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Author: Roy H. Bible
Publisher: Springer Science & Business Media
ISBN: 1468482882
Category : Science
Languages : en
Pages : 154
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Book Description
In writing this book I had two main objectives: (1) to teach the organic chemist how to interpret proton magnetic resonance spectra, and (2) to provide the reference data which are constantly needed in the use of proton spectra. I have felt that it was im portant to point out not only the information which can be gained from spectra, but also the limitations and the potential pitfalls. All of the important facts are organized into tabular summaries. Every effort has been made to present the material clearly, con cisely, completely, and accurately. At the same time, subjects not directly related to the interpretation of spectra have been omitted. Thus, while the conclusions drawn from theory are presented, the theory itself has been avoided. There are a number of advantages in learning the empirical facts before learning the theory. First of all, in interpreting spectra one usually has to rely on his knowledge of the accumulated empirical correlations much more than on his knowledge of the theory. In fact, one could know all of the theory and still not b~ able to interpret spectra unless he also knew the empirical facts. Secondly, the theory is much more easilyunderstoodafter the facts have been mastered.
Author: Roy H. Bible
Publisher: Springer Science & Business Media
ISBN: 1468482882
Category : Science
Languages : en
Pages : 154
Get Book Here
Book Description
In writing this book I had two main objectives: (1) to teach the organic chemist how to interpret proton magnetic resonance spectra, and (2) to provide the reference data which are constantly needed in the use of proton spectra. I have felt that it was im portant to point out not only the information which can be gained from spectra, but also the limitations and the potential pitfalls. All of the important facts are organized into tabular summaries. Every effort has been made to present the material clearly, con cisely, completely, and accurately. At the same time, subjects not directly related to the interpretation of spectra have been omitted. Thus, while the conclusions drawn from theory are presented, the theory itself has been avoided. There are a number of advantages in learning the empirical facts before learning the theory. First of all, in interpreting spectra one usually has to rely on his knowledge of the accumulated empirical correlations much more than on his knowledge of the theory. In fact, one could know all of the theory and still not b~ able to interpret spectra unless he also knew the empirical facts. Secondly, the theory is much more easilyunderstoodafter the facts have been mastered.
Author: Neil E. Jacobsen
Publisher: John Wiley & Sons
ISBN: 1119047145
Category : Science
Languages : en
Pages : 652
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Book Description
Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings
Author: Antonio Randazzo
Publisher: Loghia Di Amoresano Claudia
ISBN: 9788895122403
Category : Medical
Languages : en
Pages : 344
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Book Description
This book is designed to provide undergraduate and graduate students with practical strategies, methods and explanations to interpret the NMR spectra of small organic molecules. In particular, it is organized in a way that basic 1H- and 13iNMR concepts are introduced and immediately applied in a number of problems, solved and discussed in a step-by-step fashion. It contains almost exclusively real NMR data and it describes how to interpret the chemical shift, intensity and splitting pattern of the proton and carbon NMR signals (Chapters 1-5), paying attention to the effects of the magnetically non-equivalent nuclei (Chapter 4). The role of the solvent is also explained (Chapter 6), and a description of the interpretation of the most common two-dimensional NMR experiments is reported in Chapter 7. Chapter 8 is dedicated to the strategy for structural elucidation, while Chapter 9 contains exclusively summary problems.
Author: Yong-Cheng Ning
Publisher: John Wiley & Sons
ISBN: 0470828315
Category : Science
Languages : en
Pages : 426
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Book Description
Although there are a number of books in this field, most of them lack an introduction of comprehensive analysis of MS and IR spectra, and others do not provide up-to-date information like tandem MS. This book fills the gap. The merit of this book is that the author will not only introduce knowledge for analyzing nuclear magnetic resonance spectra including 1H spectra (Chapter 1), 13C spectra (Chapter 2) and 2D NMR spectra (Chapter 3), he also arms readers systemically with knowledge of Mass spectra (including EI MS spectra and MS spectra by using soft ionizations) (Chapter 4) and IR spectra (Chapter 5). In each chapter the author presents very practical application skills by providing various challenging examples. The last chapter (Chapter 6) provides the strategy, skills and methods on how to identify an unknown compound through a combination of spectra. Based on nearly 40 years researching and teaching experience, the author also proposes some original and creative ideas, which are very practical for spectral interpretation.
Author: Roman Valiulin
Publisher: Walter de Gruyter GmbH & Co KG
ISBN: 3110608464
Category : Science
Languages : en
Pages : 247
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Book Description
A visual guide for the interpretation of complex 1H-NMR spectra with a concise and illustrative practice problems section. This book is an easy-to-grasp source for (organic) chemists and students that want to understand and practice NMR spectroscopy.
Author: Raymond J. Abraham
Publisher: John Wiley & Sons
ISBN: 0470721812
Category : Science
Languages : en
Pages : 392
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Book Description
Provides a theoretical introduction to graduate scientists and industrial researchers towards the understanding of the assignment of 1H NMR spectra Discusses, and includes on enclosed CD, one of the best, the fastest and most applicable pieces of NMR prediction software available Allows students of organic chemistry to solve problems on 1H NMR with access to over 500 assigned spectra
Author: Neil E. Jacobsen
Publisher: John Wiley & Sons
ISBN: 0470173343
Category : Science
Languages : en
Pages : 686
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Book Description
NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.
Author: Metin Balci
Publisher: Elsevier
ISBN: 0080525539
Category : Science
Languages : en
Pages : 441
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Book Description
Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful and theoretically complex analytical tool. Basic 1H- and 13C-NMR Spectroscopy provides an introduction to the principles and applications of NMR spectroscopy. Whilst looking at the problems students encounter when using NMR spectroscopy, the author avoids the complicated mathematics that are applied within the field. Providing a rational description of the NMR phenomenon, this book is easy to read and is suitable for the undergraduate and graduate student in chemistry. - Describes the fundamental principles of the pulse NMR experiment and 2D NMR spectra - Easy to read and written with the undergraduate and graduate chemistry student in mind - Provides a rational description of NMR spectroscopy without complicated mathematics
Author: James Keeler
Publisher: John Wiley & Sons
ISBN: 1119964938
Category : Science
Languages : en
Pages : 533
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Book Description
This text is aimed at people who have some familiarity with high-resolution NMR and who wish to deepen their understanding of how NMR experiments actually ‘work’. This revised and updated edition takes the same approach as the highly-acclaimed first edition. The text concentrates on the description of commonly-used experiments and explains in detail the theory behind how such experiments work. The quantum mechanical tools needed to analyse pulse sequences are introduced set by step, but the approach is relatively informal with the emphasis on obtaining a good understanding of how the experiments actually work. The use of two-colour printing and a new larger format improves the readability of the text. In addition, a number of new topics have been introduced: How product operators can be extended to describe experiments in AX2 and AX3 spin systems, thus making it possible to discuss the important APT, INEPT and DEPT experiments often used in carbon-13 NMR. Spin system analysis i.e. how shifts and couplings can be extracted from strongly-coupled (second-order) spectra. How the presence of chemically equivalent spins leads to spectral features which are somewhat unusual and possibly misleading, even at high magnetic fields. A discussion of chemical exchange effects has been introduced in order to help with the explanation of transverse relaxation. The double-quantum spectroscopy of a three-spin system is now considered in more detail. Reviews of the First Edition “For anyone wishing to know what really goes on in their NMR experiments, I would highly recommend this book” – Chemistry World “...I warmly recommend for budding NMR spectroscopists, or others who wish to deepen their understanding of elementary NMR theory or theoretical tools” – Magnetic Resonance in Chemistry
Author: John L. Markley
Publisher: Oxford University Press
ISBN: 0195094689
Category : Medical
Languages : en
Pages : 375
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Book Description
This book presents a critical assessment of progress on the use of nuclear magnetic resonance spectroscopy to determine the structure of proteins, including brief reviews of the history of the field along with coverage of current clinical and in vivo applications. The book, in honor of Oleg Jardetsky, one of the pioneers of the field, is edited by two of the most highly respected investigators using NMR, and features contributions by most of the leading workers in the field. It will be valued as a landmark publication that presents the state-of-the-art perspectives regarding one of today's most important technologies.
