Microdiffusion Analysis and Volumetric Error PDF Download

Author: Edward Joseph Conway
Publisher:
ISBN:
Category : Science
Languages : en
Pages : 488

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Book Description
CONTENTS - I. INTRODUCTORY - PART I - APPARATUS AND PRINCIPLES USED IN MICRODIFFUSION ANALYSIS - II. A STANDARD MICRO DIFFUSION APPARATUS OR 'UNIT' - III. FACTORS INFLUENCING THE ABSORPTION RATE FROM OUTER TO INNER CHAMBER WITH SPECIAL REFERENCE TO AMMONIA - IV. GENERAL PRINCIPLES GOVERNING THE ABSORPTION TIME IN MICRO DIFFUSION ANALYSIS - V. PIPETTES (SUITABLE FOR USE WITH THE STANDARD UNITS) AND THEIR DELIVERY ERRORS - VI. MICRO-BURETTES (SUITABLE FOR USE WITH THE STANDARD UNITS) AND ERRORS INVOLVED IN THEIR USE - VII. THE MICRODIFFUSION METHOD WITH END-POINT VOLUMES AROUND 20 CUBIC MILLIMETRES - VII. COLORIMETRY IN THE MICRODIFFUSION METHODS - PART II - DESCRIPTION OF METHODS WITH THE STANDARD UNITS - A. VOLATILE BASES - Aa. Ammonia Group - IX. AMMONIA. GENERAL METHOD USING STANDARD ACID AS ABSORBENT - X. AMMONIA. GENERAL METHOD (USING THE BORIC-HCL PROCEDURE) - XI. SPECIAL FACTORS INFLUENCING THE RATE OF AMMONIA ABSORPTION - XII. OTHER METHODS FOR DETERMINING THE ABSORBED AMMONIA IN THE MICRO DIFFUSION PROCEDURE - XIII. AMMONIA. BIOLOGICAL DETERMINATIONS - XIV. TOTAL NITROGEN (OVER 100 µg N). - XV. TOTAL NITROGEN (UNDER 100 µg N) FURTHER PROCEDURE - XVI. TOTAL NITROGEN (1 TO 0·1 µg N) - XVII. UREA (BLOOD AND URINE) - XVIII. UREA IN TISSUES - XIX. ADENOSINETRIPHOSPHORIC ACID, ADENYLIC ACID, ADENOSINE, ETC. - XX. NITRATE, NITRITE AND AMIDE NITROGEN - XXI. AMIDES (continued). GLUTAMINE - XXII. MONOAMINE OXIDASE AND HISTAMINASE IN TISSUES - Ab. Amine Group - XXIII. DETERMINATION OF VOLATILE AMINES - B. VOLATILE ACIDS - Ba. The Carbon Dioxide Group - XXIV. CARBONATES AND BICARBONATE - XXV. BLOOD GLUCOSE AND FERMENTABLE SUGAR IN NORMAL URINE - XXVI. DETERMINATION OF CARBONIC ANHYDRASE - XXVII. OXIDATION RATES OF ORGANIC SUBSTANCES WITH A STANDARD OXIDANT WITH APPLICATION TO DETERMINATION OF MINUTE AMOUNTS OF CALCIUM AS OXALATE - Bb. 1 Volatile Fatty Acids - XXVIII. ACETIC ACID AND OTHER LOWER FATTY ACIDS - XXIX. ASSAY OF ACETYLCHOLINESTERASE - Bc. Volatile Weak Inorganic Acids and Phenols - XXX. CYANIDE, AZIDE, SULPHIDE, PHENOLS - C. VOLATILE ALCOHOLS - XXXI. METHANOL AND ISOPROPANOL GROUP - XXXII. ETHANOL - XXXIII. ETHANOL FROM URETHANE - D. VOLATILE ALDEHYDES - Da. Formaldehyde Group XXXIV. FORMALDEHYDE - XXXV. FORMALDEHYDOGENIC STEROIDS (PERIODIC ACID AS OXIDANT) - XXXVI. FORMALDEHYDOGENIC STEROIDS (SODIUM BISMUTHATE AS OXIDANT) - XXXVII. GLYCINE (FORMALDEHYDE PRODUCED BY NINHYDRIN OXIDATION) - Db. Acetaldehyde Group XXXVIII. ACETALDEHYDE (SEMICARBAZIDE ABSORPTION) - XXXIX. ACETALDEHYDE FROM LACTIC ACID AND THREONINE WITH BISULPHITE ABSORPTION - E. VOLATILE KETONES - XL. ACETONE (INCLUDING A RAPID CLINICAL METHOD USING THE NESSLER SOLUTION) - F. VARIOUS VOLATILE OXIDISING AND REDUCING SUBSTANCES - Fa. The Halogens - XLI. THE HALOGENS (INTRODUCTORY) - XLII. CHLORIDE (BY OXIDATION TO CHLORINE AND ABSORPTION INTO IODIDE) - XLIII. CHLORIDE (BY OXIDATION TO CHLORINE AND ABSORPTION INTO FAST GREEN) - XLIV. BROMIDE - XLV. IODIDES AND HALOGEN MIXTURES - XLVI. SERIAL DETERMINATION OF ORGANICALLY BOUND HALOGEN - XLVII. VOLATILE HALOGENATED HYDROCARBONS (CHLOROFORM, TRICHLORETHYLENE AND CARBON TETRACHLORIDE) - Fb. Carbon Monoxide - XLVIII. CARBON MONOXIDE - XLIX. A RAPID CLINICAL METHOD FOR CARBON MONOXIDE DETERMINATION - G. VOLATILE SUBSTANCES OF TOXICOLOGICAL INTEREST - L. FELDSTEIN AND KLENDSHOJ'S SYSTEM FOR THE DETERMINATION OF VOLATILE POISONS BY MICRODIFFUSION - H. OTHER MISCELLANEOUS APPLICATIONS OF THE MICRODIFFUSION PRINCIPLE - LI. TOTAL MOLECULAR CONCENTRATION IN FLUID SAMPLES OF ABOUT 3-4 MILLIGRAMS - LII. SEPARATION OF CRYSTALS AND' GUMS' BY MICRODIFFUSION - QUALITATIVE MICRO-DIFFUSION ANALYSIS - LIII. SOME CONSIDERATIONS ON QUALITATIVE MICRO-DIFFUSION ANALYSIS - PART III - THE ERROR OF VOLUMETRIC TITRATION - LIV. INTRODUCTORY - LV. THE VARIABLE GLASS ERROR - LVI. THE TOTAL VARIABLE GLASS ERROR AND ITS CONTROL - LVII. THE VARIABLE CHEMICAL ERROR IN TITRATION - LVIII. THE RATIONALE OF MICRO TITRATION - LIX. THE CONSTANT GLASS ERROR - LX. THE CONSTANT CHEMICAL ERROR - LXI. VOLUMETRIC ERROR IN KJELDAHL NITROGEN ANALYSES - LXIII. UREA EXCRETION AS RENAL FUNCTION TEST - REFERENCES - INDEX OF SUBJECTS -