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Author: Amrut Gaddamwar
Publisher: GRIN Verlag
ISBN: 3656420025
Category : Science
Languages : en
Pages : 212
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Book Description
This book is designed to cover the “Basics principles of practical chemistry” Syllabus of M.Sc, B.Sc level courses and This book embodies eight chapters which are of basic importance in the curriculum of M.Sc chemistry students and provide a core course of organic chemistry, B.Sc for all branches of sciences. Each chapter consists of a methodical introduction, discussion of basic physicochemical principles involved and practical application & significances.Chapter on Organic synthesis contains Preparation of m-Dinitrobenzene, m-Nitroaniline, Hippuric Acid, Azlactone, phthalimide, 2, 4-Dihydroxyacetophenone,Anthracene-Maleicanhydrideadduct Microwave Assisted Synthesis of Aspirin, P-Bromoacetanilide,P-Bromoaniline 2, 4, 6 Tribromoaniline; 1, 3, 5 Tribromobenzene, Aspirin, Tetrahydrocarbazole, 7-Hydroxy4-Methyl Coumarin (Umbelliferon) and Synthesis of Phenyl Indole, 7 Hydroxy-3-Methyl Flavone, 2, 5 Di hydroxy Acetophenone, 4-Chloro Toluene, Benzilic Acid, Benzpinacol, 7-Hydroxy Coumarin, Maleic Anhydride, Benzophenone, Benzanilide, Caprolactam, Vanillyl Alcohol, Ortho and Para Nitro Phenols, Acridone.In chapter two consists of Isolation of Natural product such as Isolation of Piperine from Black-pepper, Caffeine from Tea Leaves, and Cineole from Eucalyptus Leaves. Chapter three is “Drug synthesis” it mainly contains synthesis of Paracetamol, Phenytoin, Benzocaine, Methyl Uracil, chlorbutol, Sulphanilamide, flourescein, Antipyrine Chapter four is Organic mixture analysis explained the binary as well as ternary mixture and solid- solid, solid-liquid, liquid-liquid types of mixture. While chapter five consists of spectral analysis in which UV, visible, NMR, IR etc and different types of chromatographic techniques. In chapter six Estimation of Mg+2 in Soil, Carbonates & Bicarbonates in soil, Ca2+ & Fe3+ in cement sample, Calcium in a Given Tablet and Determination of Chemical Oxygen Demand, Sodium, Potassium, Calcium, Li, Phosphorous In Human Serum, Manganese in Steel, Quinine, by flame photometry; Determination of Riboflavin by Flourometry, Blood Cholesterol by Colorimetry, Blood Glucose Colorimetry chapter seven consist of Assay of Ibuprofen, Analgin, Ascorbic Acid, Sulfanilamide, Riboflavin and Diazepam the last chapter is the “Advanced Applied analysis &Preparations” it consists of Preparation of Urea- Formaldehyde Resin, phenol-formaldehyde resin and Determinations of Acid value of Oil, Viscosity of lubricating oil, Zn2+ ions by complexometric titration.
Author: G. Pass
Publisher: Springer Science & Business Media
ISBN: 9401727449
Category : Science
Languages : en
Pages : 254
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Book Description
In revising the text opportunity has been taken to introduce SI units throughout. An Appendix has been included which contains tables of SI units and a table of conversion factors for use when consulting data in non-SI units. Chapter 19 now includes experiments demon strating the use of ion-exchange and solid-liquid chromatography_ Exercises involving colorimetry have been included in Chapter 17. These techniques are introduced as part of a complementary exercise where their relevance is seen as part of a complete piece of work. Minor improvements have been made to some of the experimental procedures and we are grateful to those who have made helpful suggestions in this respect. G. PASS H. SUTCLIFFE iii Preface to the First Edition The student of inorganic chemistry is fortunate in having a wide choice of textbooks covering the descriptive and theoretical aspects of the sUbject. There is no comparable choice of textbooks covering practical inorganic chemistry. Moreover, there is a tendency for many students to draw an unfortunate distinction between chemistry taught in the lecture room, and laboratory work. Consideration of these points prompted the preparation of this book, in which we have attempted to emphasize the relationship between theory and practice.
Author: R. John Errington
Publisher: CRC Press
ISBN: 1040294227
Category : Science
Languages : en
Pages : 303
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Book Description
While the boundaries between the areas of chemistry traditionally labeled as inorganic, organic and physical are gradually diffusing, the practical techniques adopted by workers in each of these areas are often radically different. The breadth and variety of research classed as "inorganic chemistry" is readily apparent from an inspection of some of the leading international journals, and can be quite daunting for newcomers to this domain who are likely to have only limited experience of the methodologies involved. This book has therefore been written to provide guidance for those unfamiliar with the techniques most often encountered in synthetic inorganic / metalorganic chemistry, with an emphasis on procedures for handling air-sensitive compounds. One chapter is devoted to more specialized techniques such as metal vapor synthesis, and a review of preparative methods for a selection of starting materials is included as an aid to those planning research projects. While this book is aimed primarily at postgraduate and advanced undergraduate students involved in inorganic research projects, synthetic organic chemists and industrial chemists will also find much useful information within its pages. Similarly, it serves as a useful reference source for materials and polymer scientists who wish to take advantage of recent progress in precursor synthesis and catalyst development.
Author: Amrut Gaddamwar
Publisher: GRIN Verlag
ISBN: 3656420025
Category : Science
Languages : en
Pages : 212
Get Book Here
Book Description
This book is designed to cover the “Basics principles of practical chemistry” Syllabus of M.Sc, B.Sc level courses and This book embodies eight chapters which are of basic importance in the curriculum of M.Sc chemistry students and provide a core course of organic chemistry, B.Sc for all branches of sciences. Each chapter consists of a methodical introduction, discussion of basic physicochemical principles involved and practical application & significances.Chapter on Organic synthesis contains Preparation of m-Dinitrobenzene, m-Nitroaniline, Hippuric Acid, Azlactone, phthalimide, 2, 4-Dihydroxyacetophenone,Anthracene-Maleicanhydrideadduct Microwave Assisted Synthesis of Aspirin, P-Bromoacetanilide,P-Bromoaniline 2, 4, 6 Tribromoaniline; 1, 3, 5 Tribromobenzene, Aspirin, Tetrahydrocarbazole, 7-Hydroxy4-Methyl Coumarin (Umbelliferon) and Synthesis of Phenyl Indole, 7 Hydroxy-3-Methyl Flavone, 2, 5 Di hydroxy Acetophenone, 4-Chloro Toluene, Benzilic Acid, Benzpinacol, 7-Hydroxy Coumarin, Maleic Anhydride, Benzophenone, Benzanilide, Caprolactam, Vanillyl Alcohol, Ortho and Para Nitro Phenols, Acridone.In chapter two consists of Isolation of Natural product such as Isolation of Piperine from Black-pepper, Caffeine from Tea Leaves, and Cineole from Eucalyptus Leaves. Chapter three is “Drug synthesis” it mainly contains synthesis of Paracetamol, Phenytoin, Benzocaine, Methyl Uracil, chlorbutol, Sulphanilamide, flourescein, Antipyrine Chapter four is Organic mixture analysis explained the binary as well as ternary mixture and solid- solid, solid-liquid, liquid-liquid types of mixture. While chapter five consists of spectral analysis in which UV, visible, NMR, IR etc and different types of chromatographic techniques. In chapter six Estimation of Mg+2 in Soil, Carbonates & Bicarbonates in soil, Ca2+ & Fe3+ in cement sample, Calcium in a Given Tablet and Determination of Chemical Oxygen Demand, Sodium, Potassium, Calcium, Li, Phosphorous In Human Serum, Manganese in Steel, Quinine, by flame photometry; Determination of Riboflavin by Flourometry, Blood Cholesterol by Colorimetry, Blood Glucose Colorimetry chapter seven consist of Assay of Ibuprofen, Analgin, Ascorbic Acid, Sulfanilamide, Riboflavin and Diazepam the last chapter is the “Advanced Applied analysis &Preparations” it consists of Preparation of Urea- Formaldehyde Resin, phenol-formaldehyde resin and Determinations of Acid value of Oil, Viscosity of lubricating oil, Zn2+ ions by complexometric titration.
Author: Arthur I. Vogel
Publisher:
ISBN:
Category :
Languages : en
Pages : 1188
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Book Description
Author: Carlos A. M. Afonso
Publisher: Royal Society of Chemistry
ISBN: 1849739633
Category : Science
Languages : en
Pages : 976
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Book Description
This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment. Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.
Author: Robert A. Stockland, Jr.
Publisher: John Wiley & Sons
ISBN: 1118612809
Category : Science
Languages : en
Pages : 697
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Book Description
A practical handbook for chemists performing bond forming reactions, this book features useful information on the synthesis of common functional groups in organic chemistry. • Details modern functional group synthesis through carbon-heteroelement (N, O, P, S, B, halogen) bond forming reactions with a focus on operational simplicity and sustainability. • Summarizes key and recent developments – which are otherwise scattered across journal literature – into a single source • Contains over 100 detailed preparations of common functional groups • Included 25 troubleshooting guides with suggestions and potential solutions to common problems. • Complements the text in enhanced ebook editions with tutorial videos where the author provides an introduction to microwave assisted chemistry
Author: Zory Vlad Todres
Publisher: CRC Press
ISBN: 1040202594
Category : Science
Languages : en
Pages : 190
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Book Description
Organic Mechanochemistry and Its Practical Applications gathers physical and organic chemistry-based molecular principles, evolving interpretations of scientific data, and real world applications to demonstrate the synthetic advantages of mechanically initiated organic reactions. This book considers transformations of organic substances upon
Author: V K Ahluwalia, Sunita Dhingra
Publisher: Universities Press
ISBN: 9788173715068
Category :
Languages : en
Pages : 528
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Book Description
Author: Frederick George Mann
Publisher: Orient Blackswan
ISBN: 9788125013808
Category : Analytical chemistry
Languages : en
Pages : 612
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Book Description
A Clear And Reliable Guide To Students Of Practical Organic Chemistry At The Undergraduate And Postgraduate Levels. This Edition S Special Emphasis Is On Semi Micro Methods And Modern Techniques And Reactions.
Author: William Sabel
Publisher: Elsevier
ISBN: 1483213773
Category : Science
Languages : en
Pages : 207
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Book Description
Basic Techniques of Preparative Organic Chemistry covers a detailed guide for carrying out the procedures commonly needed in preparative organic chemistry. The book discusses the nature of organic reactions; the basic principles of preparative organic chemistry; unit operations; and good laboratory practice. The text then provides a review of apparatus and equipment and describes the potential hazards involved in a chemical operation, such as toxicity, bodily injuries, smoking, fire, explosion, and implosion. Techniques and unit operations for carrying out a reaction and for isolating and purifying a reaction product; and the criteria for and methods of assessing purity are also considered. The book further tackles packing and storing products and samples and making reports and communications. Students taking organic chemistry courses will find the text useful.
