphasis along with their titles; some have been combined under a new name whereas others have had to be discontinued. The current list of Specialist Periodical Reports can be seen on the inside flap of this volume.
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Languages : en
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Author: Luis J. Matienzo
Publisher:
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Category : Organometallic compounds
Languages : en
Pages :
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Author: N N Greenwood
Publisher: Royal Society of Chemistry
ISBN: 1847554938
Category : Science
Languages : en
Pages : 559
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Book Description
Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr
