Author: Robert F. Overman
Publisher:
ISBN:
Category : Plutonium
Languages : en
Pages : 16
Book Description
Analytical Method for In-line Plutonium Analyses
Author: Robert F. Overman
Publisher:
ISBN:
Category : Plutonium
Languages : en
Pages : 16
Book Description
Publisher:
ISBN:
Category : Plutonium
Languages : en
Pages : 16
Book Description
Analytical Method for Inline Plutonium Analyses
Author:
Publisher:
ISBN:
Category :
Languages : en
Pages :
Book Description
Laboratory studies demonstrated the feasibility of a colorimetric method for the in-line analysis of plutonium(III) and plutonium(IV) in the Purex process. Negligible interference was caused by normal variations in the concentration of nitric acid, nitrous acid, or ferric sulfate. (auth).
Publisher:
ISBN:
Category :
Languages : en
Pages :
Book Description
Laboratory studies demonstrated the feasibility of a colorimetric method for the in-line analysis of plutonium(III) and plutonium(IV) in the Purex process. Negligible interference was caused by normal variations in the concentration of nitric acid, nitrous acid, or ferric sulfate. (auth).
A Colorimeter for In-line Analysis of Uranium and Plutonium Solutions
Author: Donald W. Colvin
Publisher:
ISBN:
Category : Colorimetric analysis
Languages : en
Pages : 28
Book Description
Publisher:
ISBN:
Category : Colorimetric analysis
Languages : en
Pages : 28
Book Description
Chemical Analyses of Plutonium and Plutonium Alloys
Author: Rose Kraft
Publisher:
ISBN:
Category : Plutonium
Languages : en
Pages : 112
Book Description
Publisher:
ISBN:
Category : Plutonium
Languages : en
Pages : 112
Book Description
Analytical Procedures for the Plutonium Metal Fabrication Process
Author: L. F. Kendall
Publisher:
ISBN:
Category : Metallurgy
Languages : en
Pages : 20
Book Description
Publisher:
ISBN:
Category : Metallurgy
Languages : en
Pages : 20
Book Description
Acid Dissolution Method for the Analysis of Plutonium in Soil
Author: E. L. Whittaker
Publisher:
ISBN:
Category : Analytical chemistry
Languages : en
Pages : 72
Book Description
Publisher:
ISBN:
Category : Analytical chemistry
Languages : en
Pages : 72
Book Description
Quantitative Metallography of Plutonium Using Point-count Techniques
Author: R. L. Greeson
Publisher:
ISBN:
Category : Metallorgraphy
Languages : en
Pages : 36
Book Description
Publisher:
ISBN:
Category : Metallorgraphy
Languages : en
Pages : 36
Book Description
Nuclear Science Abstracts
Author:
Publisher:
ISBN:
Category : Nuclear energy
Languages : en
Pages : 1108
Book Description
NSA is a comprehensive collection of international nuclear science and technology literature for the period 1948 through 1976, pre-dating the prestigious INIS database, which began in 1970. NSA existed as a printed product (Volumes 1-33) initially, created by DOE's predecessor, the U.S. Atomic Energy Commission (AEC). NSA includes citations to scientific and technical reports from the AEC, the U.S. Energy Research and Development Administration and its contractors, plus other agencies and international organizations, universities, and industrial and research organizations. References to books, conference proceedings, papers, patents, dissertations, engineering drawings, and journal articles from worldwide sources are also included. Abstracts and full text are provided if available.
Publisher:
ISBN:
Category : Nuclear energy
Languages : en
Pages : 1108
Book Description
NSA is a comprehensive collection of international nuclear science and technology literature for the period 1948 through 1976, pre-dating the prestigious INIS database, which began in 1970. NSA existed as a printed product (Volumes 1-33) initially, created by DOE's predecessor, the U.S. Atomic Energy Commission (AEC). NSA includes citations to scientific and technical reports from the AEC, the U.S. Energy Research and Development Administration and its contractors, plus other agencies and international organizations, universities, and industrial and research organizations. References to books, conference proceedings, papers, patents, dissertations, engineering drawings, and journal articles from worldwide sources are also included. Abstracts and full text are provided if available.
Plutonium Recycle Test Reactor Final Safeguards Analysis
Author: Hanford Atomic Products Operation. Reactor Engineering Development Operation
Publisher:
ISBN:
Category : Nuclear reactors
Languages : en
Pages : 92
Book Description
Publisher:
ISBN:
Category : Nuclear reactors
Languages : en
Pages : 92
Book Description
APPLICATION OF COLUMN EXTRACTION METHOD FOR IMPURITIES ANALYSIS ON HB-LINE PLUTONIUM OXIDE IN SUPPORT OF MOX FEED PRODUCT SPECIFICATIONS.
Author:
Publisher:
ISBN:
Category :
Languages : en
Pages :
Book Description
The current mission at H-Canyon involves the dissolution of an Alternate Feedstocks 2 (AFS-2) inventory that contains plutonium metal. Once dissolved, HB-Line is tasked with purifying the plutonium solution via anion exchange, precipitating the Pu as oxalate, and calcining to form plutonium oxide (PuO2). The PuO2 will provide feed product for the Mixed Oxide (MOX) Fuel Fabrication Facility, and the anion exchange raffinate will be transferred to H-Canyon. The results presented in this report document the potential success of the RE resin column extraction application on highly concentrated Pu samples to meet MOX feed product specifications. The original 'Hearts Cut' sample required a 10000x dilution to limit instrument drift on the ICP-MS method. The instrument dilution factors improved to 125x and 250x for the sample raffinate and sample eluent, respectively. As noted in the introduction, the significantly lower dilutions help to drop the total MRL for the analyte. Although the spike recoveries were half of expected in the eluent for several key elements, they were between 94-98% after Nd tracer correction. It is seen that the lower ICD limit requirements for the rare earths are attainable because of less dilution. Especially important is the extremely low Ga limit at 0.12?g/g Pu; an ICP-MS method is now available to accomplish this task on the sample raffinate. While B and V meet the column A limits, further development is needed to meet the column B limits. Even though V remained on the RE resin column, an analysis method is ready for investigation on the ICP-MS, but it does not mean that V cannot be measured on the ICP-ES at a low dilution to meet the column B limits. Furthermore, this column method can be applicable for ICP-ES as shown in Table 3-2, in that it trims the sample of Pu, decreasing and sometimes eliminating Pu spectral interferences.
Publisher:
ISBN:
Category :
Languages : en
Pages :
Book Description
The current mission at H-Canyon involves the dissolution of an Alternate Feedstocks 2 (AFS-2) inventory that contains plutonium metal. Once dissolved, HB-Line is tasked with purifying the plutonium solution via anion exchange, precipitating the Pu as oxalate, and calcining to form plutonium oxide (PuO2). The PuO2 will provide feed product for the Mixed Oxide (MOX) Fuel Fabrication Facility, and the anion exchange raffinate will be transferred to H-Canyon. The results presented in this report document the potential success of the RE resin column extraction application on highly concentrated Pu samples to meet MOX feed product specifications. The original 'Hearts Cut' sample required a 10000x dilution to limit instrument drift on the ICP-MS method. The instrument dilution factors improved to 125x and 250x for the sample raffinate and sample eluent, respectively. As noted in the introduction, the significantly lower dilutions help to drop the total MRL for the analyte. Although the spike recoveries were half of expected in the eluent for several key elements, they were between 94-98% after Nd tracer correction. It is seen that the lower ICD limit requirements for the rare earths are attainable because of less dilution. Especially important is the extremely low Ga limit at 0.12?g/g Pu; an ICP-MS method is now available to accomplish this task on the sample raffinate. While B and V meet the column A limits, further development is needed to meet the column B limits. Even though V remained on the RE resin column, an analysis method is ready for investigation on the ICP-MS, but it does not mean that V cannot be measured on the ICP-ES at a low dilution to meet the column B limits. Furthermore, this column method can be applicable for ICP-ES as shown in Table 3-2, in that it trims the sample of Pu, decreasing and sometimes eliminating Pu spectral interferences.