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Author: Andrzej Katrusiak
Publisher: Springer Science & Business Media
ISBN: 140202102X
Category : Science
Languages : en
Pages : 574
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Book Description
Despite the tremendous advances in the techniques and equipment for carrying out high-pressure crystallography, the application or exploration of the high-pressure variable in detailed structural studies remains rare. The chapters in this book provide a set of lecture notes and supplementary material for a course on high pressure crystallography. The material comprises state-of-the-art reviews of high-pressure experiments using X-ray and neutron diffraction techniques at synchrotron and neutron facilities and in the laboratory, as well as complementary experimental high-pressure techniques and theoretical methods for investigating matter at elevated pressures. The materials studies range from elemental solids and liquids to inorganic compounds, minerals, organic compounds, clathrates and pharmaceutical compounds, to large biological molecules such as proteins and viruses. The book provides a reference for workers in high-pressure science wishing to learn more about crystallography and for established crystallographers potentially interested in high pressure as a variable, as well as an introductory guide to new researchers in the field.
Author: Andrzej Katrusiak
Publisher: Springer Science & Business Media
ISBN: 140202102X
Category : Science
Languages : en
Pages : 574
Get Book Here
Book Description
Despite the tremendous advances in the techniques and equipment for carrying out high-pressure crystallography, the application or exploration of the high-pressure variable in detailed structural studies remains rare. The chapters in this book provide a set of lecture notes and supplementary material for a course on high pressure crystallography. The material comprises state-of-the-art reviews of high-pressure experiments using X-ray and neutron diffraction techniques at synchrotron and neutron facilities and in the laboratory, as well as complementary experimental high-pressure techniques and theoretical methods for investigating matter at elevated pressures. The materials studies range from elemental solids and liquids to inorganic compounds, minerals, organic compounds, clathrates and pharmaceutical compounds, to large biological molecules such as proteins and viruses. The book provides a reference for workers in high-pressure science wishing to learn more about crystallography and for established crystallographers potentially interested in high pressure as a variable, as well as an introductory guide to new researchers in the field.
Author: Elena Boldyreva
Publisher: Springer Science & Business Media
ISBN: 9048192579
Category : Science
Languages : en
Pages : 603
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Book Description
This unique book is devoted to the theme of crystallographic studies at high pressure. It places emphasis on the phenomena characteristic to the compressed state of matter, as well as experimental and theoretical techniques, used to study these phenomena.
Author: D. Michael P. Mingos
Publisher: Springer Nature
ISBN: 3030647439
Category : Science
Languages : en
Pages : 285
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Book Description
This volume summarises recent developments and possible future directions for small molecule X-ray crystallography. It reviews specific areas of crystallography which are rapidly developing and places them in a historical context. The interdisciplinary nature of the technique is emphasised throughout. It introduces and describes the chemical crystallographic and synchrotron facilities which have been at the cutting edge of the subject in recent decades. The introduction of new computer-based algorithms has proved to be very influential and stimulated and accelerated the growth of new areas of science. The challenges which will arise from the acquisition of ever larger databases are considered and the potential impact of artificial intelligence techniques stressed. Recent advances in the refinement and analysis of X-ray crystal structures are highlighted. In addition the recent developments in time resolved single crystal X-ray crystallography are discussed. Recent years have demonstrated how this technique has provided important mechanistic information on solid-state reactions and complements information from traditional spectroscopic measurements. The volume highlights how the prospect of being able to routinely “watch” chemical processes as they occur provides an exciting possibility for the future. Recent advances in X-ray sources and detectors that have also contributed to the possibility of dynamic single-crystal X-ray diffraction methods are presented. The coupling of crystallography and quantum chemical calculations provides detailed information about electron distributions in crystals and has resulted in a more detailed understanding of chemical bonding. The volume will be of interest to chemists and crystallographers with an interest in the synthesis, characterisation and physical and catalytic properties of solid-state materials. Postgraduate students entering the field will benefit from a historical introduction to the subject and a description of those techniques which are currently used. Since X-ray crystallography is used so widely in modern chemistry it will serve to alert senior chemists to those developments which will become routine in coming decades. It will also be of interest to the broad community of computational chemists who study chemical systems.
Author: Robert M. Hazen
Publisher: Walter de Gruyter GmbH & Co KG
ISBN: 1501508709
Category : Science
Languages : en
Pages : 604
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Book Description
Volume 41 of Reviews in Mineralogy and Geochemistry introduces to the field of high-temperature and high-pressure crystal chemistry, both as a guide to the dramatically improved techniques and as a summary of the voluminous crystal chemical literature on minerals at high temperature and pressure. The three parts of the book introduces crystal chemical considerations of special relevance to non-ambient crystallographic studies, reviews the temperature- and pressure-variation of structures in major mineral groups and presents experimental techniques for high-temperature and high-pressure studies of single crystals and polycrystalline samples as well as special considerations relating to diffractometry on samples at non-ambient conditions.
Author: E. Yu Tonkov
Publisher: CRC Press
ISBN: 1420037609
Category : Science
Languages : en
Pages : 390
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Book Description
As laboratories replace heavy hydraulic presses and bulky high-pressure chambers with miniature diamond anvils, traditional heaters with laser heating, and continue to improve methods of shock compression, there has been considerable new data obtained from the high-pressure, high-temperature modification of pure elements. The dense metallic modification of elements shows the potential for achieving superconductivity akin to theoretical predictions. Phase Transformations of Elements Under High Pressure contains the latest theoretical and experimental information on nearly 100 elements, including first-and second-phase transitions, melting lines, crystal structures of stable and metastable phases, stability of polymorphic modifications, and other useful properties and data. It emphasizes features such as changes in the liquid state, amorphization, and metallization, and provides temperature-pressure diagrams for every element. The book also describes the transitions of polymeric forms of fullerene, crystal modifications of elements stable under high pressures, and provides data that confirms their superconducting and magnetic properties. This handbook will be a lasting reference for scientists in a broad range of disciplines, including solid-state physics, chemistry, crystallography, mineralogy, and materials science.
Author: John Loveday
Publisher: CRC Press
ISBN: 1439814287
Category : Science
Languages : en
Pages : 344
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Book Description
High-pressure science has undergone a revolution in the last 15 years. The development of intense new x-ray and neutron sources, improved detectors, new instrumentation, greatly increased computation power, and advanced computational algorithms have enabled researchers to determine the behavior of matter at static pressures in excess of 400 GPa. Shock-wave techniques have allowed access to the experimental pressure-temperature range beyond 1 TPa and 10,000 K. High-Pressure Physics introduces the current state of the art in this field. Based on lectures presented by leading researchers at the 63rd Scottish Universities Summer School in Physics, the book summarizes the latest experimental and theoretical techniques. Highlighting applications in a range of physics disciplines—from novel materials synthesis to planetary interiors—this book cuts across many areas and supplies a solid grounding in high-pressure physics. Chapters cover a wide array of topics and techniques, including: High-pressure devices The design of pressure cells Electrical transport experiments The fabrication process for customizing diamond anvils Equations of state (EOS) for solids in a range of pressures and temperatures Crystallography, optical spectroscopy, and inelastic x-ray scattering (IXS) techniques Magnetism in solids The internal structure of Earth and other planets Measurement and control of temperature in high-pressure experiments Solid state chemistry and materials research at high pressure Liquids and glasses The study of hydrogen at high density A resource for graduate students and young researchers, this accessible reference provides an overview of key research areas and applications in high-pressure physics.
Author: Elena Boldyreva
Publisher: Springer Science & Business Media
ISBN: 9048192609
Category : Science
Languages : en
Pages : 602
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Book Description
This unique book is devoted to the theme of crystallographic studies at high pressure. It places emphasis on the phenomena characteristic to the compressed state of matter, as well as experimental and theoretical techniques, used to study these phenomena.
Author: Anthony Michael Glazer
Publisher: Oxford University Press
ISBN: 0198717598
Category : Science
Languages : en
Pages : 169
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Book Description
A long history -- Symmetry -- Crystal structures -- Diffraction -- Seeing atoms -- Sources of radiation
Author: Eberhard J. Jaeschke
Publisher: Springer
ISBN: 9783319143934
Category : Science
Languages : en
Pages : 0
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Book Description
Hardly any other discovery of the nineteenth century did have such an impact on science and technology as Wilhelm Conrad Röntgen’s seminal find of the X-rays. X-ray tubes soon made their way as excellent instruments for numerous applications in medicine, biology, materials science and testing, chemistry and public security. Developing new radiation sources with higher brilliance and much extended spectral range resulted in stunning developments like the electron synchrotron and electron storage ring and the freeelectron laser. This handbook highlights these developments in fifty chapters. The reader is given not only an inside view of exciting science areas but also of design concepts for the most advanced light sources. The theory of synchrotron radiation and of the freeelectron laser, design examples and the technology basis are presented. The handbook presents advanced concepts like seeding and harmonic generation, the booming field of Terahertz radiation sources and upcoming brilliant light sources driven by laser-plasma accelerators. The applications of the most advanced light sources and the advent of nanobeams and fully coherent x-rays allow experiments from which scientists in the past could not even dream. Examples are the diffraction with nanometer resolution, imaging with a full 3D reconstruction of the object from a diffraction pattern, measuring the disorder in liquids with high spatial and temporal resolution. The 20th century was dedicated to the development and improvement of synchrotron light sources with an ever ongoing increase of brilliance. With ultrahigh brilliance sources, the 21st century will be the century of x-ray lasers and their applications. Thus, we are already close to the dream of condensed matter and biophysics: imaging single (macro)molecules and measuring their dynamics on the femtosecond timescale to produce movies with atomic resolution.
Author: Kari Rissanen
Publisher: Springer Science & Business Media
ISBN: 3642274064
Category : Science
Languages : en
Pages : 190
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Book Description
Computational Studies of Crystal Structure and Bonding, by Angelo Gavezzotti Cryo-Crystallography: Diffraction at Low Temperature and More, by Piero Macchi High-Pressure Crystallography, by Malcolm I. McMahon Chemical X-Ray Photodiffraction: Principles, Examples, and Perspectives, by Panče Naumov Powder Diffraction Crystallography of Molecular Solids, by Kenneth D. M. Harris
