Electrically Based Microstructural Characterization II. PDF Download
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Languages : en
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Languages : en
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Category : Materials
Languages : en
Pages : 0
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Author: Rosario A. Gerhardt
Publisher: Cambridge University Press
ISBN: 9781107413559
Category : Technology & Engineering
Languages : en
Pages : 384
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Book Description
This book provides a forum for researchers who have been using a variety of electrical measurements as a means to obtain microstructural information about their materials. Microstructure in this context includes features at all length scales - atomic to macroscopic. Even though numerous examples of microstructure/electrical property correlations exist, this book focuses on the myriad of applications that have already been successful. In addition, advances in techniques for the interpretation of data and modelling of materials-related phenomena are emphasized. The effects of percolation and connectivity of electrical paths are of particular interest as they determine the resultant electrical response. These in turn are intimately linked to how a material is processed, what phases it contains, and how the phases are distributed in real space. All classes of materials are covered including semiconductors, electroceramics, biological materials, polymers, metals, geomaterials and a variety of composites. Topics include: advances in localized electrical testing; semiconductor and microelectronic applications; magnetic and polymeric materials; dielectrics and ferroelectrics; varistors; ionic and mixed conductors and composites and percolation systems.
Author:
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Category : Materials
Languages : en
Pages : 367
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Author:
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Category : Materials
Languages : en
Pages : 488
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Author: Rosario A. Gerhardt
Publisher:
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Category : Science
Languages : en
Pages : 406
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Among the topics of invited papers are the electrical characterization of inhomogeneous and heterogeneous systems with microstructural periodicity, impedance spectroscopy in ferromagnetic materials, the materials characterization and device performance of a CMR- ferroelectric heterostructure, and broadband dielectric spectroscopic investigations into the influence of confinement on the molecular reorientational dynamics of liquid crystals. Many papers besides the 48 selected here are expected to appear in various scientific journals. Annotation copyrighted by Book News, Inc., Portland, OR
Author: Edward J. Garboczi
Publisher: Materials Research Society
ISBN: 9781558993143
Category : Technology & Engineering
Languages : en
Pages : 0
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Impedance and/or dielectric spectroscopy are being used to monitor hydration in cements, flux solder in PC boards, sintering of ceramic materials, mechanical and environmental degradation of materials, etc. This is the first book from MRS to focus on the application of electrical measurements for the detection of microstructural features at all length scales (atomic to macroscopic). The electrical techniques discussed include dc and ac resistivity measurements, complex impedance analysis, multiplane analysis and various other methods such as electron energy loss spectroscopy, ellipsometry, capacitance voltage measurements and others. Research covers all classes of materials including electroceramics, biological materials, polymers, metals and a variety of composites. Advances in the techniques for the interpretation of data and monitoring of materials-related phenomena are emphasized. Topics include: advances in experimental techniques and applications; advances in interpretation of frequency dependence; characterization of defects; composition and structure profiling; electrode effects; grain boundary effects; composites and porous materials.
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Category : Materials
Languages : en
Pages : 435
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Author: Materials Research Society
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Author: Ratnanabha Sain
Publisher: Stanford University
ISBN:
Category :
Languages : en
Pages : 224
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This dissertation describes numerical experiments quantifying the influence of pore-scale heterogeneities and their evolution on macroscopic elastic, electrical and transport properties of porous media. We design, implement and test a computational recipe to construct granular packs and consolidated microstructures replicating geological processes and to estimate the link between process-to-property trends. This computational recipe includes five constructors: a Granular Dynamics (GD) simulation, an Event Driven Molecular Dynamics (EDMD) simulation and three computational diagenetic schemes; and four property estimators based on GD for elastic, finite-elements (FE) for elastic and electrical conductivity, and Lattice-Boltzmann method (LBM) for flow property simulations. Our implementation of GD simulation is capable of constructing realistic, frictional, jammed sphere packs under isotropic and uniaxial stress states. The link between microstructural properties in these packs, like porosity and coordination number (average number of contacts per grain), and stress states (due to compaction) is non-unique and depends on assemblage process and inter-granular friction. Stable jammed packs having similar internal stress and coordination number (CN) can exist at a range of porosities (38-42%) based on how fast they are assembled or compressed. Similarly, lower inter-grain friction during assemblage creates packs with higher coordination number and lower porosity at the same stress. Further, the heterogeneities in coordination number, spatial arrangement of contacts, the contact forces and internal stresses evolve with compaction non-linearly. These pore-scale heterogeneities impact effective elastic moduli, calculated by using infinitesimal perturbation method. Simulated stress-strain relationships and pressure-dependent elastic moduli for random granular packs show excellent match with laboratory experiments, unlike theoretical models based on Effective Medium Theory (EMT). We elaborately discuss the reasons why Effective Medium Theory (EMT) fails to correctly predict pressure-dependent elastic moduli, stress-strain relationships and stress-ratios (in uniaxial compaction) of granular packs or unconsolidated sediments. We specifically show that the unrealistic assumption of homogeneity in disordered packs and subsequent use of continuum elasticity-based homogeneous strain theory creates non-physical packs, which is why EMT fails. In the absence of a rigorous theory which can quantitatively account for heterogeneity in random granular packs, we propose relaxation corrections to amend EMT elastic moduli predictions. These pressure-dependent and compaction-dependent (isotropic or uniaxial) correction factors are rigorously estimated using GD simulation without non-physical approximations. Further, these correction factors heuristically represent the pressure-dependent heterogeneity and are also applicable for amending predictions of theoretical cementation models, which are conventionally used for granular packs. For predicting stress-ratios in uniaxial compaction scenario, we show the inappropriateness of linear elasticity-based equations, which use elastic constants only and do not account for dissipative losses like grain sliding. We further implement and test a computational recipe to construct consolidated microstructures based on different geological scenarios, like sorting, compaction, cementation types and cement materials. Our diagenetic trends of elastic, electrical and transport properties show excellent match with laboratory experiments on core plugs. This shows the feasibility of implementing a full-scale computational-rock-physics-based laboratory to construct and estimate properties based on geological processes. However, the elastic property estimator (FE simulation) shows limitations of finite resolution while computing elastic properties of unconsolidated sediments and fluid-saturated microstructures.
